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1. 发明授权

US4696996A Preparation of polyphenylene ethers, and an apparatus for this purpose 失效
标题翻译：聚苯醚的制备及其用途
公开(公告)号：US4696996A
公开(公告)日：1987-09-29
申请号：US797884
申请日：1985-11-14
申请人： Hermann Brandt , Hermann Fischer , Hermann Dreher , Eduard Heil , Juergen Hambrecht , Herbert Naarmann , Adolf Echte , Hermann Gausepohl , Peter Siebel , Johann Swoboda , Gerd Schwoebel , Albert Nikles
发明人： Hermann Brandt , Hermann Fischer , Hermann Dreher , Eduard Heil , Juergen Hambrecht , Herbert Naarmann , Adolf Echte , Hermann Gausepohl , Peter Siebel , Johann Swoboda , Gerd Schwoebel , Albert Nikles
IPC分类号： B01J10/00 , B01J19/18 , C08G65/44 , C08G65/38
CPC分类号： C08G65/44 , B01J19/1862 , B01J19/1881 , B01J2219/00094 , B01J2219/00103 , B01J2219/0011
摘要： Polyphenylene ethers are prepared from monohydric phenols, which possess alkyl substituents in the two ortho-positions and, if desired, in the meta-position, but not in the para-position, by an oxidative coupling reaction with oxygen at from 15.degree. to 50.degree. C. and under from 1 to 10 bar in the presence of a catalyst complex, of a solvent and, if required, of an activator, by a method in which the conversion of the phenols is carried out in two more reaction zones, in which some or all of the solvent, the catalyst complex and the phenols and, where relevant, the activator is initially taken and is circulated by means of a conveying unit, and about 60-100% of the stoichiometric amount of oxygen required for the oxidative coupling is introduced into the first reaction zone and from 0 to about 40% of the said stoichiometric amount is introduced into the second reaction zone.
摘要翻译：聚苯醚由单羟基苯酚制得，它们在两个邻位具有烷基取代基，如果需要，在间位，而不是在对位，通过与15至50的氧的氧化偶联反应，在催化剂配合物存在下，在溶剂和如果需要的情况下，活化剂存在下，在1至10巴下，通过酚的转化在两个更多的反应区中进行，在其中一些或全部溶剂，催化剂络合物和酚，并且在相关的情况下，活化剂最初被摄取并通过输送单元循环，并且约60-100％的化学计量量的氧化所需的氧将偶联引入第一反应区，并将0至约40％的所述化学计量量引入第二反应区。

2. 发明授权

US4868235A Thermoplastic molding materials 失效
标题翻译：热塑性成型材料
公开(公告)号：US4868235A
公开(公告)日：1989-09-19
申请号：US260591
申请日：1988-10-21
申请人： Klaus Muehlbach , Michael Portugall , Karl Ruppmich , Erhard Seiler , Hermann Brandt
发明人： Klaus Muehlbach , Michael Portugall , Karl Ruppmich , Erhard Seiler , Hermann Brandt
IPC分类号： C08L51/04 , C08L69/00
CPC分类号： C08L51/04 , C08L69/00
摘要： A thermoplastic material containing, based in each case on the molding material comprising A and B,A from 30 to 80% be weight of one or more polycarbonates andB from 70 to 20% by weight of a blend of two different components B.sub.1 and B.sub.2, each of which consists of one or more graft copolymers b.sub.11 and b.sub.21 and each of which consists of one or more copolymers (hard matrix) b.sub.12 and b.sub.22, respectively, the graft copolymer b.sub.11 being prepared in emulsion and the graft copolymer b.sub.21 being prepared by another method.
摘要翻译：包含基于每种情况的包含A和B的成型材料的热塑性材料，30至80％的A为一种或多种聚碳酸酯的重量，B为70至20重量％的两种不同组分B1和B2的共混物各自由一种或多种接枝共聚物b11和b21组成，并且各自由一种或多种共聚物（硬质基体）b12和b22组成，接枝共聚物b11分别以乳液形式制备，接枝共聚物b21由另一种方法。

3. 发明授权

US4957965A Thermoplastic molding materials 失效
标题翻译：热塑性成型材料
公开(公告)号：US4957965A
公开(公告)日：1990-09-18
申请号：US228720
申请日：1988-08-05
申请人： Christof Taubitz , Klaus Muehlbach , Hermann Brandt , Klaus Boehlke
发明人： Christof Taubitz , Klaus Muehlbach , Hermann Brandt , Klaus Boehlke
IPC分类号： C08L21/00 , C08L25/02 , C08L51/08 , C08L71/00 , C08L71/12 , C08L77/00
CPC分类号： C08L77/00 , C08L71/126 , Y10S525/905
摘要： Thermoplastic molding materials contain, as essential components,(A) 5-95% by weight of a polyamide;(B) 5-95% by weight of a modified polyphenylene ether, prepared from(b.sub.1) 4.95-99.9% by weight of a polyphenylene ether,(b.sub.2) 0-90% by weight of a vinylaromatic polymer,(b.sub.3) 0.05-10% by weight of one or more compounds from the group consisting of(b.sub.31) an .alpha.,.beta.-unsaturated dicarbonyl compound,(b.sub.32) a monomer containing amide groups and a polymerizable double bond and(b.sub.33) a monomer containing lactam groups and a polymerizable double bond,(b.sub.4) 0-80% by weight of further graft-active monomers and(b.sub.5) 0.01-0.09% by weight of a free radical initiator,(C) 0-90% by weight of an unmodified polyphenylene ether,(D) 0-45% by weight of a vinylaromatic polymer and(E) 0-40% by weight of a rubber impact modifier.
摘要翻译：热塑性成型材料作为必要成分含有（A）5-95重量％的聚酰胺; （B）5-95重量％的由（b1）4.95-99.9重量％的聚苯醚制备的改性聚苯醚，（b2）0-90重量％的乙烯基芳族聚合物，（b3）0.05- 10重量％的一种或多种选自（b31）α，β-不饱和二羰基化合物，（b32）含酰胺基和可聚合双键的单体的化合物和（b33）含有内酰胺基团的单体和（b4）0-80重量％的另外的接枝活性单体和（b5）0.01-0.09重量％的自由基引发剂，（C）0-90重量％的未改性聚苯醚，（D）0-45重量％的乙烯基芳族聚合物和（E）0-40重量％的橡胶抗冲改性剂。

4. 发明授权

US06329448B1 Method for producing dyed moulding materials 有权
标题翻译：染色成型材料的制造方法
公开(公告)号：US06329448B1
公开(公告)日：2001-12-11
申请号：US09486636
申请日：2000-02-29
申请人： Herbert Gutsche , Rainer Anderlik , Norbert Kress , Dieter Gress , Bernd Brian , Petra Baierweck , Herbert Mosner , Hermann Brandt , Helmut Heel
发明人： Herbert Gutsche , Rainer Anderlik , Norbert Kress , Dieter Gress , Bernd Brian , Petra Baierweck , Herbert Mosner , Hermann Brandt , Helmut Heel
IPC分类号： C08J320
CPC分类号： B29C47/1063 , B29C47/0011 , B29C47/1027 , B29K2105/0005
摘要： A continuous process for preparing pigmented thermoplastic molding compositions in an extruder, comprises I) in a first zone A) metering in from 10 to 99.999% by weight of a thermoplastic polymer into an extruder and II) in a subsequent zone at temperatures below the respective glass transition temperature of the thermoplastic A) B) adding from 0.001 to 60% by weight of a colorant and then heating the thermoplastic/colorant mixture in the subsequent zones, homogenizing the polymer melt and extruding the resultant mixture.
摘要翻译：在挤出机中制备着色热塑性模塑组合物的连续方法包括：I）在第一区域A）将10至99.999重量％的热塑性聚合物计量到挤出机中，和ii）在低于相应玻璃化转变温度的热塑性A）B）添加0.001至60重量％的着色剂，然后在随后的区域中加热热塑性/着色剂混合物，均化聚合物熔体并挤出所得混合物。

5. 发明授权

US4948832A Reinforced thermoplastic molding materials based on polyphenylene ether 失效
标题翻译：基于聚苯醚的增强热塑性成型材料
公开(公告)号：US4948832A
公开(公告)日：1990-08-14
申请号：US281755
申请日：1988-12-09
申请人： Bertram Ostermayer , Ehrenfried Baumgartner , Rainer Bueschl , Hermann Brandt , Klaus Boehlke , Erhard Seiler , Graham E. McKee
发明人： Bertram Ostermayer , Ehrenfried Baumgartner , Rainer Bueschl , Hermann Brandt , Klaus Boehlke , Erhard Seiler , Graham E. McKee
IPC分类号： C08L51/04 , C08L71/12 , C08L77/00
CPC分类号： C08L51/04 , C08L71/123 , C08L77/00
摘要： Reinforced thermoplastic molding materials containing, as essential components,(A) from 40 to 94 parts by weight of a polymer component of(a.sub.1) from 10 to 90% by weight of polyphenylene ether and(a.sub.2) from 10 to 90% by weight, based in each case on A, of a styrene polymer toughened with an acrylate rubber or with an unhydrogenated or hydrogenated polymer of a conjugated diene,(B) from 1 to 20 parts by weight of a copolymer of(b.sub.1) from 70 to 99.9% by weight of a monomer from the group consisting of styrene, .alpha.-methylstyrene and styrene alkylated in the nucleus or a mixture of these monomers,(b.sub.2) from 0.1 to 30% by weight of one or more compounds from the group consisting of tert-butyl acrylate and tert-butyl methacrylate, or one or more compounds from the group of compounds of the general formula I ##STR1## where R.sup.1 is hydrogen or methyl and R.sup.2, R.sup.3 and R.sup.4 are each an alkyl or alkoxy group of not more than 4 carbon atoms, or of the general formula II ##STR2## where n is an integer from 1 to 4 and R.sup.5, R.sup.6 and R.sup.7 are each one of the radicals stated for R.sup.2 or are each --O(CH.sub.2 --CH.sub.2 --O).sub.m R.sup.8, where R.sup.8 is C.sub.1 -C.sub.4 -alkyl and m is 1, 2, 3 or 4, and(b.sub.3) from 0 to 10% by weight, based on the copolymer, of a further ethylenically unsaturated monomer which is copolymerizable with b.sub.1 and b.sub.2, and(C) from 5 to 50 parts by weight of a reinforcing agent, the number of parts by weight being based on 100 parts by weight of the sum of A, B and C,are prepared and used for the production of moldings.
摘要翻译：作为必要成分的增强热塑性成型材料含有（A）40〜94重量份聚合物成分（a1），10〜90重量％聚苯醚和（a2）10〜90重量％基于A的每种情况，使用丙烯酸酯橡胶或共轭二烯的未氢化或氢化的聚合物增韧的苯乙烯聚合物，（B）1至20重量份的（b1）70至99.9重量％的共聚物，重量的来自于在核中烷基化的苯乙烯，α-甲基苯乙烯和苯乙烯的单体或这些单体的混合物，（b2）0.1-30％（重量）一种或多种下列化合物：叔 - 丙烯酸丁酯和甲基丙烯酸叔丁酯，或一种或多种通式Ⅰ化合物的化合物，其中R1是氢或甲基，R2，R3和R4分别是烷基或烷氧基不大于 4个碳原子，或通式II其中n是一个整数 1至4的取代基和R 5，R 6和R 7各自为R 2所示的基团之一或分别为-O（CH 2 -CH 2 -O）m R 8，其中R 8为C 1 -C 4 - 烷基且m为1,2,3 或（4）和（b3）0〜10重量％，基于共聚物，可与b1和b2共聚的另外的烯属不饱和单体和（C）5〜50重量份的增强剂，制备基于100重量份的A，B和C之和的重量份数，并用于制造模制品。

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