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1. 发明授权

US08362296B2 Process for preparing 4-pentenoic acid 有权
标题翻译：制备4-戊烯酸的方法
公开(公告)号：US08362296B2
公开(公告)日：2013-01-29
申请号：US12859622
申请日：2010-08-19
申请人： Joaquim Henrique Teles , Michael Schelper , Kai Gumlich , Mathieu Chabanas , Christian Müller , Anton Meier
发明人： Joaquim Henrique Teles , Michael Schelper , Kai Gumlich , Mathieu Chabanas , Christian Müller , Anton Meier
IPC分类号： C07C51/235
CPC分类号： C07C51/235 , C07C57/03
摘要： The present invention relates to a process for preparing 4-pentenoic acid, at least comprising the oxidation of a mixture (G) comprising 4-pentenal, 3-methyl-2-butanone and cyclopentene oxide, and to the use of a mixture (G) comprising 4-pentenal, 3-methyl-2-butanone and cyclopentene oxide for preparing 4-pentenoic acid. In the context of the present invention, the mixture (G) is preferably obtained as a by-product of the oxidation of cyclopentene to cyclopentanone by means of dinitrogen monoxide.
摘要翻译：本发明涉及一种制备4-戊烯酸的方法，至少包括包含4-戊烯醛，3-甲基-2-丁酮和环戊烯氧化物的混合物（G）的氧化和使用混合物（G ），其包含4-戊烯醛，3-甲基-2-丁酮和环戊烯氧化物，用于制备4-戊烯酸。在本发明的上下文中，优选通过一氧化二氮作为环戊烯氧化成环戊酮的副产物获得混合物（G）。

2. 发明申请

US20110046413A1 PROCESS FOR PREPARING 4-PENTENOIC ACID 有权
标题翻译：制备4-硝基酸的方法
公开(公告)号：US20110046413A1
公开(公告)日：2011-02-24
申请号：US12859622
申请日：2010-08-19
申请人： Joaquim Henrique Teles , Michael Schelper , Kai Gumlich , Mathieu Chabanas , Christian Müller , Anton Meier
发明人： Joaquim Henrique Teles , Michael Schelper , Kai Gumlich , Mathieu Chabanas , Christian Müller , Anton Meier
IPC分类号： C07C51/16
CPC分类号： C07C51/235 , C07C57/03
摘要： The present invention relates to a process for preparing 4-pentenoic acid, at least comprising the oxidation of a mixture (G) comprising 4-pentenal, 3-methyl-2-butanone and cyclopentene oxide, and to the use of a mixture (G) comprising 4-pentenal, 3-methyl-2-butanone and cyclopentene oxide for preparing 4-pentenoic acid. In the context of the present invention, the mixture (G) is preferably obtained as a by-product of the oxidation of cyclopentene to cyclopentanone by means of dinitrogen monoxide.
摘要翻译：本发明涉及一种制备4-戊烯酸的方法，至少包括包含4-戊烯醛，3-甲基-2-丁酮和环戊烯氧化物的混合物（G）的氧化和使用混合物（G ），其包含4-戊烯醛，3-甲基-2-丁酮和环戊烯氧化物，用于制备4-戊烯酸。在本发明的上下文中，优选通过一氧化二氮作为环戊烯氧化成环戊酮的副产物获得混合物（G）。

3. 发明申请

US20100191018A1 PROCESS FOR PREPARING PURE CYCLODODECANONE 有权
标题翻译：制备纯环己酮的方法
公开(公告)号：US20100191018A1
公开(公告)日：2010-07-29
申请号：US12694815
申请日：2010-01-27
申请人： Joaquim Henrique Teles , Beatrice Rößler-Feigel , Alexander Hauk , Anton Meier , Christian Müller , Michael Schelper , Tanja Kirchner , Susanne Szeschkus , Rolf Pinkos , Gerd-Dieter Tebben
发明人： Joaquim Henrique Teles , Beatrice Rößler-Feigel , Alexander Hauk , Anton Meier , Christian Müller , Michael Schelper , Tanja Kirchner , Susanne Szeschkus , Rolf Pinkos , Gerd-Dieter Tebben
IPC分类号： C07C45/27
CPC分类号： C07C45/82 , C07C45/28 , C07C45/62 , C07C2601/20 , C07C49/607 , C07C49/413
摘要： The present invention relates to a process for preparing at least one cyclic compound with Z cycles and 7 to 16 carbon atoms with a keto group, at least comprising the stages: (a1) oxidation of a composition (A), at least comprising one cyclic olefin with Z cycles and 7 to 16 carbon atoms and at least two C—C double bonds, by means of dinitrogen monoxide to give a composition (A1), (a2) separating off the at least one cyclic olefin with Z cycles and 7 to 16 carbon atoms with at least two C—C double bonds from the composition (A1) in order to obtain a composition (A2), and (b) distillative treatment of the composition (A2) from step (a2) in order to obtain a composition (B), comprising the at least one cyclic compound with Z cycles and 7 to 16 carbon atoms with a keto group and less than 1.0% by weight of the at least one compound with Z−1 cycles and 7 to 16 carbon atoms with at least one aldehyde group, where Z can be 1, 2, 3 or 4.
摘要翻译：本发明涉及一种制备具有Z环和至少具有7至16个碳原子的酮基的至少一种环状化合物的方法，至少包括以下步骤：（a1）组合物（A）的氧化，至少包含一个环状烯烃，Z循环和7至16个碳原子和至少两个C-C双键，借助于一氧化二氮，得到组合物（A1），（a2）以Z循环分离至少一种环状烯烃， 16个碳原子与来自组合物（A1）的至少两个C-C双键，以获得组合物（A2），和（b）从步骤（a2）中的组合物（A2）的蒸馏处理，以获得组合物（B），其包含至少一种Z循环的环状化合物和具有酮基的7至16个碳原子和小于1.0重量％的至少一种具有Z-1循环和7至16个碳原子的化合物，至少一个醛基，其中Z可以是1,2,3或4个。

4. 发明授权

US08188320B2 Process for preparing pure cyclododecanone 有权
标题翻译：制备纯环十二酮的方法
公开(公告)号：US08188320B2
公开(公告)日：2012-05-29
申请号：US12694815
申请日：2010-01-27
申请人： Joaquim Henrique Teles , Beatrice Röβler-Feigel , Alexander Hauk , Anton Meier , Christian Müller , Michael Schelper , Tanja Kirchner , Susanne Szeschkus , Rolf Pinkos , Gerd-Dieter Tebben
发明人： Joaquim Henrique Teles , Beatrice Röβler-Feigel , Alexander Hauk , Anton Meier , Christian Müller , Michael Schelper , Tanja Kirchner , Susanne Szeschkus , Rolf Pinkos , Gerd-Dieter Tebben
IPC分类号： C07C45/27
CPC分类号： C07C45/82 , C07C45/28 , C07C45/62 , C07C2601/20 , C07C49/607 , C07C49/413
摘要： The present invention relates to a process for preparing at least one cyclic compound with Z cycles and 7 to 16 carbon atoms with a keto group, at least comprising the stages: (a1) oxidation of a composition (A), at least comprising one cyclic olefin with Z cycles and 7 to 16 carbon atoms and at least two C—C double bonds, by means of dinitrogen monoxide to give a composition (A1), (a2) separating off the at least one cyclic olefin with Z cycles and 7 to 16 carbon atoms with at least two C—C double bonds from the composition (A1) in order to obtain a composition (A2), and (b) distillative treatment of the composition (A2) from step (a2) in order to obtain a composition (B), comprising the at least one cyclic compound with Z cycles and 7 to 16 carbon atoms with a keto group and less than 1.0% by weight of the at least one compound with Z−1 cycles and 7 to 16 carbon atoms with at least one aldehyde group, where Z can be 1, 2, 3 or 4.
摘要翻译：本发明涉及一种制备具有Z环和至少具有7至16个碳原子的酮基的至少一种环状化合物的方法，至少包括以下步骤：（a1）组合物（A）的氧化，至少包含一个环状烯烃，Z循环和7至16个碳原子和至少两个C-C双键，借助于一氧化二氮，得到组合物（A1），（a2）以Z循环分离至少一种环状烯烃， 16个碳原子与来自组合物（A1）的至少两个C-C双键，以获得组合物（A2），和（b）从步骤（a2）中的组合物（A2）的蒸馏处理，以获得组合物（B），其包含至少一种Z循环的环状化合物和具有酮基的7至16个碳原子和小于1.0重量％的至少一种具有Z-1循环和7至16个碳原子的化合物，至少一个醛基，其中Z可以是1,2,3或4个。

5. 发明授权

US08212082B2 Process for the isolation of dodecatrienal and its use as aroma substance 有权
标题翻译：分离十二碳三烯的方法及其作为芳香物质的用途
公开(公告)号：US08212082B2
公开(公告)日：2012-07-03
申请号：US12694851
申请日：2010-01-27
申请人： Joaquim Henrique Teles , Beatrice Röβler-Feigel , Alexander Hauk , Christian Müller , Michael Schelper , Tanja Kirchner , Susanne Szeschkus
发明人： Joaquim Henrique Teles , Beatrice Röβler-Feigel , Alexander Hauk , Christian Müller , Michael Schelper , Tanja Kirchner , Susanne Szeschkus
IPC分类号： C07C45/28 , A61K8/35 , A61K47/08 , C11D3/50
CPC分类号： C11B9/0015 , C07C45/28 , C07C45/62 , C07C45/82 , Y02P20/582 , C07C47/21 , C07C47/02
摘要： The present invention relates to a process for preparing at least one compound with Z−1 cycles and 7 to 16 carbon atoms with at least one aldehyde group, at least comprising the stages: (a1) oxidation of a composition (A), at least comprising a cyclic olefin with Z cycles and 7 to 16 carbon atoms and at least two C—C double bonds, by means of dinitrogen monoxide to give a composition (A1), (a2) separating off the at least one cyclic olefin with Z cycles and 7 to 16 carbon atoms with at least two C—C double bonds from the composition (A1) from stage (a1) in order to obtain a composition (A2), (b1) separating off the at least one cyclic compound with Z cycles and 7 to 16 carbon atoms with a keto group from the composition (A2) from step (a2), in order to obtain a composition (B1), comprising at least 50% by weight of the at least one compound with Z−1 cycles and 7 to 16 carbon atoms with at least one aldehyde group and at least two C—C double bonds, where Z may be 1, 2, 3 or 4.
摘要翻译：本发明涉及至少一种具有Z-1个循环和7-16个碳原子的化合物与至少一个醛基的制备方法，至少包括以下步骤：（a1）组合物（A）的氧化，至少包含具有Z循环和7至16个碳原子的环烯烃以及至少两个C-C双键的方法，借助于一氧化二氮，得到组合物（A1），（a2）以Z循环分离出至少一种环状烯烃和从碳（a1）组合物（A1）至少具有两个C-C双键的碳原子数为7〜16的碳原子，以获得组合物（A2），（b1）以Z循环分离出至少一种环状化合物和具有来自步骤（a2）的组合物（A2）的酮基的7至16个碳原子，以获得组合物（B1），其包含至少50重量％的至少一种Z-1循环的化合物和具有至少一个醛基和至少两个C-C双键的7至16个碳原子，其中Z可以是1,2,3或4。

6. 发明申请

US20100190869A1 PROCESS FOR THE ISOLATION OF DODECATRIENAL AND ITS USE AS AROMA SUBSTANCE 有权
标题翻译：分离多糖的方法及其作为芳香物质的使用
公开(公告)号：US20100190869A1
公开(公告)日：2010-07-29
申请号：US12694851
申请日：2010-01-27
申请人： Joaquim Henrique Teles , Beatrice Rößler-Feigel , Alexander Hauk , Christian Müller , Michael Schelper , Tanja Kirchner , Susanne Szeschkus
发明人： Joaquim Henrique Teles , Beatrice Rößler-Feigel , Alexander Hauk , Christian Müller , Michael Schelper , Tanja Kirchner , Susanne Szeschkus
IPC分类号： A61K8/35 , C07C45/28 , C11D3/50 , A61K47/08 , A61Q13/00
CPC分类号： C11B9/0015 , C07C45/28 , C07C45/62 , C07C45/82 , Y02P20/582 , C07C47/21 , C07C47/02
摘要： The present invention relates to a process for preparing at least one compound with Z−1 cycles and 7 to 16 carbon atoms with at least one aldehyde group, at least comprising the stages: (a1) oxidation of a composition (A), at least comprising a cyclic olefin with Z cycles and 7 to 16 carbon atoms and at least two C—C double bonds, by means of dinitrogen monoxide to give a composition (A1), (a2) separating off the at least one cyclic olefin with Z cycles and 7 to 16 carbon atoms with at least two C—C double bonds from the composition (A1) from stage (a1) in order to obtain a composition (A2), (b1) separating off the at least one cyclic compound with Z cycles and 7 to 16 carbon atoms with a keto group from the composition (A2) from step (a2), in order to obtain a composition (B1), comprising at least 50% by weight of the at least one compound with Z−1 cycles and 7 to 16 carbon atoms with at least one aldehyde group and at least two C—C double bonds, where Z may be 1, 2, 3 or 4.
摘要翻译：本发明涉及至少一种具有Z-1个循环和7-16个碳原子的化合物与至少一个醛基的制备方法，至少包括以下步骤：（a1）组合物（A）的氧化，至少包含具有Z循环和7至16个碳原子的环烯烃以及至少两个C-C双键的方法，通过一氧化二氮来得到组合物（A1），（a2）以Z循环分离出至少一种环状烯烃和从碳（a1）组合物（A1）至少具有两个C-C双键的碳原子数为7〜16的碳原子，以获得组合物（A2），（b1）以Z循环分离出至少一种环状化合物和具有来自步骤（a2）的组合物（A2）的酮基的7至16个碳原子，以获得组合物（B1），其包含至少50重量％的至少一种Z-1循环的化合物和具有至少一个醛基和至少两个C-C双键的7至16个碳原子，其中Z可以是1,2,3或4。

7. 发明申请

US20120157719A1 TUBE BUNDLE REACTOR FOR UNCATALYZED OR HOMOGENEOUSLY CATALYZED REACTIONS 有权
标题翻译：用于未加氢化或均相催化反应的管组反应器
公开(公告)号：US20120157719A1
公开(公告)日：2012-06-21
申请号：US13380207
申请日：2010-01-19
申请人： Joaquim Henrique Teles , Peter Resch , Wilhelm Ruppel , Ulrike Wegerle , Wolfgang Gerliing , Beatrice Rössler-Feigel , Anton Meier , Christian Müller
发明人： Joaquim Henrique Teles , Peter Resch , Wilhelm Ruppel , Ulrike Wegerle , Wolfgang Gerliing , Beatrice Rössler-Feigel , Anton Meier , Christian Müller
IPC分类号： C07C45/00 , B01J19/00
CPC分类号： B01J19/2425 , B01J4/001 , B01J19/006 , B01J2219/00085 , B01J2219/00166 , F28D7/16 , F28F9/0265 , F28F9/0275 , F28F9/0278 , Y02P20/582
摘要： The invention relates to a tube bundle reactor with a flat feed hood. Alternatively, the release hood may also have a flat design. The flat design reduces the heat of reaction which arises in the hood in the case of reaction types which take place not only in the tube bundle (uncatalyzed reactions and reactions with homogeneously distributed catalyst). This greatly suppresses undesired reactions which already take place in the hood owing to accumulated heat, which achieves a higher selectivity in the case of thermally sensitive reactions. In addition, the thermal distribution within the hoods can be controlled precisely.The tube bundle reactor comprises a tube bundle which has a feed end which is connected to a feed hood of the tube bundle reactor, wherein the feed hood is configured in a flat design with a cross-sectional area at the feed end and an internal volume, and the ratio of internal volume to cross-sectional area is less than 0.35 m. The invention is further implemented by means of a process for operating a tube bundle reactor, comprising: introducing a reactant mixture into a tube bundle and converting at least a proportion of the reactant mixture within the tube bundle to a product. The introducing comprises: feeding the reactant mixture into an interior of a feed hood of the tube bundle reactor and passing the reactant mixture on into a feed end of the tube bundle in the form of a fluid stream. The fluid stream has a cross-sectional area on entry into the feed end, and the interior of the feed hood through which the fluid stream flows has an internal volume; where the ratio of internal volume to cross-sectional area is less than 0.35 m.
摘要翻译：本发明涉及具有扁平进料罩的管束反应器。或者，释放罩也可以具有平坦的设计。在反应类型不仅在管束（未催化的反应和具有均匀分布的催化剂的反应）的情况下，扁平设计减少了发动机罩中产生的反应热。这大大地抑制了由于积热而在罩中发生的不期望的反应，这在热敏反应的情况下实现了更高的选择性。此外，可以精确地控制罩内的热分布。管束反应器包括管束，其具有连接到管束反应器的进料罩的进料端，其中进料罩构造成平坦设计，在进料端具有横截面积，内部体积，内部体积与横截面积的比值小于0.35μm。通过用于操作管束反应器的方法进一步实现本发明，其包括：将反应物混合物引入管束并将至少一部分管束内的反应物混合物转化成产物。引入包括：将反应物混合物进料到管束反应器的进料罩的内部，并将反应物混合物以流体流的形式送入管束的进料端。流体流在进入进料端时具有横截面面积，流体流流过的进料罩的内部具有内部容积; 其中内部体积与横截面积的比值小于0.35μm。

8. 发明授权

US09174192B2 Tube bundle reactor for uncatalyzed or homogeneously catalyzed reactions 有权
标题翻译：用于未催化或均匀催化反应的管束反应器
公开(公告)号：US09174192B2
公开(公告)日：2015-11-03
申请号：US13380207
申请日：2010-01-19
申请人： Joaquim Henrique Teles , Peter Resch , Wilhelm Ruppel , Ulrike Wegerle , Wolfgang Gerlinger , Beatrice Röβler-Feigel , Anton Meier , Christian Müller
发明人： Joaquim Henrique Teles , Peter Resch , Wilhelm Ruppel , Ulrike Wegerle , Wolfgang Gerlinger , Beatrice Röβler-Feigel , Anton Meier , Christian Müller
IPC分类号： B01J19/24 , B01J19/00 , B01J4/00 , F28D7/16 , F28F9/02
CPC分类号： B01J19/2425 , B01J4/001 , B01J19/006 , B01J2219/00085 , B01J2219/00166 , F28D7/16 , F28F9/0265 , F28F9/0275 , F28F9/0278 , Y02P20/582
摘要： The invention relates to a tube bundle reactor with a flat feed hood. Alternatively, the release hood may also have a flat design. The flat design reduces the heat of reaction which arises in the hood in the case of reaction types which take place not only in the tube bundle (uncatalyzed reactions and reactions with homogeneously distributed catalyst). This greatly suppresses undesired reactions which already take place in the hood owing to accumulated heat, which achieves a higher selectivity in the case of thermally sensitive reactions. In addition, the thermal distribution within the hoods can be controlled precisely.The tube bundle reactor comprises a tube bundle which has a feed end which is connected to a feed hood of the tube bundle reactor, wherein the feed hood is configured in a flat design with a cross-sectional area at the feed end and an internal volume, and the ratio of internal volume to cross-sectional area is less than 0.35 m. The invention is further implemented by means of a process for operating a tube bundle reactor, comprising: introducing a reactant mixture into a tube bundle and converting at least a proportion of the reactant mixture within the tube bundle to a product. The introducing comprises: feeding the reactant mixture into an interior of a feed hood of the tube bundle reactor and passing the reactant mixture on into a feed end of the tube bundle in the form of a fluid stream. The fluid stream has a cross-sectional area on entry into the feed end, and the interior of the feed hood through which the fluid stream flows has an internal volume; where the ratio of internal volume to cross-sectional area is less than 0.35 m.
摘要翻译：本发明涉及具有扁平进料罩的管束反应器。或者，释放罩也可以具有平坦的设计。在反应类型不仅在管束（未催化的反应和具有均匀分布的催化剂的反应）的情况下，扁平设计减少了发动机罩中产生的反应热。这大大地抑制了由于积热而在罩中发生的不期望的反应，这在热敏反应的情况下实现了更高的选择性。此外，可以精确地控制罩内的热分布。管束反应器包括管束，其具有连接到管束反应器的进料罩的进料端，其中进料罩构造成平坦设计，在进料端具有横截面积，内部体积，内部体积与横截面积的比值小于0.35μm。通过用于操作管束反应器的方法进一步实现本发明，其包括：将反应物混合物引入管束并将至少一部分管束内的反应物混合物转化成产物。引入包括：将反应物混合物进料到管束反应器的进料罩的内部，并将反应物混合物以流体流的形式送入管束的进料端。流体流在进入进料端时具有横截面面积，流体流流过的进料罩的内部具有内部容积; 其中内部体积与横截面积的比值小于0.35μm。

9. 发明授权

US07714172B2 Method for the production of cyclic ketones 失效
标题翻译：环酮生产方法
公开(公告)号：US07714172B2
公开(公告)日：2010-05-11
申请号：US12306827
申请日：2007-06-27
申请人： Joaquim Henrique Teles , Beatrice Röβler , Rolf Pinkos , Gerd Tebben , Christian Müller , Harald Rust
发明人： Joaquim Henrique Teles , Beatrice Röβler , Rolf Pinkos , Gerd Tebben , Christian Müller , Harald Rust
IPC分类号： C07C45/27
CPC分类号： C07C45/28 , C07C45/62 , C07C45/80 , C07C45/81 , C07C45/82 , C07C45/85 , C07C2601/18 , C07C2601/20 , C07C49/607 , C07C49/413
摘要： The present invention relates to a process for preparing a cyclic ketone having from 7 to 16 carbon atoms, which comprises at least the steps (a) oxidation of a composition (I) comprising at least one cyclic alkene which has from 7 to 16 carbon atoms and at least one C—C double bond by means of dinitrogen monoxide to give a composition (A), (b) treatment of the composition (A) with at least one base to give a composition (B), (c) hydrogenation of the composition (B) in the presence of at least one catalyst to give a composition (C), (d) purification of the composition (C), comprising at least the steps (di) thermal treatment of the composition (C) with at least one acid or at least one catalyst comprising at least one transition metal, (dii) further purification by a method selected from the group consisting of distillation, extraction and crystallization.
摘要翻译：本发明涉及一种制备具有7至16个碳原子的环酮的方法，其至少包括步骤（a）氧化包含至少一个具有7至16个碳原子的环烯烃的组合物（I）和至少一个C-C双键，得到组合物（A），（b）用至少一种碱处理组合物（A），得到组合物（B），（c）氢化所述组合物（B）在至少一种催化剂的存在下反应以得到组合物（C），（d）组合物（C）的纯化，所述组合物（C）至少包含步骤（ii）组合物（C）至少一种酸或至少一种包含至少一种过渡金属的催化剂，（dii）通过选自蒸馏，萃取和结晶的方法进一步纯化。

10. 发明申请

US20090281357A1 METHOD FOR THE PRODUCTION OF CYCLIC KETONES 失效
标题翻译：生产环状酮的方法
公开(公告)号：US20090281357A1
公开(公告)日：2009-11-12
申请号：US12306841
申请日：2007-06-27
申请人： Joaquim Henrique Teles , Beatrice Rössler , Rolf Pinkos , Gerd Tebben , Christian Müller
发明人： Joaquim Henrique Teles , Beatrice Rössler , Rolf Pinkos , Gerd Tebben , Christian Müller
IPC分类号： C07C45/27
CPC分类号： C07C45/28 , C07C45/62 , C07C45/85 , C07C2601/20 , C07C49/607 , C07C49/413
摘要： The present invention relates to a process for preparing a cyclic ketone having from 7 to 16 carbon atoms, which comprises at least the steps (a) oxidation of a composition (I) comprising at least one cyclic olefin which has from 7 to 16 carbon atoms and at least one C—C double bond by means of dinitrogen monoxide to give a composition (A), (b) treatment of the composition (A) with at least one base to give a composition (B).
摘要翻译：本发明涉及一种制备具有7至16个碳原子的环酮的方法，其至少包括步骤（a）包含至少一种具有7至16个碳原子的环烯烃的组合物（I）的氧化和至少一个CC双键，得到组合物（A），（b）用至少一个碱处理组合物（A）以得到组合物（B）。

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