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1. 发明授权

US4414282A Glass ceramic seals to inconel 失效
标题翻译：玻璃陶瓷密封件以铬镍铁合金
公开(公告)号：US4414282A
公开(公告)日：1983-11-08
申请号：US369965
申请日：1982-04-19
申请人： Howard L. McCollister , Scott T. Reed
发明人： Howard L. McCollister , Scott T. Reed
IPC分类号： C03C10/00 , C03C27/04 , B32B15/00
CPC分类号： C03C10/00 , C03C27/046
摘要： A glass ceramic composition prepared by subjecting a glass composition comprising, by weight, 65-80% SiO.sub.2, 8-16%, Li.sub.2 O, 2-8% , Al.sub.2 O.sub.3, 1-8% K.sub.2 O, 1-5% P.sub.2 O.sub.5 and 1.5-7% B.sub.2 O.sub.3, to the following processing steps of heating the glass composition to a temperature sufficient to crystallize lithium metasilicate therein, holding the glass composition at a temperature and for a time period sufficient to dissolve the lithium metasilicate therein thereby creating cristobalite nucleii, cooling the glass composition and maintaining the composition at a temperature and for a time period sufficient to recrystallize lithium metasilicate therein, and thermally treating the glass composition at a temperature and for a time period sufficient to cause growth of cristobalite and further crystallization of lithium metasilicate producing a glass ceramic composition having a specific thermal expansion coefficient and products containing said composition.
摘要翻译：一种玻璃陶瓷组合物，其通过将包含65-80％SiO 2，8-16％，Li 2 O，2-8％，Al 2 O 3，1-8％K 2 O，1-5％P 2 O 5和1.5-7重量％的玻璃组合物％B 2 O 3，以下加工步骤将玻璃组合物加热至足以使硅酸锂结晶的温度，将玻璃组合物保持在足以溶解偏硅酸锂的温度和时间期间，从而产生方英石核，冷却玻璃组成并将组合物保持在足以使偏硅酸锂重结晶的温度和时间内，并且在足以引起方英石生长的温度和时间段下热处理玻璃组合物，并进一步结晶生产玻璃陶瓷的偏硅酸锂具有特定热膨胀系数的组合物和含有所述组合物的产品。

2. 发明授权

US5820989A Method of processing "BPS" glass ceramic and seals made therewith 失效
标题翻译：加工“BPS”玻璃陶瓷和密封件的方法
公开(公告)号：US5820989A
公开(公告)日：1998-10-13
申请号：US706852
申请日：1996-09-03
申请人： Scott T. Reed , Ronald G. Stone , Howard L. McCollister , Paul R. Wengert, deceased
发明人： Scott T. Reed , Ronald G. Stone , Howard L. McCollister , Paul R. Wengert, deceased
IPC分类号： C03C10/00 , C03C27/04 , B32B17/06
CPC分类号： C03C27/044 , C03C10/0027 , C03C10/0054 , Y10T428/131 , Y10T428/1352 , Y10T428/139
摘要： A glass ceramic composition, a glass ceramic-to-metal seal, and more specifically a hermetic glass ceramic-to-metal seal prepared by subjecting a glass composition comprising, by weight percent, SiO.sub.2 (65-80%), LiO.sub.2 (8-16%), Al.sub.2 O.sub.3 (2-8%), K.sub.2 O (1-8%), P.sub.2 O.sub.5 (1-5%), B.sub.2 O.sub.3 (0.5-7%), and ZnO (0-5%) to the following processing steps: 1) heating the glass composition in a belt furnace to a temperature sufficient to melt the glass and crystallize lithium phosphate, 2) holding at a temperature and for a time sufficient to create cristobalite nuclei, 3) cooling at a controlled rate and to a temperature to cause crystallization of lithium silicates and growth of cristobalite, and 4) still further cooling in stages to ambient temperature. This process produces a glass ceramic whose high coefficient of thermal expansion (up to 200.times.10.sup.-7 in/in/.degree.C.) permits the fabrication of glass ceramic-to-metal seals, and particularly hermetic glass ceramic seals to nickel-based and stainless steel alloys and copper.
摘要翻译：玻璃陶瓷组合物，玻璃陶瓷 - 金属密封件，更具体地，是通过将包含以重量百分比计SiO 2（65-80％），LiO 2（8- 16％），Al 2 O 3（2-8％），K 2 O（1-8％），P 2 O 5（1-5％），B 2 O 3（0.5-7％）和ZnO（0-5％ 1）将带式炉中的玻璃组合物加热到足以熔化玻璃并使磷酸锂结晶的温度，2）在足以产生方英石核的温度和时间内保持3）以受控的速度和温度引起硅酸锂的结晶和方英石的生长，以及4）逐步进一步冷却至环境温度。该方法生产玻璃陶瓷，其高热膨胀系数（高达200×10 -7 in / in /℃）允许制造玻璃陶瓷 - 金属密封件，特别是密封的玻璃陶瓷密封件，以镍基和不锈钢钢合金和铜。

3. 发明授权

US06258305B1 Method for net-shaping using aerogels 有权
标题翻译：使用气凝胶进行净整形的方法
公开(公告)号：US06258305B1
公开(公告)日：2001-07-10
申请号：US09539199
申请日：2000-03-29
申请人： C. Jeffrey Brinker , Carol S. Ashey , Scott T. Reed , Chunangad S. Sriram , Thomas M. Harris
发明人： C. Jeffrey Brinker , Carol S. Ashey , Scott T. Reed , Chunangad S. Sriram , Thomas M. Harris
IPC分类号： B29C7100
CPC分类号： B01J13/0091
摘要： A method of net-shaping using aerogel materials is provided by first forming a sol, aging the sol to form a gel, with the gel having a fluid component and having been formed into a medium selected from the group consisting of a powder, bulk material, or granular aerobeads, derivatizing the surface of the gel to render the surface unreactive toward further condensation, removing a portion of the fluid component of the final shaped gel to form a partially dried medium, placing the medium into a cavity, wherein the volume of said medium is less that the volume of the cavity, and removing a portion of the fluid component of the medium. The removal, such as by heating at a temperature of approximately less than 50° C., applying a vacuum, or both, causes the volume of the medium to increase and to form a solid aerogel. The material can be easily removed by exposing the material to a solvent, thereby reducing the volume of the material. In another embodiment, the gel is derivatized and then formed into a shaped medium, where subsequent drying reduces the volume of the shaped medium, forming a net-shaping material. Upon further drying, the material increases in volume to fill a cavity. The present invention is both a method of net-shaping and the material produced by the method.
摘要翻译：通过首先形成溶胶，使溶胶老化以形成凝胶，使凝胶具有流体成分并形成介质，提供使用气凝胶材料的网状成形方法，所述介质选自粉末，散装材料或颗粒状aerobeads，衍生化凝胶的表面以使表面不反应进一步冷凝，去除最终成形凝胶的流体组分的一部分以形成部分干燥的介质，将介质置于空腔中，其中体积所述介质小于空腔的体积，并且去除介质的流体组分的一部分。诸如通过在大约低于50℃的温度下加热，施加真空或两者的去除使得介质的体积增加并形成固体气凝胶。通过将材料暴露于溶剂，可以容易地除去材料，从而减小材料的体积。在另一个实施方案中，将凝胶衍生化，然后形成成形介质，其中随后的干燥减小成形介质的体积，形成网状成形材料。在进一步干燥时，材料的体积增加以填充空腔。本发明既是净成形方法，也是由该方法制造的材料。

4. 发明授权

US4476156A Low temperature process for obtaining thin glass films 失效
标题翻译：用于获得薄玻璃薄膜的低温工艺
公开(公告)号：US4476156A
公开(公告)日：1984-10-09
申请号：US473845
申请日：1983-03-10
申请人： C. Jeffrey Brinker , Scott T. Reed
发明人： C. Jeffrey Brinker , Scott T. Reed
IPC分类号： C03B19/00 , C03B8/02 , C03B19/12 , C03C1/00 , C03C17/02 , C04B41/50 , C04B41/86 , C23D5/02 , B05D5/12 , C03C17/00
CPC分类号： C04B41/009 , C03C17/02 , C04B41/5022 , C04B41/86 , C23C18/1216 , C23C18/1241 , C23C18/1245 , C23C18/1254 , C23D5/02 , C23C18/1291
摘要： A method for coating a substrate with a glass-like film comprises,applying to the substrate an aqueous alcoholic solution containing a polymeric network of partially hydrolyzed metal alkoxide into which network there is incorporated finely powdered glass, whereby there is achieved on the substrate a coherent and adherent initial film; andheating said film to a temperature sufficient to melt said powdered glass component, thereby converting said initial film to a final densified film.
摘要翻译：用玻璃状膜涂覆基材的方法包括向基材施加含有部分水解的金属醇盐的聚合物网络的含水醇溶液，其中网络结合有细粉末状玻璃，由此在基材上实现相干和贴近的初始影片; 并将所述膜加热到足以熔化所述粉末状玻璃组分的温度，从而将所述初始膜转化为最终致密的膜。

5. 发明授权

US06632542B1 Solar selective absorption coatings 有权
标题翻译：太阳能选择性吸收涂层
公开(公告)号：US06632542B1
公开(公告)日：2003-10-14
申请号：US09569990
申请日：2000-05-11
申请人： Alan R. Mahoney , Scott T. Reed , Carol S. Ashley , F. Edward Martinez
发明人： Alan R. Mahoney , Scott T. Reed , Carol S. Ashley , F. Edward Martinez
IPC分类号： B32B1500
CPC分类号： C23C28/00 , C23C18/1212 , C23C18/122 , C23C18/1241 , C23C18/1254 , C25D3/562 , F24S70/25 , Y02E10/40 , Y10T428/12611 , Y10T428/25 , Y10T428/256
摘要： A new class of solar selective absorption coatings are disclosed. These coatings comprise a structured metallic overlayer such that the overlayer has a sub-micron structure designed to efficiently absorb solar radiation, while retaining low thermal emissivity for infrared thermal radiation. A sol-gel layer protects the structured metallic overlayer from mechanical, thermal, and environmental degradation. Processes for producing such solar selective absorption coatings are also disclosed.
摘要翻译：公开了一类新型的太阳能选择性吸收涂层。这些涂层包括结构化的金属覆盖层，使得覆盖层具有设计成有效吸收太阳辐射的亚微米结构，同时保持用于红外热辐射的低热辐射率。溶胶 - 凝胶层保护结构化的金属覆层免受机械，热和环境退化。还公开了用于生产这种太阳能选择性吸收涂层的方法

6. 发明授权

US06494326B1 Composite zeolite membranes 有权
标题翻译：复合沸石膜
公开(公告)号：US06494326B1
公开(公告)日：2002-12-17
申请号：US09596205
申请日：2000-06-15
申请人： Tina M. Nenoff , Steven G. Thoma , Carol S. Ashley , Scott T. Reed
发明人： Tina M. Nenoff , Steven G. Thoma , Carol S. Ashley , Scott T. Reed
IPC分类号： B01D7102
CPC分类号： B01D69/12 , B01D69/141 , B01D71/028 , B01D2323/12 , B01D2325/10 , B01J2229/64
摘要： A new class of composite zeolite membranes and synthesis techniques therefor has been invented. These membranes are essentially defect-free, and exhibit large levels of transmembrane flux and of chemical and isotopic selectivity.
摘要翻译：已经发明了一类新型复合沸石膜及其合成技术。这些膜基本上是无缺陷的，并且表现出大量的跨膜通量和化学和同位素选择性。

7. 发明授权

US06783653B2 Solar selective absorption coatings 有权
标题翻译：太阳能选择性吸收涂层
公开(公告)号：US06783653B2
公开(公告)日：2004-08-31
申请号：US10310710
申请日：2002-12-04
申请人： Alan R. Mahoney , Scott T. Reed , Carol S. Ashley , F. Edward Martinez
发明人： Alan R. Mahoney , Scott T. Reed , Carol S. Ashley , F. Edward Martinez
IPC分类号： C23C2800
CPC分类号： C23C28/00 , C23C18/1212 , C23C18/122 , C23C18/1241 , C23C18/1254 , C25D3/562 , F24S70/25 , Y02E10/40 , Y10T428/12611 , Y10T428/25 , Y10T428/256
摘要： A new class of solar selective absorption coatings are disclosed. These coatings comprise a structured metallic overlayer such that the overlayer has a sub-micron structure designed to efficiently absorb solar radiation, while retaining low thermal emissivity for infrared thermal radiation. A sol-gel layer protects the structured metallic overlayer from mechanical, thermal, and environmental degradation. Processes for producing such solar selective absorption coatings are also disclosed.
摘要翻译：公开了一类新型的太阳能选择性吸收涂层。这些涂层包括结构化的金属覆盖层，使得覆盖层具有设计成有效吸收太阳辐射的亚微米结构，同时保持用于红外热辐射的低热辐射率。溶胶 - 凝胶层保护结构化的金属覆层免受机械，热和环境退化。还公开了用于生产这种太阳能选择性吸收涂层的方法。

8. 发明授权

US4929278A Sol-gel antireflective coating on plastics 失效
标题翻译：塑料上的溶胶 - 凝胶抗反射涂层
公开(公告)号：US4929278A
公开(公告)日：1990-05-29
申请号：US148458
申请日：1988-01-26
申请人： Carol S. Ashley , Scott T. Reed
发明人： Carol S. Ashley , Scott T. Reed
IPC分类号： G02B1/11 , H01L31/0216
CPC分类号： H01L31/02167 , F24J2/505 , G02B1/111 , Y02E10/40 , Y02E10/50
摘要： An antireflection film made from a reliquified sol-gel hydrolyzation, condensation polymeric reaction product of a silicon, alkoxides and/or metal alkoxides, or mixtures thereof. The film is particularly useful for coating plastics.
摘要翻译：由经修饰的溶胶 - 凝胶水解产生的抗反射膜，硅，醇盐和/或金属醇盐的缩合聚合反应产物，或其混合物。该胶片特别适用于涂料塑料。

9. 发明授权

US08226839B1 Method of patterning an aerogel 有权
标题翻译：图案化气凝胶的方法
公开(公告)号：US08226839B1
公开(公告)日：2012-07-24
申请号：US12480158
申请日：2009-06-08
申请人： Scott T. Reed
发明人： Scott T. Reed
IPC分类号： C03C15/00
CPC分类号： C03C17/30 , C03C17/006 , C03C2217/425 , C03C2218/118 , C03C2218/33 , G03F7/0043 , G03F7/2014
摘要： A method for producing a pattern in an aerogel disposed as a coating on a substrate comprises exposing the aerogel coating to the vapors of a hydrophobic silane compound, masking the aerogel coating with a shadow photomask and irradiating the aerogel coating with ultraviolet (UV) irradiation. The exposure to UV through the shadow mask creates a pattern of hydrophobic and hydrophilic regions in the aerogel coating. Etching away the hydrophilic regions of the aerogel coating, preferably with a 1 molar solution of sodium hydroxide, leaves the unwetted and unetched hydrophobic regions of the aerogel layer on the substrate, replicating the pattern of the photomask. The hydrophobic aerogel pattern can be further exposed to UV irradiation if desired, to create a hydrophilic aerogel pattern.
摘要翻译：用于在气相凝胶中制备作为涂层涂布在基质上的图案的方法包括将气凝胶涂层暴露于疏水硅烷化合物的蒸气，用阴影光掩模掩蔽气凝胶涂层并用紫外线（UV）照射照射气凝胶涂层。通过荫罩暴露于UV会在气凝胶涂层中产生疏水和亲水区域的图案。蚀刻气溶胶涂层的亲水区域，优选用1摩尔浓度的氢氧化钠溶液离开基底上的气凝胶层的未经蚀刻和未蚀刻的疏水区域，复制光掩模图案。如果需要，疏水性气凝胶图案可以进一步暴露于UV照射，以产生亲水性气凝胶图案。

10. 发明授权

US4966812A Sol-gel antireflective coating on plastics 失效
公开(公告)号：US4966812A
公开(公告)日：1990-10-30
申请号：US359458
申请日：1989-06-01
申请人： Carol S. Ashley , Scott T. Reed
发明人： Carol S. Ashley , Scott T. Reed
IPC分类号： G02B1/11 , H01L31/0216
CPC分类号： G02B1/111 , H01L31/02167 , Y02E10/50 , Y10T428/31507 , Y10T428/31663
摘要： An antireflection film made from a reliquified sol-gel hydrolyzation, condensation polymeric reaction product of a silicon, alkoxides and/or metal alkoxides, or mixtures thereof. The film is particularly useful for coating plastics.

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