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1. 发明授权

US4937011A Detergent compositions containing active chlorine and ketone foam inhibitors 失效
标题翻译：含有活性氯和酮泡沫抑制剂的洗涤剂组合物
公开(公告)号：US4937011A
公开(公告)日：1990-06-26
申请号：US295880
申请日：1989-01-11
申请人： Karl-Heinz Schmid , Adolf Asbeck , Christoph Breucker , Bernhard Gutsche , Alfred Meffert , Horst Rutzen
发明人： Karl-Heinz Schmid , Adolf Asbeck , Christoph Breucker , Bernhard Gutsche , Alfred Meffert , Horst Rutzen
IPC分类号： B01D19/04 , C11D3/20 , C11D3/395
CPC分类号： C11D3/0026 , C11D3/2072 , C11D3/395
摘要： Alkaline dishwashing machine detergent compositions containing an active chlorine composition and a foam inhibiting amount of a ketone containing at least 25 carbon atoms. A process for their preparation wherein the ketone is introduced into the composition as a dispersion in a liquid.
摘要翻译：含有活性氯组合物和泡沫抑制量的含有至少25个碳原子的酮的碱性餐具洗涤机洗涤剂组合物。其制备方法，其中酮作为液体中的分散体引入组合物中。

2. 发明授权

US4678605A Cationic surfactants based on quaternary ammonium compounds and methods of using same 失效
标题翻译：基于季铵化合物的阳离子表面活性剂及其使用方法
公开(公告)号：US4678605A
公开(公告)日：1987-07-07
申请号：US820281
申请日：1986-01-17
申请人： Juergen Geke , Horst Rutzen
发明人： Juergen Geke , Horst Rutzen
IPC分类号： B01F17/38 , B01F17/18 , C11D1/62
CPC分类号： C11D1/62
摘要： The invention relates to new cationic surfactants based on quaternary ammonium compounds corresponding to the general formulaR.sup.1 -CHOH-CHR.sup.2 -N.sup.+ R.sup.3 R.sup.4 R.sup.5 R.sup.6 CO.sub.2.sup.- (1)whereinR.sup.1 is a linear or branched alkyl residue having from 1 to 22 carbon atoms;R.sup.2 is hydrogen or a linear or branched alkyl residue having from 1 to 21 carbon atoms, the total number of carbon atoms of the substituents R.sup.1 and R.sup.2 being in the range of from 8 to 22;R.sup.3 and R.sup.4 each represent methyl, ethyl, 2-hydroxyethyl or 2-hydroxypropyl;R.sup.5 represents an alkyl residue having from 4 to 6 carbon atoms or a phenalkyl residue having from 1 to 3 carbon atoms in the alkyl residue; andR.sup.6 represents a linear or branched alkyl residue having from 4 to 15 carbon atoms.The cationic surfactants have particular utility in cleaning agents.
摘要翻译：本发明涉及基于对应于通式R1-CHOH-CHR2-N + R3R4R5R6CO2-（1）的季铵化合物的新型阳离子表面活性剂，其中R1是具有1至22个碳原子的直链或支链烷基; R2是氢或具有1至21个碳原子的直链或支链烷基，取代基R 1和R 2的碳原子总数在8至22的范围内; R3和R4各自表示甲基，乙基，2-羟乙基或2-羟丙基; R5代表具有4至6个碳原子的烷基残基或在烷基残基中具有1至3个碳原子的苯烷基残基; 并且R 6表示具有4至15个碳原子的直链或支链烷基。阳离子表面活性剂在清洁剂中具有特别的用途。

3. 发明授权

US4480126A Process for the preparation of quaternary ammonium compounds 失效
标题翻译：制备季铵化合物的方法
公开(公告)号：US4480126A
公开(公告)日：1984-10-30
申请号：US369759
申请日：1982-04-19
申请人： Horst Rutzen
发明人： Horst Rutzen
IPC分类号： C11D3/30 , C07C67/00 , C07C209/00 , C07C209/12 , C07C211/63 , C07C211/64 , C09K3/16 , C11D1/62 , D06M13/02 , D06M13/322 , D06M13/385 , D06M13/46 , D06M13/463 , D06M16/00 , C07C91/40
CPC分类号： C11D1/62 , D06M13/385 , D06M13/463 , D06M16/00 , D06M2200/00 , D06M2200/50
摘要： Process for the preparation of quaternary ammonium compounds by reacting a tertiary amine with a vicinal halohydrin having at least 6 carbon atoms, and quaternary ammonium compounds prepared thereby.
摘要翻译：通过使叔胺与具有至少6个碳原子的连位卤代醇反应来制备季铵化合物的方法，以及由此制备的季铵化合物。

4. 发明授权

US4167421A Process for dispersing pigments and fillers using aminoalkanols and salt, alkoxylation and quaternization derivatives thereof 失效
标题翻译：使用氨基链烷醇和盐分散颜料和填料的方法，烷氧基化和季铵化衍生物
公开(公告)号：US4167421A
公开(公告)日：1979-09-11
申请号：US930228
申请日：1978-08-02
申请人： Heinrich Linden , Horst Rutzen , Bernd Wegemund
发明人： Heinrich Linden , Horst Rutzen , Bernd Wegemund
IPC分类号： C09C1/00 , C09B67/08 , C09B67/18 , C09B67/20 , C09C1/22 , C09C1/24 , C09C1/36 , C09C3/00 , C09C3/08 , C09D7/12
CPC分类号： C09B67/0011 , C09B67/0004 , C09B67/002 , C09C1/24 , C09C1/3692 , C09C3/006 , C01P2004/84
摘要： A process for improving the dispersibility of inorganic and organic pigments and fillers which comprises contacting said pigments and fillers with (a) aminoalkanols of the formulae ##STR1## wherein R.sub.1 is alkyl having 6 to 22 carbon atoms, R.sub.2 is hydrogen or methyl, provided there is only one methyl group per (CH).sub.x group, R.sub.3 and R.sub.4 are the same or different and are hydrogen, alkyl having 1 to 4 carbon atoms or hydroxyalkyl having 2 to 4 carbon atoms, x is an integer of from 2 to 6 and y is an integer of from 0 to 3, with the proviso that, if y is 0, R.sub.3 and R.sub.4 are not both hydrogen, or (b) salts, (c) alkoxylation products, and (d) quaternization products of said aminoalkanols, and recovering highly dispersible pigments and fillers.
摘要翻译：一种改善无机和有机颜料和填料的分散性的方法，其包括使所述颜料和填料与式（Ⅰ）或（II）的氨基链烷醇接触，其中R1是具有6-22个碳原子，R2为氢或甲基，条件是每个（CH）x基团仅有一个甲基，R 3和R 4相同或不同，为氢，具有1至4个碳原子的烷基或具有2至4个碳原子的羟基烷基，x为2〜6的整数，y为0〜3的整数，条件是如果y为0，则R3和R4不同时为氢，或（b）为盐，（c）烷氧基化产物，和（d）所述氨基链烷醇的季铵化产物，和回收高度分散的颜料和填料。

5. 发明授权

US4090969A Method of oil recovery by flooding employing betaine solutions 失效
标题翻译：采用甜菜碱溶液淹油回收方法
公开(公告)号：US4090969A
公开(公告)日：1978-05-23
申请号：US758039
申请日：1977-01-10
申请人： Karlheinz Koch , Horst Rutzen
发明人： Karlheinz Koch , Horst Rutzen
IPC分类号： C09K3/00 , C09K8/584 , E21B43/22
CPC分类号： C09K8/584 , Y10S507/936
摘要： A method of extracting mineral oil from subterranean formation by flooding comprising the steps of forcing an aqueous liquid into a subterranean formation containing mineral oil and displacing the mineral oil through at least one bore hole in the subterranean formation, said aqueous liquid containing from 0.01% to 15% by weight of an amphoteric surface-active compound selected from the group consisting of (1) a betaine having the formula ##STR1## wherein R.sub.1 and R.sub.2 are members selected from the group consisting of hydrogen and alkyl having from 1 to 18 carbon atoms, with the proviso that the sum of the carbon atoms in R.sub.1 + R.sub.2 is from 9 to 18, R.sub.3 and R.sub.4 are members selected from the group consisting of lower alkyl and lower alkylol, x is an integer from 2 to 4, y is an integer from 0 to 1 and z is an integer from 1 to 4, and (2) mixtures of said betaine with up to 20% by weight of an acid having the formula ##STR2## wherein R.sub.1, R.sub.2, R.sub.3, R.sub.4, x and z have the above-assigned values.
摘要翻译：一种通过淹水从地层中提取矿物油的方法，包括以下步骤：将含水液体强制进入含有矿物油的地层，并使矿物油通过地层中的至少一个钻孔排出，所述含水液体含有0.01％至 15重量％的选自以下的两性表面活性化合物：（1）具有式“IMAGE”的甜菜碱，其中R 1和R 2是选自氢和具有1至18个碳原子的烷基的成员，条件是R1 + R2中的碳原子总数为9至18，R3和R4为选自低级烷基和低级羟烷基的成员，x为2至4的整数，y为 0至1的整数，z为1至4的整数，和（2）所述甜菜碱与至多20重量％的具有下式的酸的混合物：其中R1，R2，R3，R4，x和 z具有上述赋值。

6. 发明授权

US4090845A Process for the dyeing of polyacrylonitrile fibrous material 失效
标题翻译：聚丙烯腈纤维材料染色工艺
公开(公告)号：US4090845A
公开(公告)日：1978-05-23
申请号：US750727
申请日：1976-12-15
申请人： Manfred Petzold , Heinz Grunert , Wolfgang Rupilius , Horst Rutzen
发明人： Manfred Petzold , Heinz Grunert , Wolfgang Rupilius , Horst Rutzen
IPC分类号： D06P1/66 , D06P3/76 , D06P5/04 , C07C85/00
CPC分类号： D06P3/76 , D06P1/66 , Y10S8/927 , Y10S8/929
摘要： Water-soluble quaternary ammonium compounds of the formula: ##STR1## wherein R.sub.1 and R.sub.2 are each alkyl groups of C.sub.1-15 chain length wherein the sum of the carbon atoms in said groups is 9 to 18; R.sub.3 represents a C.sub.1-5 alkyl or hydroxyalkyl group; R.sub.4 represents a C.sub.1-5 alkyl, hydroxyalkyl or benzyl group; R.sub.5 represents a benzyl group; and X represents a salt-forming anion, are effective retardant-levelling agents in the dyeing of anionic polyacrylonitrile fibers with basic (i.e. cationic) dyes.
摘要翻译：下式的水溶性季铵化合物：其中R1和R2各自是C1-15链长的烷基，其中所述基团中的碳原子之和为9至18; R3表示C1-5烷基或羟烷基; R4表示C1-5烷基，羟基烷基或苄基; R5表示苄基; 和X代表成盐阴离子，是用碱性（即阳离子）染料染色阴离子聚丙烯腈纤维的有效阻燃剂。

7. 发明授权

US5254722A Process for the production of triglycerides 失效
标题翻译：甘油三酯生产工艺
公开(公告)号：US5254722A
公开(公告)日：1993-10-19
申请号：US195995
申请日：1988-05-19
申请人： Eberhard Peukert , Horst Rutzen , Gerhard Wollmann
发明人： Eberhard Peukert , Horst Rutzen , Gerhard Wollmann
IPC分类号： C07C67/03 , B01J27/232 , C07B61/00 , C07C69/18 , C07C69/30
CPC分类号： C07C67/03
摘要： A process for the production of triglycerides of C.sub.1 -C.sub.4 alkyl esters of C.sub.6 -C.sub.22 fatty acids:a) where dry sodium carbonate catalyst is dissolved in glycerol and mixed with a molar excess of preferably the methyl ester of C.sub.6 -C.sub.22 fatty acid at a temperature between about 150.degree. C. and 250.degree. C. at less than atmospheric pressure and under substantially anhydrous conditions to produce an initial reaction mixture containing the corresponding triglycerides of said fatty acids, and partially reacted glycerol with unreacted hydroxyl groups (OH values 10-40),b) thereafter, a portion of the initial reaction mixture is reacted with additional C.sub.1 -C.sub.4 alkyl ester of C.sub.6 -C.sub.22 fatty acid under conditions to achieve substantially full conversion of said unreacted hydroxyl groups (OH values of 5 or less), andc) a product containing the corresponding triglycerides of said fatty acids is separated from unreacted alkyl ester and from the sodium carbonate catalyst. Improved light colored triglyceride products are achieved and can be separated readily from the sodium carbonate catalyst by filtration.
摘要翻译：制备C 6 -C 22脂肪酸的C 1 -C 4烷基酯的甘油三酸酯的方法：a）其中将干燥的碳酸钠催化剂溶解在甘油中，并与摩尔过量的优选C6-C22脂肪酸的甲酯在温度在约150℃至250℃之间，低于大气压和基本无水条件下，以产生含有所述脂肪酸的相应甘油三酸酯和部分反应的甘油与未反应的羟基的初始反应混合物（OH值10- 40），b）此后，一部分初始反应混合物与另外的C 6 -C 22脂肪酸的C 1 -C 4烷基酯在使所述未反应的羟基基本上完全转化（OH值为5以下）的条件下反应，和c）含有所述脂肪酸的相应甘油三酯的产物与未反应的烷基酯和碳酸钠催化剂分离。实现了改进的浅色甘油三酸酯产物，并且可以通过过滤容易地与碳酸钠催化剂分离。

8. 发明授权

US4923642A Quaternary ammonium compounds, their production and use in fabric aftertreatment preparations 失效
标题翻译：季铵化合物，其生产和用于织物后处理制剂
公开(公告)号：US4923642A
公开(公告)日：1990-05-08
申请号：US121267
申请日：1987-11-16
申请人： Horst Rutzen , Horst Baumann , Bert Gruber
发明人： Horst Rutzen , Horst Baumann , Bert Gruber
IPC分类号： D06M13/46 , C07C219/06 , C11D1/62 , D06M13/02 , D06M13/322 , D06M13/463
CPC分类号： C11D1/62 , D06M13/463 , D06M2200/50
摘要： Quaternary ammonium compounds containing one or two long-chain ester or amide radicals of etherified hydroxycarboxylic acids and, for the remainder, short-chain radicals, which are liquid to pasty substances that may readily be dissolved or dispersed in water or alcohol/water mixtures. They may be used in dilute or concentrated, storable form for softening fabrics without the absorbency of the treated fabrics being adversely affected. The quaternary ammonium compounds are obtained by reaction of epoxyfatty acid esters with amines and subsequent quaternization.
摘要翻译：含有一个或两个醚化羟基羧酸的长链酯或酰胺基团的季铵化合物，以及其余的短链基团，其是易于溶解或分散在水或醇/水混合物中的液态至糊状物质。它们可以以稀释或浓缩，可储存的形式用于软化织物，而不会对被处理织物的吸收性受到不利影响。季铵化合物通过环氧脂肪酸酯与胺的反应和随后的季铵化反应获得。

9. 发明授权

US4492802A Process for manufacture of quaternary ammonium compounds 失效
标题翻译：制备季铵化合物的方法
公开(公告)号：US4492802A
公开(公告)日：1985-01-08
申请号：US369760
申请日：1982-04-19
申请人： Horst Rutzen , Peter Nikolaus , Martin Bischoff , Rudolf Lehmann
发明人： Horst Rutzen , Peter Nikolaus , Martin Bischoff , Rudolf Lehmann
IPC分类号： D06M13/46 , A01N33/12 , B01J31/02 , C07B61/00 , C07C67/00 , C07C213/00 , C07C213/04 , C07C215/40 , C07C217/50 , C07D453/02 , C11D1/62 , D06M13/02 , D06M13/322 , D06M13/385 , D06M13/463 , D06M13/47 , D06M13/477 , C07C89/02
CPC分类号： A01N33/12 , C11D1/62 , D06M13/385 , D06M13/463 , D06M2200/50
摘要： Process for the manufacture of quaternary ammonium compounds by reacting a compound having a terminal epoxide troup with a salt of a tertiary amine in the presence of a quaternary ammonium compound as catalyst.
摘要翻译：通过在季铵化合物作为催化剂存在下使具有末端环氧化物团的化合物与叔胺的盐反应来制备季铵化合物的方法。

10. 发明授权

US4421932A Manufacture of quaternary ammonium compounds 失效
标题翻译：季铵化合物的制造
公开(公告)号：US4421932A
公开(公告)日：1983-12-20
申请号：US369810
申请日：1982-04-19
申请人： Horst Rutzen , Manfred Petzold
发明人： Horst Rutzen , Manfred Petzold
IPC分类号： C09K3/16 , A01N33/12 , C07B31/00 , C07B43/04 , C07C67/00 , C07C213/00 , C07C213/04 , C07C215/40 , C11D1/62 , D06M13/02 , D06M13/322 , D06M13/385 , D06M13/46 , D06M13/463 , C07C89/00
CPC分类号： C11D1/62 , A01N33/12 , D06M13/385 , D06M13/463 , D06M2200/00 , D06M2200/50
摘要： Process for the manufacture of quaternary ammonium compounds by reacting a compound having a terminal epoxy group with a tertiary amine which is partly present as the free amine and partly present in the form of a salt, followed by the addition of sufficient acid at the end of the reaction to complete salt formation of the quaternary ammonium compound.
摘要翻译：通过使具有末端环氧基的化合物与作为游离胺部分存在并部分以盐形式存在的叔胺反应制备季铵化合物的方法，然后在末端加入足够的酸完成季铵化合物盐形成的反应。

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