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1. 发明授权

US4421932A Manufacture of quaternary ammonium compounds 失效
标题翻译：季铵化合物的制造
公开(公告)号：US4421932A
公开(公告)日：1983-12-20
申请号：US369810
申请日：1982-04-19
申请人： Horst Rutzen , Manfred Petzold
发明人： Horst Rutzen , Manfred Petzold
IPC分类号： C09K3/16 , A01N33/12 , C07B31/00 , C07B43/04 , C07C67/00 , C07C213/00 , C07C213/04 , C07C215/40 , C11D1/62 , D06M13/02 , D06M13/322 , D06M13/385 , D06M13/46 , D06M13/463 , C07C89/00
CPC分类号： C11D1/62 , A01N33/12 , D06M13/385 , D06M13/463 , D06M2200/00 , D06M2200/50
摘要： Process for the manufacture of quaternary ammonium compounds by reacting a compound having a terminal epoxy group with a tertiary amine which is partly present as the free amine and partly present in the form of a salt, followed by the addition of sufficient acid at the end of the reaction to complete salt formation of the quaternary ammonium compound.
摘要翻译：通过使具有末端环氧基的化合物与作为游离胺部分存在并部分以盐形式存在的叔胺反应制备季铵化合物的方法，然后在末端加入足够的酸完成季铵化合物盐形成的反应。

2. 发明授权

US4090845A Process for the dyeing of polyacrylonitrile fibrous material 失效
标题翻译：聚丙烯腈纤维材料染色工艺
公开(公告)号：US4090845A
公开(公告)日：1978-05-23
申请号：US750727
申请日：1976-12-15
申请人： Manfred Petzold , Heinz Grunert , Wolfgang Rupilius , Horst Rutzen
发明人： Manfred Petzold , Heinz Grunert , Wolfgang Rupilius , Horst Rutzen
IPC分类号： D06P1/66 , D06P3/76 , D06P5/04 , C07C85/00
CPC分类号： D06P3/76 , D06P1/66 , Y10S8/927 , Y10S8/929
摘要： Water-soluble quaternary ammonium compounds of the formula: ##STR1## wherein R.sub.1 and R.sub.2 are each alkyl groups of C.sub.1-15 chain length wherein the sum of the carbon atoms in said groups is 9 to 18; R.sub.3 represents a C.sub.1-5 alkyl or hydroxyalkyl group; R.sub.4 represents a C.sub.1-5 alkyl, hydroxyalkyl or benzyl group; R.sub.5 represents a benzyl group; and X represents a salt-forming anion, are effective retardant-levelling agents in the dyeing of anionic polyacrylonitrile fibers with basic (i.e. cationic) dyes.
摘要翻译：下式的水溶性季铵化合物：其中R1和R2各自是C1-15链长的烷基，其中所述基团中的碳原子之和为9至18; R3表示C1-5烷基或羟烷基; R4表示C1-5烷基，羟基烷基或苄基; R5表示苄基; 和X代表成盐阴离子，是用碱性（即阳离子）染料染色阴离子聚丙烯腈纤维的有效阻燃剂。

3. 发明授权

US4937011A Detergent compositions containing active chlorine and ketone foam inhibitors 失效
标题翻译：含有活性氯和酮泡沫抑制剂的洗涤剂组合物
公开(公告)号：US4937011A
公开(公告)日：1990-06-26
申请号：US295880
申请日：1989-01-11
申请人： Karl-Heinz Schmid , Adolf Asbeck , Christoph Breucker , Bernhard Gutsche , Alfred Meffert , Horst Rutzen
发明人： Karl-Heinz Schmid , Adolf Asbeck , Christoph Breucker , Bernhard Gutsche , Alfred Meffert , Horst Rutzen
IPC分类号： B01D19/04 , C11D3/20 , C11D3/395
CPC分类号： C11D3/0026 , C11D3/2072 , C11D3/395
摘要： Alkaline dishwashing machine detergent compositions containing an active chlorine composition and a foam inhibiting amount of a ketone containing at least 25 carbon atoms. A process for their preparation wherein the ketone is introduced into the composition as a dispersion in a liquid.
摘要翻译：含有活性氯组合物和泡沫抑制量的含有至少25个碳原子的酮的碱性餐具洗涤机洗涤剂组合物。其制备方法，其中酮作为液体中的分散体引入组合物中。

4. 发明授权

US4678605A Cationic surfactants based on quaternary ammonium compounds and methods of using same 失效
标题翻译：基于季铵化合物的阳离子表面活性剂及其使用方法
公开(公告)号：US4678605A
公开(公告)日：1987-07-07
申请号：US820281
申请日：1986-01-17
申请人： Juergen Geke , Horst Rutzen
发明人： Juergen Geke , Horst Rutzen
IPC分类号： B01F17/38 , B01F17/18 , C11D1/62
CPC分类号： C11D1/62
摘要： The invention relates to new cationic surfactants based on quaternary ammonium compounds corresponding to the general formulaR.sup.1 -CHOH-CHR.sup.2 -N.sup.+ R.sup.3 R.sup.4 R.sup.5 R.sup.6 CO.sub.2.sup.- (1)whereinR.sup.1 is a linear or branched alkyl residue having from 1 to 22 carbon atoms;R.sup.2 is hydrogen or a linear or branched alkyl residue having from 1 to 21 carbon atoms, the total number of carbon atoms of the substituents R.sup.1 and R.sup.2 being in the range of from 8 to 22;R.sup.3 and R.sup.4 each represent methyl, ethyl, 2-hydroxyethyl or 2-hydroxypropyl;R.sup.5 represents an alkyl residue having from 4 to 6 carbon atoms or a phenalkyl residue having from 1 to 3 carbon atoms in the alkyl residue; andR.sup.6 represents a linear or branched alkyl residue having from 4 to 15 carbon atoms.The cationic surfactants have particular utility in cleaning agents.
摘要翻译：本发明涉及基于对应于通式R1-CHOH-CHR2-N + R3R4R5R6CO2-（1）的季铵化合物的新型阳离子表面活性剂，其中R1是具有1至22个碳原子的直链或支链烷基; R2是氢或具有1至21个碳原子的直链或支链烷基，取代基R 1和R 2的碳原子总数在8至22的范围内; R3和R4各自表示甲基，乙基，2-羟乙基或2-羟丙基; R5代表具有4至6个碳原子的烷基残基或在烷基残基中具有1至3个碳原子的苯烷基残基; 并且R 6表示具有4至15个碳原子的直链或支链烷基。阳离子表面活性剂在清洁剂中具有特别的用途。

5. 发明授权

US4480126A Process for the preparation of quaternary ammonium compounds 失效
标题翻译：制备季铵化合物的方法
公开(公告)号：US4480126A
公开(公告)日：1984-10-30
申请号：US369759
申请日：1982-04-19
申请人： Horst Rutzen
发明人： Horst Rutzen
IPC分类号： C11D3/30 , C07C67/00 , C07C209/00 , C07C209/12 , C07C211/63 , C07C211/64 , C09K3/16 , C11D1/62 , D06M13/02 , D06M13/322 , D06M13/385 , D06M13/46 , D06M13/463 , D06M16/00 , C07C91/40
CPC分类号： C11D1/62 , D06M13/385 , D06M13/463 , D06M16/00 , D06M2200/00 , D06M2200/50
摘要： Process for the preparation of quaternary ammonium compounds by reacting a tertiary amine with a vicinal halohydrin having at least 6 carbon atoms, and quaternary ammonium compounds prepared thereby.
摘要翻译：通过使叔胺与具有至少6个碳原子的连位卤代醇反应来制备季铵化合物的方法，以及由此制备的季铵化合物。

6. 发明授权

US4167421A Process for dispersing pigments and fillers using aminoalkanols and salt, alkoxylation and quaternization derivatives thereof 失效
标题翻译：使用氨基链烷醇和盐分散颜料和填料的方法，烷氧基化和季铵化衍生物
公开(公告)号：US4167421A
公开(公告)日：1979-09-11
申请号：US930228
申请日：1978-08-02
申请人： Heinrich Linden , Horst Rutzen , Bernd Wegemund
发明人： Heinrich Linden , Horst Rutzen , Bernd Wegemund
IPC分类号： C09C1/00 , C09B67/08 , C09B67/18 , C09B67/20 , C09C1/22 , C09C1/24 , C09C1/36 , C09C3/00 , C09C3/08 , C09D7/12
CPC分类号： C09B67/0011 , C09B67/0004 , C09B67/002 , C09C1/24 , C09C1/3692 , C09C3/006 , C01P2004/84
摘要： A process for improving the dispersibility of inorganic and organic pigments and fillers which comprises contacting said pigments and fillers with (a) aminoalkanols of the formulae ##STR1## wherein R.sub.1 is alkyl having 6 to 22 carbon atoms, R.sub.2 is hydrogen or methyl, provided there is only one methyl group per (CH).sub.x group, R.sub.3 and R.sub.4 are the same or different and are hydrogen, alkyl having 1 to 4 carbon atoms or hydroxyalkyl having 2 to 4 carbon atoms, x is an integer of from 2 to 6 and y is an integer of from 0 to 3, with the proviso that, if y is 0, R.sub.3 and R.sub.4 are not both hydrogen, or (b) salts, (c) alkoxylation products, and (d) quaternization products of said aminoalkanols, and recovering highly dispersible pigments and fillers.
摘要翻译：一种改善无机和有机颜料和填料的分散性的方法，其包括使所述颜料和填料与式（Ⅰ）或（II）的氨基链烷醇接触，其中R1是具有6-22个碳原子，R2为氢或甲基，条件是每个（CH）x基团仅有一个甲基，R 3和R 4相同或不同，为氢，具有1至4个碳原子的烷基或具有2至4个碳原子的羟基烷基，x为2〜6的整数，y为0〜3的整数，条件是如果y为0，则R3和R4不同时为氢，或（b）为盐，（c）烷氧基化产物，和（d）所述氨基链烷醇的季铵化产物，和回收高度分散的颜料和填料。

7. 发明授权

US4090969A Method of oil recovery by flooding employing betaine solutions 失效
标题翻译：采用甜菜碱溶液淹油回收方法
公开(公告)号：US4090969A
公开(公告)日：1978-05-23
申请号：US758039
申请日：1977-01-10
申请人： Karlheinz Koch , Horst Rutzen
发明人： Karlheinz Koch , Horst Rutzen
IPC分类号： C09K3/00 , C09K8/584 , E21B43/22
CPC分类号： C09K8/584 , Y10S507/936
摘要： A method of extracting mineral oil from subterranean formation by flooding comprising the steps of forcing an aqueous liquid into a subterranean formation containing mineral oil and displacing the mineral oil through at least one bore hole in the subterranean formation, said aqueous liquid containing from 0.01% to 15% by weight of an amphoteric surface-active compound selected from the group consisting of (1) a betaine having the formula ##STR1## wherein R.sub.1 and R.sub.2 are members selected from the group consisting of hydrogen and alkyl having from 1 to 18 carbon atoms, with the proviso that the sum of the carbon atoms in R.sub.1 + R.sub.2 is from 9 to 18, R.sub.3 and R.sub.4 are members selected from the group consisting of lower alkyl and lower alkylol, x is an integer from 2 to 4, y is an integer from 0 to 1 and z is an integer from 1 to 4, and (2) mixtures of said betaine with up to 20% by weight of an acid having the formula ##STR2## wherein R.sub.1, R.sub.2, R.sub.3, R.sub.4, x and z have the above-assigned values.
摘要翻译：一种通过淹水从地层中提取矿物油的方法，包括以下步骤：将含水液体强制进入含有矿物油的地层，并使矿物油通过地层中的至少一个钻孔排出，所述含水液体含有0.01％至 15重量％的选自以下的两性表面活性化合物：（1）具有式“IMAGE”的甜菜碱，其中R 1和R 2是选自氢和具有1至18个碳原子的烷基的成员，条件是R1 + R2中的碳原子总数为9至18，R3和R4为选自低级烷基和低级羟烷基的成员，x为2至4的整数，y为 0至1的整数，z为1至4的整数，和（2）所述甜菜碱与至多20重量％的具有下式的酸的混合物：其中R1，R2，R3，R4，x和 z具有上述赋值。

8. 发明授权

US4281196A Quaternary ammonium compounds, their preparation, and their use as softening agents 失效
标题翻译：季铵化合物，它们的制备及其用作软化剂
公开(公告)号：US4281196A
公开(公告)日：1981-07-28
申请号：US83850
申请日：1979-10-11
申请人： Horst Rutzen , Jochen Heidrich , Martin Bischoff , Udo Kloubert , Peter Waltenberger , Ingo Wegener
发明人： Horst Rutzen , Jochen Heidrich , Martin Bischoff , Udo Kloubert , Peter Waltenberger , Ingo Wegener
IPC分类号： C11D1/62 , C11D3/00 , D06M13/372 , D06M13/463 , C07C91/26
CPC分类号： D06M13/372 , C11D1/62 , C11D3/001 , D06M13/463 , D06M2200/00 , D06M2200/20 , D06M2200/25 , D06M2200/50
摘要： This invention is directed to quaternary compounds of the formula ##STR1## wherein R.sup.1 represents an aliphatic hydrocarbon radical of from about 1 to 21 carbon atoms; R.sup.2 represents hydrogen or has the same meaning as R.sup.1, the total number of carbon atoms in R.sup.1 and R.sup.2 being from 6 to 22, and, when R.sup.2 is hydrogen, R.sup.1 has from 6 to 21 carbon atoms; R.sup.3 represents an alkyl or hydroxyalkyl group having from 1 to 4 carbon atoms or a radical of formula ##STR2## wherein R and R are devined above, X and Y are each either hydrogen or a methyl group, with the proviso that X and Y cannot both be a methyl group, and p is an integer of from 1 to 20; R.sup.4 represents an alkyl radical of from 1 to 4 carbon atoms; m and n are integers of from about 1 to 20; and A.crclbar. is an anion. The quaternary compounds are useful as fabric softeners.
摘要翻译：本发明涉及式（I）的季铵化合物，其中R 1表示约1至21个碳原子的脂族烃基; R2表示氢或具有与R1相同的含义，R 1和R 2中的碳原子总数为6至22，并且当R 2为氢时，R 1具有6至21个碳原子; R3表示具有1至4个碳原子的烷基或羟烷基或式（Ia）的基团，其中R和R分别位于上，X和Y各自为氢或甲基，条件是X Y不能同时为甲基，p为1〜20的整数。 R4表示1〜4个碳原子的烷基; m和n为约1至20的整数; 而A（ - ）是阴离子。四元化合物可用作织物柔软剂。

9. 发明授权

US4171278A Surface-active compound combination containing hydroxyalkylamines 失效
标题翻译：含羟基烷基胺的表面活性化合物组合
公开(公告)号：US4171278A
公开(公告)日：1979-10-16
申请号：US941902
申请日：1978-11-02
申请人： Hans Andree , Gunter Jakobi , Wolfgang Rupilius , Horst Rutzen , Ulrich Zeidler , Markus Berg , Jochen Kaufmann , Gunther Vogt
发明人： Hans Andree , Gunter Jakobi , Wolfgang Rupilius , Horst Rutzen , Ulrich Zeidler , Markus Berg , Jochen Kaufmann , Gunther Vogt
IPC分类号： C11D1/38 , C11D1/40 , C11D1/44 , C11D1/52 , C11D3/30 , C11D3/32
CPC分类号： C11D1/528 , C11D1/44 , C11D3/30 , C11D3/32
摘要： A surface-active compound combination for use in textile washing agent compositions consisting essentially of(1) at least one tenside of the anionic sulfonate or sulfate type or non-ionic ethoxylated type, and(2) at least one hydroxyalkylamine having vicinal oxygen and nitrogen bridging atoms, ethoxylated/propoxylated derivatives thereof, acylated derivatives thereof, or ethoxylated/propoxylated acylated derivatives thereof, where the amount of component (1) to component (2) is in the weight ratio of 100:1 to 1:1. The surface-active compound composition is useful in preparation of low temperature detergents and low phosphate detergents.
摘要翻译：用于织物洗涤剂组合物的表面活性化合物组合物，其基本上由（1）至少一种阳离子磺酸盐或硫酸盐型或非离子型乙氧基化型的二氧化硫，和（2）至少一种具有维生素和硝酸的羟基甲酰胺桥联物，其乙氧基化物/其氧化衍生物，其衍生物或其乙氧基化/丙氧基化的衍生物，其中组分（1）与组分（2）的量以100:1至1:1的重量比组成。表面活性化合物组合物可用于制备低温洗涤剂和低磷酸盐洗涤剂。

10. 发明授权

US4076743A Novel betaines, processes for the preparation thereof and recovery of underground petroleum therewith 失效
标题翻译：新颖的甜菜碱，其制备方法和回收地下石油
公开(公告)号：US4076743A
公开(公告)日：1978-02-28
申请号：US758035
申请日：1977-01-10
申请人： Karlheinz Koch , Horst Rutzen
发明人： Karlheinz Koch , Horst Rutzen
IPC分类号： C09K3/00 , C07C67/00 , C07C227/00 , C07C229/16 , C09K8/04 , C09K8/58 , C09K8/584 , C07C101/12 , C07C101/24
CPC分类号： C09K8/584 , Y10S507/936
摘要： The reaction of an aminoalkanol of the formula: ##STR1## wherein R.sup.1 and R.sup.2 are C.sub.1-17 aliphatic hydrocarbon groups (the sum of the carbon atoms in R.sup.1 + R.sup.2 being from 9 to 18); R.sup.3 and R.sup.4 represent the same or different C.sub.1-6 alkyl or alkylol groups; x represents a integer from 2 to 4; and y represents 0 or 1, with a water-soluble halocarboxylic acid provides quaternary ammonium compounds. The compounds are amphoteric surface-active agents which are soluble in water containing high concentrations of NaCl, and are useful in the recovery of underground petroleum by the flooding method.
摘要翻译：下式的氨基链烷醇的反应：其中R 1和R 2是C 1-17脂族烃基（R1 + R2中的碳原子总和为9-18）; R3和R4代表相同或不同的C1-6烷基或烷醇基; x表示2〜4的整数， y表示0或1，水溶性卤代羧酸提供季铵化合物。该化合物是可溶于含有高浓度NaCl的水的两性表面活性剂，可用于通过淹水法回收地下石油。

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