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1. 发明授权

US3962116A Compositions of optical brightness and aluminosilicates and methods of their production 失效
标题翻译：光学亮度和铝酸盐的组成及其生产方法
公开(公告)号：US3962116A
公开(公告)日：1976-06-08
申请号：US541208
申请日：1975-01-15
申请人： Helmut Bloching , Heinz Smolka , Milan Johann Schwuger
发明人： Helmut Bloching , Heinz Smolka , Milan Johann Schwuger
IPC分类号： D06L3/12 , C09K11/30
CPC分类号： D06L3/1264
摘要： Heat dried, finely-divided compositions of optical brighteners and fillers comprising as said fillers at least partly of a finely-divided water-insoluble silicate compound containing at least some combined water and having a calcium binding power of at least 50 mg CaO/gm of anhydrous active substance and the formula on the anhydrous basis(M.sub.2 /.sub.n O).sub.x . Me.sub.2 O.sub.3 . (SiO.sub.2).sub.ywhere M is a cation of the valence n, exchangeable with calcium, x is a member of from 0.7 to 1.5, Me is a member selected from the group consisting of aluminum and boron, and y is a number from 0.8 to 6, preferably from 1.3 to 4, in an amount of at least 5% by weight of the mixture, as well as a process for producing the same comprising the steps of mixing said silicate compound, while at least still moist from its production, with said optical brighteners and converting the entire mixture of components into a pourable product.
摘要翻译： 1499902荧光增白剂和填充剂DEUTSCHE GOLD - UND SILBER-SCHEIDEAN雪松和HENKEL＆CIE GmbH 1975年1月16日[1974年1月17日] 1869/75标题D1P干粉状组合物含有荧光增白剂和细分（最大粒径0.1mm）具有至少50mg CaO / g无水硅酸盐（= AS）的钙结合能力和通式的水不溶性铝 - 或硼硅酸盐; 其中Cat表示可与钙交换的阳离子和n价的x，x表示0.7至1.5的数，M表示硼或铝，y表示0.8至6的数。可交换阳离子可以是氢，锂，钾，铵或镁或水溶性有机碱的阳离子，但优选为钠。增白剂对棉，聚酰胺或聚酯可能是实质的，并且可以是二氨基芪二磺酸，二芳基吡唑啉喹诺酮，1,2-二（2-苯并恶唑基） - 或1,2-二 - （2-苯甲酰亚氨基唑基） - 乙烯，苯并恶唑基噻吩，香豆素或曲辛二烯二苯基衍生物。组合物可以通过热干燥形成。通过单一喷雾或辊子，组分的浆料。在改性中，形成硅酸盐，例如，通过将铝酸钠和硅酸钠混合在水性悬浮液中，在光亮剂存在下，其在干燥时由硅酸盐涂覆。因此可以形成空心珠。硅酸盐可以是无定形或微晶的。其他水溶性或细分散的水不溶性惰性物质也可能存在。

2. 发明授权

US4071377A Method of mechanical dishwashing and compositions 失效
标题翻译：机械洗碗和组合物的方法
公开(公告)号：US4071377A
公开(公告)日：1978-01-31
申请号：US458333
申请日：1974-04-05
申请人： Milan Johann Schwuger , Heinz Smolka , Theodor Altenschopfer , Manfred Rostek
发明人： Milan Johann Schwuger , Heinz Smolka , Theodor Altenschopfer , Manfred Rostek
IPC分类号： C11D7/60 , A47L15/44 , C11D3/00 , C11D3/02 , C11D3/08 , C11D3/10 , C11D3/12 , A47L15/00 , C02B1/44 , C11D3/60
CPC分类号： C11D3/128 , C11D1/72 , C11D11/0023 , C11D3/044 , C11D3/08 , C11D3/10 , C11D3/3955 , Y10S423/24
摘要： A method for the mechanical washing of dishes, wherein the soiled dishes are treated with an aqueous alkaline liquor having a pH of from 8 to 13 which contains at least one compound inhibiting alkaline earth metal ion precipitation, rinsing and recovering cleaned dishes comprising using finely-dispersed, water-insoluble silicate compounds having a calcium-binding power of at least 50 mg CaO/gm of anhydrous substance and having the formula, combined water not shown, of(M.sub.2/n O).sub.x .multidot. Me.sub.2 O.sub.3 .multidot. (SiO.sub.2).sub.ywhere M is a cation of the valence n, exchangeable with calcium, x is a number of from 0.7 to 1.5, Me is a member selected from aluminum and boron and y is a number of from 0.8 to 6, as said compound inhibiting alkaline earth metal ion precipitation as well as alkaline-reacting mechanical dish washing compositions containing said silicate compounds.
摘要翻译：一种用于机械洗涤餐具的方法，其中用含有至少一种抑制碱土金属离子沉淀的化合物的pH为8至13的碱性水溶液处理污染的菜肴，冲洗并回收清洁的菜肴，（M2 / nO）xxMe2O3 x（SiO2）y WHERE M为（M2 / nO）xxMe2O3 x（SiO2）y的组合水，分散的水不溶性硅酸盐化合物，其钙结合能力为至少50mg CaO / gm无水物质，化合价n的阳离子可与钙交换，x为0.7〜1.5，Me为选自铝和硼的成员，y为0.8〜6的数，作为所述抑制碱土金属离子析出的化合物以及含有所述硅酸盐化合物的碱性反应机械洗碗组合物。

3. 发明授权

US4092261A Process for the production of powdery washing and cleansing agent compositions 失效
标题翻译：生产粉状洗涤剂和清洁剂组合物的方法
公开(公告)号：US4092261A
公开(公告)日：1978-05-30
申请号：US620386
申请日：1975-10-07
申请人： Gerhard Sperling , Dieter Jung , Klaus Hachmann , Milan Johann Schwuger , Heinz Smolka
发明人： Gerhard Sperling , Dieter Jung , Klaus Hachmann , Milan Johann Schwuger , Heinz Smolka
IPC分类号： C11D1/02 , C11D1/66 , C11D1/72 , C11D1/88 , C11D3/00 , C11D3/12 , C11D10/04 , C11D11/00 , C02B1/44 , C11D9/18 , C11D11/02
CPC分类号： C11D11/0082 , C11D10/04 , C11D3/128 , C11D1/02 , C11D1/66 , C11D1/72 , C11D1/88
摘要： An improvement in the process for the production of powdery washing and cleansing agent compositions containing finely-divided water-insoluble silicate compounds, capable of binding calcium, soap, and, optionally, other surface-active compounds, builders and other customary detergent additives by spray-drying a slurry and recovering said powdery washing and cleansing agent composition which comprises separately spray-drying a slurry rich in said silicate compounds and combining the spray-dried powders with the remaining ingredients in powdery form; as well as the powdery washing and cleansing agents so produced.
摘要翻译：生产含有精细分散的水不溶性硅酸盐化合物的粉末洗涤和清洁剂组合物的方法的改进，其能够通过喷雾结合钙，皂和任选的其它表面活性化合物，助洗剂和其它常规洗涤剂添加剂干燥浆料并回收所述粉末洗涤和清洁剂组合物，其包括分别喷雾富含所述硅酸盐化合物的浆料并将喷雾干燥的粉末与粉末形式的其余成分组合; 以及如此生产的粉末洗涤和清洁剂。

4. 发明授权

US4083793A Washing compositions containing aluminosilicates and nonionics and method of washing textiles 失效
标题翻译：含有硅铝酸盐和非离子表面活性剂的洗涤组合物和洗涤纺织品的方法
公开(公告)号：US4083793A
公开(公告)日：1978-04-11
申请号：US723728
申请日：1976-09-16
申请人： Gunter Jakobi , Peter Krings , Milan Johann Schwuger , Heinz Smolka
发明人： Gunter Jakobi , Peter Krings , Milan Johann Schwuger , Heinz Smolka
IPC分类号： C11D1/83 , C11D3/08 , C11D3/12 , B01J1/04 , C11D1/825 , C11D1/831
CPC分类号： C11D3/08 , C11D1/8305 , C11D3/1286
摘要： A method of washing soiled textiles, wherein the soiled textiles are immersed in an aqueous liquor which contains at least one compound inhibiting alkaline earth metal ion precipitation on said soiled textiles and surface-active compounds comprising using finely-dispersed, water-insoluble silicate compounds having a calcium-binding power of at least 50 mg CaO/gm of anhydrous active substance and having the formula, combined water not shown(M.sub.2/n O).sub.x . Me.sub.2 O.sub.3 . (SiO.sub.2).sub.ywhere M is a cation of the valence n, exchangeable with calcium, x is a number of from 0.7 to 1.5, Me is a member selected from aluminum and boron and y is a number of from 0.8 to 6, as said compound inhibiting alkaline earth metal ion precipitation, together with surface-active compounds including non-ionic surface-active compounds being constituted by a mixture of compounds of different degrees of ethoxylation where one of the ethoxylated compounds has 8 to 20 ethylene oxide units and the other has from 2 to 6 ethylene oxide units; as well as washing compositions containing said silicate compounds and said surface-active compounds.
摘要翻译：一种洗涤污染织物的方法，其中将污染的纺织品浸入含有至少一种抑制碱土金属离子沉淀的化合物的水性液体中，所述化合物在所述污染的纺织品和表面活性化合物上包括使用细分散的水不溶性硅酸盐化合物，具有至少50mg CaO / gm无水活性物质并具有下式的组合水（M2 / nO）x的钙结合力。 Me2O3。（SiO 2）y其中M是价数为n的阳离子，可与钙交换，x为0.7至1.5的数，Me为选自铝和硼的成员，y为0.8至6的数，如所述化合物抑制碱土金属离子沉淀，以及包括非离子表面活性化合物在内的表面活性化合物由不同程度乙氧基化的化合物的混合物构成，其中一种乙氧基化合物具有8至20个环氧乙烷单元，另一种具有2至6个环氧乙烷单元; 以及含有所述硅酸盐化合物和所述表面活性化合物的洗涤组合物。

5. 发明授权

US4136051A Pourable washing compositions containing a luminosilicates and non-ionics and method for their preparation 失效
标题翻译：含有乳酸和非离子体的可洗涤组合物及其制备方法
公开(公告)号：US4136051A
公开(公告)日：1979-01-23
申请号：US814046
申请日：1977-07-08
申请人： Herbert Saran , Peter Krings , Milan J. Schwuger , Heinz Smolka
发明人： Herbert Saran , Peter Krings , Milan J. Schwuger , Heinz Smolka
IPC分类号： C11D1/66 , C11D3/12 , C11D11/00 , C11D17/00 , C02B1/44 , C11D3/39 , C11D17/06
CPC分类号： C11D3/3942 , C11D1/66 , C11D11/0082 , C11D11/0088 , C11D17/0034 , C11D3/128
摘要： Pourable washing agent compositions comprising essentially a premix powder component and optionally a second powder component obtained by hot drying of an aqueous composition containing conventional heat-insensitive components, consisting essentially of(1) from 30% to 100% by weight of a premix consisting essentially of(A) finely-dispersed, water-insoluble silicate compounds having a calcium-binding power of at least 50 mg CaO/gm of anhydrous active substance and having the formula, combined water not shown, of(M.sub.2/n O).sub.x .multidot. Me.sub.2 O.sub.3 .multidot. (SiO.sub.2).sub.y where M is a cation of the valence n, exchangeable with calcium, x is a number of from 0.7 to 1.5, Me is a member selected from aluminum and boron and y is a number of from 0.8 to 6, which silicate compounds optionally are partly replaced by highly dispersed silica in amounts of not more than 4% by weight, based on the weight of the premix;(B) optionally bleaching components selected from the group consisting of inorganic peroxyhydrate compounds capable of supplying H.sub.2 O.sub.2 in water, activators for percompounds, stabilizers for percompounds and mixtures thereof;(C) non-ionic surface-active compounds finely distributed on and throughout component (A) or the mixture of components (A) and (B);where the mixture of component (A) to component (C) is in the ratio of 10:1 to 1:3; and(2) from 0 to 70% by weight of a powdery component obtained by hot drying of an aqueous composition containing conventional heat-insensitive washing components; as well as a process for the production of said pourable washing compositions.

6. 发明授权

US4755319A Process for the production of solid, pourable washing or cleaning agents with a content of a calcium binding silicate 失效
标题翻译：用于生产具有钙结合硅酸盐含量的固体，可倾倒的洗涤剂或清洁剂的方法
公开(公告)号：US4755319A
公开(公告)日：1988-07-05
申请号：US437518
申请日：1982-10-29
申请人： Heinz Smolka , Milan J. Schwuger
发明人： Heinz Smolka , Milan J. Schwuger
IPC分类号： C01B39/00 , C01B39/02 , C01B39/06 , C11D3/00 , C11D3/12 , C01B33/28 , C02F1/42 , C11D11/00
CPC分类号： C11D3/128
摘要： A process for the production of solid, pourable, washing or cleaning agents containing surface-active compounds, builders, and calcium binding compounds, said calcium binding compounds consisting of at least one finely-dispersed water-insoluble silicate compound containing at least some combined water and having a calcium binding power of at least 50 mg CaO/gm of anhydrous active substance and the formula on the anhydrous basis:(M.sub.2/n O).sub.x .multidot.Me.sub.2 O.sub.3 .multidot.(SiO.sub.2).sub.ywhere M is a cation of the valence n, exchangeable with calcium, x is a member of from 0.7 to 1.5, Me is a member selected from the group consisting of aluminum and boron, and y is a number form 0.8 to 6, comprising the steps of mixing said silicate compound, while still moist from its production, with at least part of the remaining components of the washing and cleaning agent and converting the entire mixture of components into a pourable product.
摘要翻译：一种用于生产含有表面活性化合物，助洗剂和钙结合化合物的固体，可倾倒，洗涤或清洁剂的方法，所述钙结合化合物由至少一种细分散的水不溶性硅酸盐化合物组成，所述硅酸盐化合物含有至少一些组合的水并且具有至少50mg CaO / gm的无水活性物质的钙结合能力和以无水为基准的式：（M2 / nO）xxMe2O3x（SiO2）y其中M是价数为n的阳离子，可与钙交换， x为0.7〜1.5的成员，Me为选自铝和硼的成员，y为数字形式，为0.8〜6，包括以下步骤：将硅酸酯化合物从其生产中仍然湿润，与洗涤和清洁剂的剩余组分的至少一部分并将整个组分混合物转化成可倾倒的产品。

7. 发明授权

US4330423A Process for the production of solid, pourable washing or cleaning agents with a content of a calcium binding silicate 失效
标题翻译：用于生产具有钙结合硅酸盐含量的固体，可倾倒的洗涤剂或清洁剂的方法
公开(公告)号：US4330423A
公开(公告)日：1982-05-18
申请号：US813436
申请日：1977-07-07
申请人： Heinz Smolka , Milan J. Schwuger
发明人： Heinz Smolka , Milan J. Schwuger
IPC分类号： C01B39/00 , C01B39/02 , C01B39/06 , C11D3/00 , C11D3/12 , C01B33/28 , C02F1/42 , C11D11/00
CPC分类号： C11D3/128
摘要： A process for the production of solid, pourable, washing or cleaning agents containing surface-active compounds, builders, and calcium binding compounds, said calcium binding compounds consisting of at least one finely-dispersed water-insoluble silicate compound containing at least some combined water and having a calcium binding power of at least 50 mg CaO/gm of anhydrous active substance and the formula on the anhydrous basis(M.sub.2 /n.sup.O)x.Me.sub.2 O.sub.3.(SiO.sub.2).sub.ywhere M is a cation of the valence n, exchangeable with calcium, x is a member of from 0.7 to 1.5, Me is a member selected from the group consisting of aluminum and boron, and y is a number from 0.8 to 6, comprising the steps of mixing said silicate compound, while still moist from its production, with at least part of the remaining components of the washing and cleaning agent and converting the entire mixture of components into a pourable product.
摘要翻译：一种用于生产含有表面活性化合物，助洗剂和钙结合化合物的固体，可倾倒，洗涤或清洁剂的方法，所述钙结合化合物由至少一种细分散的水不溶性硅酸盐化合物组成，所述硅酸盐化合物含有至少一些组合的水并且具有至少50mg CaO / gm无水活性物质的钙结合力和无水基础上的式（M2 / nO）x.Me 2 O 3（SiO 2）y，其中M是价数n的阳离子，可与钙，x为0.7〜1.5的成员，Me为选自铝和硼的成员，y为0.8至6的数，包括以下步骤：将所述硅酸盐化合物从其中生产，至少部分洗涤和清洁剂的剩余组分，并将整个组分混合物转化成可倾倒的产品。

8. 发明授权

US4179268A Method of machine washing of solid soiled materials by reversibly contacting the circulating wash liquid with aluminosilicates 失效
标题翻译：通过将循环洗涤液与铝硅酸盐可逆地接触来洗涤固体污染物质的方法
公开(公告)号：US4179268A
公开(公告)日：1979-12-18
申请号：US852028
申请日：1977-11-16
申请人： Elmar Reinwald , Heinz Smolka , Milan J. Schwuger , Edgar Koppelmann
发明人： Elmar Reinwald , Heinz Smolka , Milan J. Schwuger , Edgar Koppelmann
IPC分类号： B08B3/08 , B01D15/04 , C11D3/12 , C11D11/00 , D06F39/10 , D06L1/12 , B08B3/00 , C02B1/00
CPC分类号： C11D3/128 , C11D11/0005 , D06F39/10 , D06L1/12
摘要： An improvement in the machine washing of solid soiled materials comprising withdrawing and recycling the wash liquor in contact with said solid soiled materials through a silicate cation exchange compound having some combined water and a particle size of at least 10.mu. of the formula:(M.sub.2/n O).sub.x.Me.sub.2 O.sub.3.(SiO.sub.2).sub.ywherein M is a cation of valence n exchangeable with calcium, Me is a member selected from aluminum and boron, x is a number from 0.7 to 1.5 and y is a number from 0.8 to 6, said silicate compound having a calcium binding power of at least 50 mg of CaO per gram, said silicate compound being maintained out of contact with said solid soiled materials, for such time that the recycling wash liquor has passed through said silicate compound at least twice, in the presence of other soluble washing and cleaning compounds, while reversing the direction of flow of said wash liquor through said silicate compound repeatedly.
摘要翻译：固体污染物质的洗涤方法的改进包括通过具有一定组合的水和至少10微米的粒径的硅酸盐阳离子交换化合物来取出和再循环与所述固体污染物接触的洗涤液：（M2 / nO）x.Me 2 O 3（SiO 2）y其中M是可与钙交换的价数n的阳离子，Me是选自铝和硼的成员，x是0.7至1.5的数，y是0.8至6的数，所述硅酸盐化合物具有每克至少50mg CaO的钙结合力，所述硅酸盐化合物与所述固体污染的材料保持脱离接触，使得再循环洗涤液已经通过所述硅酸盐化合物至少两次，在其它可溶性洗涤和清洁化合物的存在下，同时反复地将所述洗涤液体的流动方向反转通过所述硅酸盐化合物。

9. 发明授权

US4148603A Method of washing textiles and composition containing inorganic silicates and polycarboxylates and/or polyphosphonates 失效
标题翻译：洗涤纺织品和含有无机硅酸盐和聚羧酸盐和/或多聚膦酸盐的组合物的方法
公开(公告)号：US4148603A
公开(公告)日：1979-04-10
申请号：US873381
申请日：1978-01-30
申请人： Milan J. Schwuger , Heinz Smolka , Manfred Rostek
发明人： Milan J. Schwuger , Heinz Smolka , Manfred Rostek
IPC分类号： C11D3/00 , C11D3/12 , B08B3/00
CPC分类号： C11D3/128 , C11D3/364
摘要： A method of treating soiled textiles, wherein the soiled textiles are immersed in an aqueous liquor which contains at least two compounds inhibiting alkaline earth metal ion precipitation on said soiled textiles comprising using (1) from 0.2 to 10 gm of anhydrous active substance per liter of at least one finely-dispersed, water-insoluble silicate compound having a calcium-binding power of at least 50 mg CaO/gm of anhydrous active substance and having the formula, combined water not shown(M.sub.2/n O).sub.x . Me.sub.2 O.sub.3 . (SiO.sub.2).sub.ywhere M is a cation of the valence n, exchangeable with calcium, x is a number of from 0.7 to 1.5, Me is aluminum or boron, and y is a number from 0.8 to 6, and (2) from 0.05 to 2gm/l of at least one of certain polyphosphonates; as well as washing compositions containing said at least two compounds.
摘要翻译：一种处理污染纺织品的方法，其中将污染的纺织品浸入含有至少两种抑制所述污染纺织品上的碱土金属离子沉淀的化合物的水性液体中，其中包括使用（1）0.2至10克无水活性物质/ 至少一种细分散的水不溶性硅酸盐化合物，其钙结合力为至少50mg CaO / gm的无水活性物质，并具有下式，组合水未示出（M2 / nO）x。 Me2O3。（SiO 2）y其中M是价数为n的阳离子，可与钙交换，x为0.7至1.5的数，Me为铝或硼，y为0.8至6的数，（2）为0.05 至2gm / l的某些多聚膦酸酯中的至少一种; 以及含有所述至少两种化合物的洗涤组合物。

10. 发明授权

US4126574A Surfactant-containing aluminosilicates and process 失效
标题翻译：含表面活性剂的硅铝酸盐和工艺
公开(公告)号：US4126574A
公开(公告)日：1978-11-21
申请号：US811964
申请日：1977-06-30
申请人： Elmar Reinwald , Milan J. Schwuger , Heinz Smolka
发明人： Elmar Reinwald , Milan J. Schwuger , Heinz Smolka
IPC分类号： B01J39/08 , C11D3/12 , C01B33/28 , C02B1/44 , C11D1/38
CPC分类号： B01J39/085 , C01B33/28 , C11D3/128 , C11D3/1286 , Y10S516/07
摘要： This invention relates to cation-exchanging, water-insoluble aluminosilicates containing bound water and an ionic surface-active compound resistant to water hardness formers and having, for every mol of Al.sub.2 O.sub.3, from 0.7 to 1.5 mols Cat.sub.2/n O, where Cat is a cation having the valence n, and from 0.8 to 6 mols SiO.sub.2, and being produced by the precipitation of said aluminosilicate in an aqueous solution, wherein said reaction is conducted in the presence of an aqueous solution of said ionic surface-active compound, and optional subsequent crystallization; as well as a process for its preparation and a process for the sequestration of water hardness cations employing said aluminosilicates.
摘要翻译：本发明涉及含有结合水的阳离子交换的水不溶性硅铝酸盐和对水硬化剂具有抗性的离子表面活性化合物，并且对于每摩尔Al 2 O 3，具有0.7至1.5摩尔的Cat2 / nO，其中Cat是阳离子具有n价和0.8至6摩尔SiO 2，并且通过在水溶液中沉淀所述铝硅酸盐而制备，其中所述反应在所述离子表面活性化合物的水溶液存在下进行，并且任选地随后结晶; 以及其制备方法和使用所述铝硅酸盐螯合水硬度阳离子的方法。

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