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1. 发明授权

US07175871B2 Acyclic enol ethers, isomers thereof, organoleptic uses thereof and processes for preparing same 有权
标题翻译：非环烯醇醚，其异构体，感官用途及其制备方法
公开(公告)号：US07175871B2
公开(公告)日：2007-02-13
申请号：US10195663
申请日：2002-07-15
申请人： Braja Dulal Mookherjee , Anubhav P. S. Narula , Subha M. Patel , Edward Mark Arruda , Patrick M. Merritt
发明人： Braja Dulal Mookherjee , Anubhav P. S. Narula , Subha M. Patel , Edward Mark Arruda , Patrick M. Merritt
IPC分类号： A23L1/22
CPC分类号： C11B9/0015 , A23L2/56 , A23L27/202
摘要： Described are synthetically produced substantially pure enol ether compositions which are cis and/or trans isomers of enol ethers having the structures: wherein R1 is C4–C10 straight chain alkyl or C9 8-alkenyl; and wherein R2 is C1–C4 alkyl, C3–C4 2-alkenyl, C4 3-alkenyl or C10 non-allenic alkadienyl and uses thereof in imparting, augmenting or enhancing the aroma and/or taste of a consumable material such as a perfume composition, a cologne, a perfumed article such as a soap, cosmetic, hair preparation or detergent, a foodstuff, a chewing gum or an alcoholic or non-alcoholic beverage such as a carbonated beverage or fruit liquer. Also described is a process for synthesis of such enol ethers by means of (i) first forming an acetal having the structure: R1—CH2—CH(OR2)2 (ii) then carrying out a thermal decomposition reaction at pH
摘要翻译：描述的是合成生产的基本上纯的烯醇醚组合物，其是具有以下结构的烯醇醚的顺式和/或反式异构体：其中R 1是C 4 -C 10 直链烷基或C 9 -C 18链烯基; 并且其中R 2是C 1 -C 4烷基，C 3 -C 4烷基，亚链烯基，C 4-3链烯基或C 10非壬烯基二价基及其用于赋予，增强或增强消耗品的香气和/或味道的用途材料如香料组合物，古龙水，香料制品如肥皂，化妆品，毛发制剂或洗涤剂，食品，口香糖或酒精或非酒精饮料如碳酸饮料或水果汁。还描述了通过（i）首先形成具有以下结构的缩醛来合成这种烯醇醚的方法：<？in-line-formula description =“In-line Formulas”end =“lead”？> R _{1 -CH 2 -CH 2（OR 2 2）2 <？in-line-formula description =“In-line （ii）然后在pH <7下进行热分解反应，然后（iii）分馏蒸馏所得反应产物以提供烯醇醚。}

2. 发明授权

US4108876A 5-Methyl-alpha[(methylthio)methyl]-2-furan acrolein 失效
标题翻译： 5-甲基-α{8（甲硫基）甲基{9-2-呋喃丙烯醛
公开(公告)号：US4108876A
公开(公告)日：1978-08-22
申请号：US827211
申请日：1977-08-24
申请人： Donald Arthur Withycombe , Anne Hruza , Manfred Hugo Vock , Christopher Giacino , Braja Dulal Mookherjee , Alan Owen Pittet , William L. Schreiber
发明人： Donald Arthur Withycombe , Anne Hruza , Manfred Hugo Vock , Christopher Giacino , Braja Dulal Mookherjee , Alan Owen Pittet , William L. Schreiber
IPC分类号： A23L27/20 , C07C67/00 , C07C313/00 , C07C323/22 , C07D307/46
CPC分类号： C07D307/46 , A23L27/204 , A23L27/2052 , C07C323/00
摘要： Processes and compositions are described for use in foodstuff flavors and as foodstuff article aroma and taste augmenting and enhancing materials of at least one alpha-substituted alkylidene methionals having the structure: ##STR1## wherein R.sub.1 or R.sub.2 is one of the moieties: ##STR2## AND THE OTHER IS HYDROGEN OR METHYL. Addition of one or more alpha-substituted alkylidene methionals to foodstuff flavorings or to foostuffs is indicated to produce the following aroma and flavor characteristics, in the alternative taken together:AromaPotato; Methional-like; Green; Hydrolyzed vegetable protein-like; Chicken-like; Cabbage; Green potato; Green weedy; Broccoli-like; and Green bean-like.FlavorPotato; Metallic; Sulfury-green; Cabbage-like; Chicken; Mushroom-like; Green-weedy; Broccoli-like; and Green bean-like. The compounds of our invention are useful in augmenting or enhancing the flavor and aroma nuances of vegetable (including potato and cabbage) and chicken flavors.
摘要翻译：描述了用于食品香料的方法和组合物，以及作为食品制品香气和味道增强和增强至少一种具有以下结构的α-取代的亚烷基甲基的材料：其中R 1或R 2是其中一个部分： ; 或，另一个是氢或甲基。指示在食品调味料或假粉末中加入一种或多种α-取代的亚烷基甲基，以产生以下芳香和风味特征，在替代方案中：芳香马铃薯; 类似地绿色; 水解植物蛋白样; 鸡肉样卷心菜; 青薯绿色杂草西兰花状和绿豆样。风味土豆金属; 硫磺绿卷心菜样鸡; 蘑菇状绿色杂草西兰花状和绿豆样。本发明的化合物可用于增强或增强蔬菜（包括马铃薯和卷心菜）和鸡肉风味的风味和香气的细微差别。

3. 发明授权

US4092333A 2-Acyl-5-substituted thiatetrahydrofuran-4-ones 失效
标题翻译： 2-酰基-5-取代的四氢呋喃-4-酮
公开(公告)号：US4092333A
公开(公告)日：1978-05-30
申请号：US819888
申请日：1977-07-28
申请人： Braja Dulal Mookherjee , William J. Evers , Alfred E. Goossens
发明人： Braja Dulal Mookherjee , William J. Evers , Alfred E. Goossens
IPC分类号： A24B15/40 , C07D307/32 , C07D307/64 , C11B9/00
CPC分类号： C07D307/32 , A24B15/406 , C07D307/64 , C11B9/0076
摘要： Described are 2-acyl-5-substituted thiatetrahydrofuran-4-ones having the generic structure: ##STR1## wherein R.sub.1, R.sub.2, R.sub.1 ' and R.sub.2 ' are the same or different and each represents hydrogen or methyl and wherein R.sub.3 represents one of C.sub.1 -C.sub.9 alkyl, benzyl, phenyl, substituted or unsubstituted allyl having the structure: ##STR2## substituted or unsubstituted 3-furyl having the structure: (wherein R.sub.4 and R.sub.8 are the same or different and each represents hydrogen or methyl) hydroxy alkyl, oxoalkyl, hydroxycycloalkyl or oxocycloalkyl having the structure: ##STR3## (wherein R.sub.5 and R.sub.6, taken separately, represent hydrogen or C.sub.1 -C.sub.3 alkyl or R.sub.5 and R.sub.6, taken together, complete a cycloalkyl group and wherein Q is one of the moieties: ##STR4## The 2-acyl-5-substituted thiatetrahydrofuran-4-ones of our invention have organoleptic properties which make them useful for augmenting or enhancing the aroma or flavor of foodstuffs, tobaccos and the aroma of perfumes and perfumed articles.
摘要翻译：描述了具有以下通用结构的2-酰基-5-取代的硫代四氢呋喃-4-酮：其中R 1，R 2，R 1'和R 2'相同或不同，各自表示氢或甲基，并且其中R 3表示C1 -C9烷基，苄基，苯基，具有以下结构的取代或未取代的烯丙基：具有以下结构的取代或未取代的3-呋喃基：其中R 4和R 8相同或不同，各自表示氢或甲基）羟基烷基，氧代烷基，羟基环烷基或氧代环烷基，其结构为：其中R 5和R 6分别代表氢或C 1 -C 3烷基或R 5和R 6一起形成环烷基，其中Q是部分之一：本发明的2-酰基-5-取代的硫代四氢呋喃-4-酮具有感官特性，使其可用于增强或增强食品，烟草的香气或风味以及香料和香料制品的香气。

4. 发明授权

US06894020B2 Macrocylic musk composition, organoleptic uses thereof and process for preparing same 有权
标题翻译：大麝香麝香组合物，感官用途及其制备方法
公开(公告)号：US06894020B2
公开(公告)日：2005-05-17
申请号：US10760691
申请日：2004-01-20
申请人： Braja Dulal Mookherjee , Anubhav P. S. Narula , Michael G. Monteleone , Robert W. Trenkle
发明人： Braja Dulal Mookherjee , Anubhav P. S. Narula , Michael G. Monteleone , Robert W. Trenkle
IPC分类号： C11B9/00 , A61K7/46
CPC分类号： C11B9/0038
摘要： Described are mixtures consisting essentially of oxomacrocyclic compounds containing greater than about 40 weight % Δ3-cyclotetradecen-1-one and greater than about 40 weight % cyclotetradecanone and less than about 5 weight %, of Δ2-cyclotetradecen-1-one, perfumery uses thereof and chemo-selective catalytic hydrogen process for preparing same by hydrogenating mixtures containing significant concentrations, greater than 15 weight %, of Δ2-cyclotetradecen-1-one. The oxocarbocyclic compound-containing mixtures have advantageous musk aroma imparting, augmenting and enhancing perfumery properties causing the mixtures to be useful in perfume compositions, perfumed articles and perfumed polymers, including particles and fibers produced therefrom.
摘要翻译：描述了基本上由含有大于约40重量％的三环多环十四碳烯-1-酮和大于约40重量％的环十四烷酮和小于约5重量％的ΔOSUP的氧杂环丙烷化合物 > 2环 - 十四碳烯-1-酮，其香料用途和化学选择性催化氢法用于制备它们，通过氢化含有大于15重量％的Δ2 O 2的显着浓度的混合物，环十四碳烯-1-酮。含有含羧基环化合物的混合物具有有利的麝香香气赋予，增强和增强香料特性，使混合物可用于香料组合物，香料制品和加香聚合物，包括由其制备的颗粒和纤维。

5. 发明授权

US4107209A 1-[3-(Methylthio)butyryl]-2,6,6-trimethyl-cyclohexene and the 1,3-cyclohexadiene analog 失效
标题翻译： 1- {8 3-（甲硫基）丁酰基{9 -2,6,6-三甲基 - 环己烯和1,3-环己二烯类似物
公开(公告)号：US4107209A
公开(公告)日：1978-08-15
申请号：US774055
申请日：1977-03-03
申请人： Richard A. Wilson , Braja Dulal Mookherjee , Anne Sanderson Hruza , Manfred Hugo Vock , Louis Schmitt Frederick , Joaquin Francisco Vinals
发明人： Richard A. Wilson , Braja Dulal Mookherjee , Anne Sanderson Hruza , Manfred Hugo Vock , Louis Schmitt Frederick , Joaquin Francisco Vinals
IPC分类号： A23L27/20 , A24B3/12 , A24B15/34 , A61K8/35 , A61K47/20 , A61Q13/00 , C07C67/00 , C07C313/00 , C07C323/22 , C07C403/00 , C11B9/00 , C11D3/50 , C11D9/44 , C07C49/61
CPC分类号： C07C323/22 , A24B15/34 , C11B9/0034 , C07C2101/16 , Y10S514/974
摘要： The compounds 1-[3-(methylthio)butyryl]-2,6,6-trimethyl-cyclohexene and/or the corresponding 1,3-cyclohexadiene analog having the generic structure: ##STR1## wherein the dashed line could be a single or a double carbon-carbon bond and processes and compositions containing same are described for the use in foodstuff, chewing gum, toothpaste and medicinal product flavor and aroma, tobacco flavor and aroma and perfume and perfumed article aroma augmenting and enhancing compositions and for use in foodstuffs, tobacco, perfume and perfumed article aroma imparting compositions; produced by a process illustrated by the reaction: ##STR2## The above-mentioned compounds produce: (A) In food flavorings, sweet, black tea-like, cocoa-like, damascenone-like, chocolate-like, dried fruit-like, rose petal-like aroma characteristics and sweet, black-tea-like, cocoa-like, damascenone-like, chocolate-like, tobacco-like, dried fruit-like and rose petal-like flavor characteristics;(b) In tobacco, a sweet honey-like, rich, slightly fruity, dried fruit-like, hay tobacco-like, woody, cedarwood, raspberry-like, blackcurrant-like aroma prior to smoking and sweet, fruity, hay tobacco and Virginia tobacco-like aroma on smoking; and(c) In perfumes, fruity, floral, natural rose oil-like and earthy aromas with potato top notes and minty, tomato vine, Brussel sprout-like and woody undertones.
摘要翻译：化合物1- [3-（甲硫基）丁酰基] -2,6,6-三甲基 - 环己烯和/或具有通用结构的相应的1,3-环己二烯类似物：其中虚线可以是单个或描述了用于食品，口香糖，牙膏和医药产品风味和香气，烟草风味和芳香和香料和香料制品香气增强和增强组合物并用于食品中的双碳 - 碳键和含有它们的方法和组合物，烟草，香水和香料制品香气赋予组合物; 由反应说明的方法制备：上述化合物产生：

6. 发明授权

US4064279A Alpha-substituted alkylidene methionals and uses thereof in foodstuffs and flavors for foodstuffs 失效
标题翻译： α-取代的亚烷基甲基及其在食品和食品中的用途
公开(公告)号：US4064279A
公开(公告)日：1977-12-20
申请号：US753462
申请日：1976-12-22
申请人： Donald Arthur Withycombe , Anne Hruza , Manfred Hugo Vock , Christopher Giacino , Braja Dulal Mookherjee , Alan Owen Pittet , William L. Schreiber
发明人： Donald Arthur Withycombe , Anne Hruza , Manfred Hugo Vock , Christopher Giacino , Braja Dulal Mookherjee , Alan Owen Pittet , William L. Schreiber
IPC分类号： A23L27/20 , C07C67/00 , C07C313/00 , C07C323/22 , C07D307/46 , A23L1/226 , A23L1/231
CPC分类号： C07D307/46 , A23L27/204 , A23L27/2052 , C07C323/00
摘要： Processes and compositions are described for use in foodstuff flavors and as foodstuff article aroma and taste augmenting and enhancing materials of at least one alpha-substituted alkylidene methionals having the structure: ##STR1## wherein R.sub.1 or R.sub.2 is one of the moieties: ##STR2## AND THE OTHER IS HYDROGEN OR METHYL. Addition of one or more alpha-substituted alkylidene methionals to foodstuff flavorings or to foodstuffs is indicated to produce the following aroma and flavor characteristics, in the alternative taken together:AROMAPotato;Methional-like;Green;Hydrolyzed vegetable protein-like;Chicken-like;Cabbage;Green potato;Green weedy;Broccoli-like; andGreen bean-like.FLAVORPotato;Metallic;Sulfury-green;Cabbage-like;Chicken;Mushroom-like;Green-weedy;Broccoli-like; andGreen bean-like.The compounds of our invention are useful in augmenting or enhancing the flavor and aroma nuances of vegetable (including potato and cabbage) and chicken flavors.
摘要翻译：描述了用于食品香料的方法和组合物，以及作为食品制品香气和味道增强和增强至少一种具有以下结构的α-取代的亚烷基甲基的材料：其中R 1或R 2是其中一个部分：或，另一个是氢或甲基。在食品调味料或食品中加入一种或多种α-取代的亚烷基甲基，可以在以下方面产生以下芳香和风味特征：AROMA Potato; 地缘样绿色; 水解植物蛋白样; 鸡肉样卷心菜; 青薯绿色杂草西兰花状和绿豆样。金属; 硫磺绿卷心菜样鸡; 蘑菇状绿色杂草西兰花状和绿豆样。

7. 发明授权

US06720303B2 Macrocyclic musk composition, organoleptic uses thereof and process for preparing same 有权
标题翻译：大环麝香组合物，感官用途及其制备方法
公开(公告)号：US06720303B2
公开(公告)日：2004-04-13
申请号：US10015975
申请日：2001-11-01
申请人： Braja Dulal Mookherjee , Anubhav P. S. Narula , Michael G. Monteleone , Robert W. Trenkle
发明人： Braja Dulal Mookherjee , Anubhav P. S. Narula , Michael G. Monteleone , Robert W. Trenkle
IPC分类号： A61K746
CPC分类号： C11B9/0038
摘要： Described are mixtures consisting essentially of oxomacrocyclic compounds containing greater than about 40 weight % &Dgr;3-cyclotetradecen-1-one and greater than about 40 weight % cyclotetradecanone and less than about 5 weight %, of &Dgr;2-cyclo-tetradecen-1-one, perfumery uses thereof and chemo-selective catalytic hydrogen process for preparing same by hydrogenating mixtures containing significant concentrations, greater than 15 weight %, of &Dgr;2-cyclotetradecen-1-one. The oxocarbocyclic compound-containing mixtures have advantageous musk aroma imparting, augmenting and enhancing perfumery properties causing the mixtures to be useful in perfume compositions, perfumed articles and perfumed polymers, including particles and fibers produced therefrom.
摘要翻译：描述的是基本上由含有大于约40重量％的Δ3-环十四碳烯-1-酮和大于约40重量％的环十四烷酮和小于约5重量％的Δ2-环十四碳烯的氧杂环丙烷化合物 -1-酮，其香料用途和化学选择性催化氢法制备，通过氢化含有大于15重量％的Δ2-环十四碳烯-1-酮的显着浓度的混合物。含有含羧基环化合物的混合物具有有利的麝香香气赋予，增强和增强香料特性，使混合物可用于香料组合物，香料制品和加香聚合物，包括由其制备的颗粒和纤维。

8. 发明授权

US4093752A Flavoring with 2,4,6-triisobutyl-1,3,5-trioxane 失效
标题翻译：用2,4,6-三异丁基-1,3,5-三恶烷调味
公开(公告)号：US4093752A
公开(公告)日：1978-06-06
申请号：US807056
申请日：1977-06-16
申请人： Donald Arthur Withycombe , Braja Dulal Mookherjee , Manfred Hugo Vock , Joaquin Francisco Vinals
发明人： Donald Arthur Withycombe , Braja Dulal Mookherjee , Manfred Hugo Vock , Joaquin Francisco Vinals
IPC分类号： C07D323/06 , A23G4/00 , A23G4/06 , A23L27/20 , A24B15/40 , C07D263/06 , C07D263/12 , C07D323/04 , A23L1/226
CPC分类号： A23G4/06 , A23L27/2052 , A23L27/2056 , A24B15/403 , C07D263/12 , C07D323/04
摘要： Processes and compositions are described for the use in foodstuff, chewing gum, toothpaste and medicinal product flavor and aroma and tobacco flavor and aroma augmenting, modifying, enhancing and imparting compositions and as foodstuff, chewing gum, toothpaste, medicinal product and tobacco aroma or flavor imparting, augmenting or enhancing materials of 2,4,6-triisobutyl-1,3,5,trioxane.
摘要翻译：描述的方法和组合物用于食品，口香糖，牙膏和药用产品香料，香气和烟草香味和香气增强，改性，增强和赋予组合物以及作为食品，口香糖，牙膏，药用产品和烟草香气或香料赋予，增强或增强2,4,6-三异丁基-1,3,5，三恶烷的材料。

9. 发明授权

US4040987A 2-Alkyl-substituted-4,5-dimethyl thiazoline perfume and cologne compositions 失效
标题翻译： 2-烷基取代-4,5-二甲基噻唑啉香料和古龙水组合物
公开(公告)号：US4040987A
公开(公告)日：1977-08-09
申请号：US730653
申请日：1976-10-07
申请人： Edward J. Shuster , Donald Arthur Withycombe , Braja Dulal Mookherjee , Cynthia J. Mussinan
发明人： Edward J. Shuster , Donald Arthur Withycombe , Braja Dulal Mookherjee , Cynthia J. Mussinan
IPC分类号： C07D277/10 , C11B9/00
CPC分类号： C11D3/0084 , C07D277/10 , C11B9/0096
摘要： Perfume and fragrance compositions and perfumed articles including soaps, detergents, powders, as well as colognes containing 2-alkyl-substituted-4,5-dimethyl thiazolines having the structure: ##STR1## wherein R.sub.1 and R.sub.3 are the same or different, and each is selected from the group consisting of methyl and hydrogen, which impart thereto chocolate-like, fresh ground coffee-like, green, cucumber, dill aromas and yielding on dry-out floral, natural tuberose-like, orris-like nuances.
摘要翻译：香料和香料组合物和香料制品，包括皂，洗涤剂，粉末，以及含有2-烷基取代的-4,5-二甲基噻唑类的古龙香，其结构如下：其中R1和R3相同或不同，选自由甲基和氢组成的组，其赋予巧克力样，新鲜研磨的咖啡状，绿色，黄瓜，莳萝香气，并且产生干燥的花卉，天然晚香玉样，或棱镜状的细微差别。

10. 发明授权

US4000050A Photochemical preparation of polycycloalkyl oxyalkanes and oxyalkenes 失效
标题翻译：聚环烷基氧基烷烃和氧辛烯的光化学制备
公开(公告)号：US4000050A
公开(公告)日：1976-12-28
申请号：US551030
申请日：1975-02-19
申请人： Braja Dulal Mookherjee , Venkatesh Kamath , Ramanlal Ranchodji Patel , Edward J. Shuster
发明人： Braja Dulal Mookherjee , Venkatesh Kamath , Ramanlal Ranchodji Patel , Edward J. Shuster
IPC分类号： A61K8/34 , A61K8/49 , A61Q13/00 , C07C27/00 , C07C31/137 , C07C33/05 , C07C67/00 , C07D303/04 , C11B9/00 , B01J1/10
CPC分类号： C11B9/0042 , C07D303/04 , C11B9/0046 , Y10S204/904 , Y10S204/912
摘要： Processes and compositions are described for altering the aroma of consumable products including perfumes, perfume compositions and perfumed articles utilizing as the essential ingredient one or more of the polycycloalkyl oxyalkanes and/or oxyalkenes (broadly hereinafter referred to as polycycloalkyl oxyhydrocarbons) having the generic formula: ##STR1## the polycyclic moiety being bicyclic or tricyclic, wherein X is one of the moieties: ##STR2## provided that the polycyclic moiety is tricyclic only when X contains an epoxide moiety; and wherein one of the dashed lines is a carbon-carbon bond and each of the wavy lines is a carbon-carbon single bond, one of the carbon-carbon single bonds represented by the wavy line being epimeric with respect to the other of the carbon-carbon single bonds represented by the wavy line; and processes for preparing individual compounds or mixtures of these compounds including the steps of:I. Subjecting one or more santalene hydrocarbons having the generic structure: ##STR3## TO PHOTOOXIDATION WITH OXYGEN, BASE AND ULTRA VIOLET LIGHT TO FORM A MIXTURE OF COMPOUNDS HAVING THE GENERIC STRUCTURES: ##STR4## ii. Optionally fractionally distilling the resulting reaction products for utilization; orIii. Optionally reacting .alpha.-santalene, beta-santalene, epi-beta-santalene or mixtures thereof with a peracid to produce onr or more epoxide compounds having the generic structure: ##STR5## IV. Optionally fractionally distilling the resulting reaction product(s) for utilization; and/orV. Optionally reducing the resulting epoxide with lithium aluminum hydride to form one or more tertiary alcohols having the generic structure: ##STR6## vi. Optionally fractionally distilling the thus formed tertiary alcohol(s); orvii. Rearranging the epoxide compounds having the generic formula: ##STR7## using diphenyl diselenide and sodium borohydride to form one or more allylic tertiary alcohols having the generic formula: ##STR8## viii. Optionally rearranging the epoxide compounds having the structure: ##STR9## using aluminum isopropoxide to form allylic secondary alcohols having the generic structure: ##STR10## ix. Optionally fractionally distilling the allylic secondary alcohols. In addition the novel compounds having the generic structure: ##STR11## as well as the structure: ##STR12## wherein X is one of the moieties: ##STR13## are described.
摘要翻译：描述的方法和组合物用于改变消耗性产品的香味，包括香料，香料组合物和使用作为必需成分的一种或多种多环烷基氧基烷烃和/或氧烯烃（以下简称为多环烷基氧代烃）的香料，其具有以下通式：多环部分是双环或三环的，其中X是部分之一：

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