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1. 发明授权

US4009015A Method of making glass-ceramics from modified basalts 失效
标题翻译：从改性玄武岩制备玻璃陶瓷的方法
公开(公告)号：US4009015A
公开(公告)日：1977-02-22
申请号：US600020
申请日：1975-07-29
申请人： Howard L. McCollister
发明人： Howard L. McCollister
IPC分类号： C03C10/00 , C03B32/00
CPC分类号： C03C10/0045
摘要： Disclosed is a method of producing hard glass-ceramics from a melt of basalt enriched with one or more of CaO, MgO and SiO.sub.2 to achieve defined ratios of certain oxides in the batch, cooling the melt to a glass and thermally in situ crystallizing the glass to a highly crystalline glass-ceramic product containing a diopside solid solution as the principal phase.
摘要翻译：公开了一种从富含CaO，MgO和SiO 2中的一种或多种的玄武岩熔体制备硬质玻璃陶瓷的方法，以实现间歇中某些氧化物的确定比例，将熔体冷却成玻璃并热原位结晶玻璃涉及含有透辉石固溶体作为主相的高度结晶的玻璃陶瓷产品。

2. 发明授权

US4414282A Glass ceramic seals to inconel 失效
标题翻译：玻璃陶瓷密封件以铬镍铁合金
公开(公告)号：US4414282A
公开(公告)日：1983-11-08
申请号：US369965
申请日：1982-04-19
申请人： Howard L. McCollister , Scott T. Reed
发明人： Howard L. McCollister , Scott T. Reed
IPC分类号： C03C10/00 , C03C27/04 , B32B15/00
CPC分类号： C03C10/00 , C03C27/046
摘要： A glass ceramic composition prepared by subjecting a glass composition comprising, by weight, 65-80% SiO.sub.2, 8-16%, Li.sub.2 O, 2-8% , Al.sub.2 O.sub.3, 1-8% K.sub.2 O, 1-5% P.sub.2 O.sub.5 and 1.5-7% B.sub.2 O.sub.3, to the following processing steps of heating the glass composition to a temperature sufficient to crystallize lithium metasilicate therein, holding the glass composition at a temperature and for a time period sufficient to dissolve the lithium metasilicate therein thereby creating cristobalite nucleii, cooling the glass composition and maintaining the composition at a temperature and for a time period sufficient to recrystallize lithium metasilicate therein, and thermally treating the glass composition at a temperature and for a time period sufficient to cause growth of cristobalite and further crystallization of lithium metasilicate producing a glass ceramic composition having a specific thermal expansion coefficient and products containing said composition.
摘要翻译：一种玻璃陶瓷组合物，其通过将包含65-80％SiO 2，8-16％，Li 2 O，2-8％，Al 2 O 3，1-8％K 2 O，1-5％P 2 O 5和1.5-7重量％的玻璃组合物％B 2 O 3，以下加工步骤将玻璃组合物加热至足以使硅酸锂结晶的温度，将玻璃组合物保持在足以溶解偏硅酸锂的温度和时间期间，从而产生方英石核，冷却玻璃组成并将组合物保持在足以使偏硅酸锂重结晶的温度和时间内，并且在足以引起方英石生长的温度和时间段下热处理玻璃组合物，并进一步结晶生产玻璃陶瓷的偏硅酸锂具有特定热膨胀系数的组合物和含有所述组合物的产品。

3. 发明授权

US5820989A Method of processing "BPS" glass ceramic and seals made therewith 失效
标题翻译：加工“BPS”玻璃陶瓷和密封件的方法
公开(公告)号：US5820989A
公开(公告)日：1998-10-13
申请号：US706852
申请日：1996-09-03
申请人： Scott T. Reed , Ronald G. Stone , Howard L. McCollister , Paul R. Wengert, deceased
发明人： Scott T. Reed , Ronald G. Stone , Howard L. McCollister , Paul R. Wengert, deceased
IPC分类号： C03C10/00 , C03C27/04 , B32B17/06
CPC分类号： C03C27/044 , C03C10/0027 , C03C10/0054 , Y10T428/131 , Y10T428/1352 , Y10T428/139
摘要： A glass ceramic composition, a glass ceramic-to-metal seal, and more specifically a hermetic glass ceramic-to-metal seal prepared by subjecting a glass composition comprising, by weight percent, SiO.sub.2 (65-80%), LiO.sub.2 (8-16%), Al.sub.2 O.sub.3 (2-8%), K.sub.2 O (1-8%), P.sub.2 O.sub.5 (1-5%), B.sub.2 O.sub.3 (0.5-7%), and ZnO (0-5%) to the following processing steps: 1) heating the glass composition in a belt furnace to a temperature sufficient to melt the glass and crystallize lithium phosphate, 2) holding at a temperature and for a time sufficient to create cristobalite nuclei, 3) cooling at a controlled rate and to a temperature to cause crystallization of lithium silicates and growth of cristobalite, and 4) still further cooling in stages to ambient temperature. This process produces a glass ceramic whose high coefficient of thermal expansion (up to 200.times.10.sup.-7 in/in/.degree.C.) permits the fabrication of glass ceramic-to-metal seals, and particularly hermetic glass ceramic seals to nickel-based and stainless steel alloys and copper.
摘要翻译：玻璃陶瓷组合物，玻璃陶瓷 - 金属密封件，更具体地，是通过将包含以重量百分比计SiO 2（65-80％），LiO 2（8- 16％），Al 2 O 3（2-8％），K 2 O（1-8％），P 2 O 5（1-5％），B 2 O 3（0.5-7％）和ZnO（0-5％ 1）将带式炉中的玻璃组合物加热到足以熔化玻璃并使磷酸锂结晶的温度，2）在足以产生方英石核的温度和时间内保持3）以受控的速度和温度引起硅酸锂的结晶和方英石的生长，以及4）逐步进一步冷却至环境温度。该方法生产玻璃陶瓷，其高热膨胀系数（高达200×10 -7 in / in /℃）允许制造玻璃陶瓷 - 金属密封件，特别是密封的玻璃陶瓷密封件，以镍基和不锈钢钢合金和铜。

4. 发明授权

US5648302A Sealing glasses for titanium and titanium alloys 失效
标题翻译：钛和钛合金密封眼镜
公开(公告)号：US5648302A
公开(公告)日：1997-07-15
申请号：US713294
申请日：1996-09-13
申请人： Richard K. Brow , Howard L. McCollister , Carol C. Phifer , Delbert E. Day
发明人： Richard K. Brow , Howard L. McCollister , Carol C. Phifer , Delbert E. Day
IPC分类号： C03C3/068 , C03C3/15 , C03C8/24
CPC分类号： C03C3/068 , A61N1/3754 , C03C3/15 , C03C8/24
摘要： Barium lanthanoborate sealing-glass compositions are provided comprising various combinations (in terms of mole-%) of boron oxide (B.sub.2 O.sub.3), barium oxide (BaO), lanthanum oxide (La.sub.2 O.sub.3), and at least one other oxide selected from the group consisting of aluminum oxide (Al.sub.2 O.sub.3), calcium oxide (CaO), lithium oxide (Li.sub.2 O), sodium oxide (Na.sub.2 O), silicon dioxide (SiO.sub.2), or titanium dioxide (TiO.sub.2). These sealing-glass compositions are useful for forming hermetic glass-to-metal seals with titanium and titanium alloys having an improved aqueous durability and favorable sealing characteristics. Examples of the sealing-glass compositions are provided having coefficients of thermal expansion about that of titanium or titanium alloys, and with sealing temperatures less than about 900.degree. C., and generally about 700.degree.-800.degree. C. The barium lanthanoborate sealing-glass compositions are useful for components and devices requiring prolonged exposure to moisture or water, and for implanted biomedical devices (e.g. batteries, pacemakers, defibrillators, pumps).
摘要翻译：提供了硼酸钡硼酸盐密封玻璃组合物，其包括氧化硼（B 2 O 3），氧化钡（BaO），氧化镧（La 2 O 3）和选自以下的至少一种其它氧化物的各种组合（以摩尔％计）：氧化铝（Al 2 O 3），氧化钙（CaO），氧化锂（Li 2 O），氧化钠（Na 2 O），二氧化硅（SiO 2）或二氧化钛（TiO 2）。这些密封玻璃组合物可用于形成具有改善的水性耐久性和良好密封特性的钛和钛合金的密封玻璃 - 金属密封。提供了密封玻璃组合物的实例，其热膨胀系数约为钛或钛合金的热膨胀系数，密封温度低于约900℃，通常约为700-800℃。钡硼酸钡密封玻璃组合物可用于需要长时间暴露于水分或水分的部件和装置，以及植入的生物医学装置（如电池，起搏器，除颤器，泵）。

5. 发明授权

US4011091A Ceramic materials containing keatite 失效
标题翻译：含陶瓷的陶瓷材料
公开(公告)号：US4011091A
公开(公告)日：1977-03-08
申请号：US604509
申请日：1975-08-13
申请人： Howard L. McCollister
发明人： Howard L. McCollister
IPC分类号： C03C10/00 , C03C15/00 , C03C3/22
CPC分类号： C03C15/00 , C03C10/0027
摘要： Disclosed are low expansion, chemically resistant, ceramic articles containing keatite as the principal crystalline phase. The articles are prepared from compositions in the Li.sub.2 O.Al.sub.2 O.sub.3.SiO.sub.2 field. In preparing this ceramic article, a glass having the desired composition is formed into the appropriate shape by molding the molten glass, compaction and sintering of glass particles or by other conventional glass and ceramic forming processes. The article thus formed is then crystallized to keatite solid solution by an appropriate heat treatment followed by acid leaching in a strong but diluted aqueous acid to produce a ceramic material having the hydroxy aluminosilicate crystalline structure. The hydroxy aluminosilicate ceramic article is then thermally dehydrated to produce a ceramic article containing keatite as a crystalline phase together with mullite with or without the presence of other phases such as amorphous or glassy SiO.sub.2, quartz and nucleants.

6. 发明授权

US5693580A Titanium sealing glasses and seals formed therefrom 失效
标题翻译：由此形成的钛密封玻璃和密封件
公开(公告)号：US5693580A
公开(公告)日：1997-12-02
申请号：US713385
申请日：1996-09-13
申请人： Richard K. Brow , Howard L. McCollister , Carol C. Phifer , Delbert E. Day
发明人： Richard K. Brow , Howard L. McCollister , Carol C. Phifer , Delbert E. Day
IPC分类号： C03C3/15 , C03C3/155 , C03C8/24 , C03C27/04 , C03C8/00
CPC分类号： C03C27/044 , A61N1/3754 , C03C3/15 , C03C3/155 , C03C8/24
摘要： Alkaline-earth lanthanoborate sealing-glass compositions containing CaO, La.sub.2 O.sub.3, B.sub.2 O.sub.3, TiO.sub.2 and Al.sub.2 O.sub.3 in various combinations of mole-% are provided. These sealing-glass compositions are useful for forming hermetic glass-to-metal seals with titanium and titanium alloys that have a high aqueous durability for component or device applications requiring exposure to moisture, water or body fluids. Particular applications of the titanium sealing-glass compositions include forming glass-to-metal seals for lithium batteries and implanted biomedical devices (e.g. batteries, pacemakers, defibrillators, pumps).
摘要翻译：提供含有各种组合摩尔％的CaO，La2O3，B2O3，TiO2和Al2O3的碱土金属硼酸盐密封玻璃组合物。这些密封玻璃组合物可用于形成具有用于需要暴露于水分，水或体液的组件或装置应用的具有高耐水性的钛和钛合金的密封玻璃 - 金属密封。钛密封玻璃组合物的特殊应用包括形成用于锂电池和植入的生物医学装置（例如电池，起搏器，去纤颤器，泵）的玻璃 - 金属密封件。

7. 发明授权

US4273826A Process of making glass articles having antireflective coatings and product 失效
标题翻译：制造具有抗反射涂层和产品的玻璃制品的方法
公开(公告)号：US4273826A
公开(公告)日：1981-06-16
申请号：US99452
申请日：1979-12-03
申请人： Howard L. McCollister , Norman L. Boling
发明人： Howard L. McCollister , Norman L. Boling
IPC分类号： C03C15/00 , C03C17/02 , C03C23/00 , G09F7/18 , B32B3/26 , B32B5/18
CPC分类号： G02B1/113 , C03C15/00 , C03C17/02 , C03C23/00 , G09F7/18 , G02B2207/107 , Y10T428/24926 , Y10T428/249961 , Y10T428/249969 , Y10T428/249988 , Y10T428/263 , Y10T428/264 , Y10T428/265
摘要： Disclosed is a process of making a glass article containing a thin surface film antireflective coating made by providing a dispersion containing at least one metalloorganic compound in solution, depositing a thin coating of such dispersion on the glass substrate, heating the film to drive off the solvent and to decompose the organic components, thus forming a glass film from the remaining inorganic oxide components, further heating the glass film layer to cause phase separation thereof, and thereafter etching and leaching such film to dissolve out preferentially one of the phases of the phase-separated glass, leaving a skeletonized surface film having a graded refractive index; and products resulting from such process.
摘要翻译：公开了一种制备含有薄表面膜抗反射涂层的玻璃制品的方法，该涂层通过在溶液中提供含有至少一种金属有机化合物的分散体，在玻璃基板上沉积这种分散体的薄涂层，加热该膜以驱除溶剂为了分解有机成分，从残留的无机氧化物成分中形成玻璃膜，进一步加热玻璃膜层，使其相分离，然后优选将该相进行蚀刻浸出，分离玻璃，留下具有渐变折射率的骨架化表面膜; 和由此过程产生的产品。

8. 发明授权

US4041215A Method for forming solid electrolyte composite 失效
标题翻译：形成固体电解质复合材料的方法
公开(公告)号：US4041215A
公开(公告)日：1977-08-09
申请号：US673784
申请日：1976-04-05
申请人： Kenneth R. Kormanyos , Howard L. McCollister , Paul L. White
发明人： Kenneth R. Kormanyos , Howard L. McCollister , Paul L. White
IPC分类号： H01M10/39 , H01M2/16
CPC分类号： H01M10/3927
摘要： A solid electrolyte composite is provided which is suitable for use as the separating member between a sodium reservoir source and a sulfur reservoir source in a sodium-sulfur battery; the solid electrolyte composite is manufactured by providing a membrane of a crystalline ionic conductive sodium polyaluminate on a portion of a porous, anhydrous crystalline supporting body consisting of alpha-Al.sub.2 O.sub.3. The sodium polyaluminate is initially applied in the form of a precursor which is then subsequently heated to form the ionic conductive crystalline sodium polyaluminate membrane.
摘要翻译：提供了一种固体电解质复合材料，适合用作钠 - 硫电池中的钠储存源和硫储存源之间的分离构件; 通过在由α-Al 2 O 3组成的多孔无水结晶支撑体的一部分上提供结晶离子导电聚铝酸钠的膜来制造固体电解质复合材料。聚铝酸钠首先以前体的形式施用，然后随后将其加热以形成离子导电结晶聚铝酸钠膜。

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