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1. 发明授权

US5981773A Preparation of perylene-3,4-dicarboxylic anhydrides 失效
标题翻译：苝-3,4-二羧酸酐的制备
公开(公告)号：US5981773A
公开(公告)日：1999-11-09
申请号：US7195
申请日：1998-01-14
申请人： Heinz Langhals , Petra Christa Von Unold , Markus Speckbacher
发明人： Heinz Langhals , Petra Christa Von Unold , Markus Speckbacher
IPC分类号： C07C51/38 , C07C63/44 , C07D221/18 , C07D311/78 , C09B3/18 , C09B5/62
CPC分类号： C09B5/62 , C07C51/38 , C07C63/44 , C07D221/18 , C09B3/18
摘要： A process for forming perylene-3, 4-dicarboxylic anhydrides by reacting a corresponding perylene-3,4:9, 10-tetracarboxylic dianhydride with a sterically hindered amine, as a base, at an elevated temperature.
摘要翻译：通过相应的苝-3,4：9,10-四羧酸二酐与空间位阻胺作为碱在高温下反应形成苝-3,4-二羧酸酐的方法。

2. 发明授权

US5886183A Naphthalenelactamimide fluorescence dyes 失效
标题翻译：萘酰胺酰亚胺荧光染料
公开(公告)号：US5886183A
公开(公告)日：1999-03-23
申请号：US729124
申请日：1996-10-11
申请人： Heinz Langhals , Petra Christa von Unold
发明人： Heinz Langhals , Petra Christa von Unold
IPC分类号： C07D221/14 , B41M5/26 , C07D471/06 , C09B57/08 , C09K9/02 , C09K11/06 , C07D221/00 , C07D471/02
CPC分类号： C07D471/06 , C09B57/08 , C09K11/06
摘要： Naphthalenelactamimides of the formula I ##STR1## in which, for example, R.sub.1 and R.sub.2 are 2,5-di-tert-butylphenyl and m and n are 0, are novel dyes which have the distinctive features of pronounced fluorescence as a solid and in solvents and a good light-fastness. They are therefore suitable, for example, for mass dyeing of high molecular weight organic material, as laser dyes and for the preparation of printing toners, colour filters, organic photoreceptors, electroluminescent and photoluminescent elements, optical information storage media or solar collectors. The compounds of the the formula I can be prepared by reaction of the corresponding naphthalenetetracarboxylic acid bisimides with a base.
摘要翻译：其中例如R 1和R 2为2,5-二叔丁基苯基且m和n为0的式I（I）的萘内酰胺酰胺是具有显着荧光的独特特征的新颖染料，固体和溶剂，耐光性好。因此，它们适用于例如用于高分子量有机材料的大量染色，作为激光染料和用于制备印刷调色剂，滤色器，有机感光体，电致发光和光致发光元件，光学信息存储介质或太阳能收集器。式I的化合物可以通过相应的萘四羧酸双酰亚胺与碱的反应来制备。

3. 发明授权

US08404705B2 Naphthalene amidine imides 有权
标题翻译：萘脒酰亚胺
公开(公告)号：US08404705B2
公开(公告)日：2013-03-26
申请号：US11989163
申请日：2006-07-21
申请人： Heinz Langhals , Harald Jaschke , Thomas Ehlis , Olof Wallquist
发明人： Heinz Langhals , Harald Jaschke , Thomas Ehlis , Olof Wallquist
IPC分类号： A61K31/439 , C07D471/08
CPC分类号： C09B5/62 , C07D471/04
摘要： Disclosed are naphthalinamidinimide of formula wherein the substituents R1-R8 are defined herein.
摘要翻译：公开了下式的萘胺亚胺，其中取代基R 1 -R 8在本文中定义。

4. 发明申请

US20100202984A1 Naphthalene amidine imides 有权
公开(公告)号：US20100202984A1
公开(公告)日：2010-08-12
申请号：US11989163
申请日：2006-07-21
申请人： Heinz Langhals , Harald Jaschke , Thomas Ehlis , Olof Wallquist
发明人： Heinz Langhals , Harald Jaschke , Thomas Ehlis , Olof Wallquist
IPC分类号： A61K8/49 , A61K31/4375 , A61Q17/04 , A61Q19/00 , C07D471/22 , A61P43/00 , A61K31/438 , C07D471/14 , A61K31/498 , D06P1/00
CPC分类号： C09B5/62 , C07D471/04
摘要： Disclosed are naphthalinamidinimide of formula (I), wherein R1, R2, R3, R4, R5 and R6 independently from each other are hydrogen; or C1-C37alkyl; wherein—one to 10 of the CH2 units of C1-C37alkyl independently from each may be substituted by carbonyl groups; oxygen atoms; sulphur atoms; selenium atoms; tellurium atoms; cis- or trans-CH═CH— groups; acetylenic C≡C— groups; 1,2-, 1,3- or 1,4-substituted phenyl radicals; 2,3-, 2,4-, 2,5-, 2,6-, 3,4- or 3,5-disubstituted pyridine radicals; 2,3-, 2,4-, 2,5- or 3,4-disubstituted thiophene radicals; 1,2-, 1,3-, 1,4-, 1,5-, 1,6-, 1,7-, 1,8-, 2,3-, 2,6- or 2,7-disubstituted 1,2-, 1,3-, 1,4-, 1,5-, 1,6-, 1,7-, 1,8-, 1,9-, 1,10-, 2,3-, 2,6-, 2,7-, 2,9-, 2,10- or 9,10-disubstituted anthracene radicals; wherein one or 2 CH— groups of the CH═CH— groups, the naphthalene radicals and the anthracene radicals may be substituted by nitrogen atoms; —up to 12 single hydrogen atoms of the CH2— groups independently from each other may be substituted at the same carbon atoms by fluorine; chlorine; bromine; or iodine; the cyano group; a linear alkyl chain with up to 18 carbon atoms; cis- or frans-CH═CH— groups; acetylenic C≡C— groups; 1,2-, 1,3- or 1,4-substituted phenyl radicals; 2,3-, 2,4-, 2,5-, 2,6-, 3,4- or 3,5-disubstituted pyridine radicals; 2,3-, 2,4-, 2,5- or 3,4-disubstituted thiophene radicals; 1,2-, 1,3-, 1,4-, 1,5-, 1,6-, 1,7-, 1,8-, 2,3-, 2,6- or 2,7-disubstituted naphthalene radicals; 1,2-, 1,3-, 1,4-, 1,5-, 1,6-, 1,7-, 1,8-, 1,9-, 1,10-, 2,3-, 2,6-, 2,7-, 2,9-, 2,10- or 9,10-disubstituted anthracene radicals; wherein up to 6 CH2— units in the alkyl chain independently from each other may be substituted by carbonyl groups, oxygen atoms, sulphur atoms, selenium atoms, tellurium atoms and up to 12 single hydrogen atoms of the CH2— groups of the alkyl radicals each independently from each other may also be substituted at the same C-atoms by fluorine, chlorine, bromine or iodine or cyano groups or linear alkyl chains with up to 18 carbon atoms, wherein one to 6 CH2-units independently from each other may be substituted by carbonyl groups, oxygen atoms, sulphur atoms, selenium atoms, tellurium atoms, cis- or frans-CH═CH— groups, wherein one CH-unit may also be substituted by a nitrogen atom, by acetylenic C≡C— groups, 1,2-, 1,3- or 1,4-substituted phenyl radicals, 2,3-, 2,4-, 2,5-, 2,6-, 3,4- or 3,5-disubstituted pyridine radicals, 2,3-, 2,4-, 2,5- or 3,4-disubstituted thiophene radicals, 1,2-, 1,3-, 1,4-, 1,5-, 1,6-, 1,7-, 1,8-, 2,3-, 2,6- or 2,7-disubstituierte naphthalene radicals, wherein one or two carbon atoms may be substituted by nitrogen atoms, by 1,2-, 1,3-, 1,4-, 1,5-, 1,6-, 1,7-, 1,8-, 1,9-, 1,10-, 2,3-, 2,6-, 2,7-, 2,9-, 2,10- or 9,10-di-substituierte anthracene radicals, wherein one or two carbon atoms may be substituted by nitrogen atoms; or instead of substituents the free valencies of the methine or quarternary carbon atoms may be linked pairwise forming rings like cyclohexane rings; or are an amino radical, if R1 C1 and R2 together with the carbon atoms C and C or R3 and R4 together with the carbon atoms C3 and C4 form a 6-membered radical; R7 and R8, independently from each other are =0; or ═NH—, if ═NH— together with the nitrogen atom N (for R6) or together with the nitrogen atom N (for R7) forms a five-membered radical. The compounds are useful for different purposes, preferably as UV absorbers for cosmetic applications.

5. 发明授权

US6156914A Donor-substituted oxindigo derivatives and their use as colorants 失效
标题翻译：供体取代的oxindigo衍生物及其作为着色剂的用途
公开(公告)号：US6156914A
公开(公告)日：2000-12-05
申请号：US155734
申请日：1998-10-05
申请人： Heinz Langhals , Barbara Wagner
发明人： Heinz Langhals , Barbara Wagner
IPC分类号： G03G9/09 , B41M5/00 , C07C215/76 , C07C217/84 , C09B7/00 , C07D307/02
CPC分类号： C09B7/00
摘要： Oxindigo derivative (1 and 2) in which four to seven of the radicals shown are hydrogen and one to four of these radicals are a radical chosen from the group consisting of a carbocyclic radical, a heterocyclic radical, halogen, C.sub.1 -C.sub.18 alkyl, --OR.sup.12, --CN, --NR.sup.10 R.sup.11, --COR.sup.9, --NR.sup.13 COR.sup.9, --NR.sup.12 COOR.sup.9, --NR.sup.12 CONR.sup.10 R.sup.11, --NHSO.sub.2 R.sup.9, --SO.sub.2 R.sup.9, --SOR.sup.9, --SO.sub.2 OR.sup.9, --CONR.sup.10 R.sup.11, --SO.sub.2 NR.sup.10 R.sup.11, --N.dbd.NR.sup.14, --OCOR.sup.9 and --OCONHR.sup.9, wherein two corresponding adjacent radicals can be combined to build up fused-on aromatic rings, in which R.sup.9 is C.sub.1 -C.sub.18 alkyl, C.sub.6 -C.sub.10 aryl, benzyl or a heterocyclic radical, R.sup.10 and R.sup.11 are hydrogen, C.sub.1 -C.sub.18 alkyl, C.sub.3 - to C.sub.24 cycloalkyl, C.sub.6 -C.sub.10 aryl or heteroaryl or in which R.sup.10 and R.sup.11, together with in each case one of the other radicals R.sub.2 to R.sub.4, form a ring, R.sup.12 is hydrogen, C.sub.1 -C.sub.18 alkyl, C.sub.3 - to C.sub.24 cycloalkyl, C.sub.6 -C.sub.10 aryl or a heteroaryl, R.sup.13 is hydrogen, C.sub.1 -C.sub.18 alkyl, C.sub.3 - to C.sub.24 cycloalkyl, C.sub.1 -C.sub.4 alkylaryl, C.sub.6 -C.sub.10 aryl or a heterocyclic radical and R.sup.14 is the radical of a coupling component or C.sub.6 -C.sub.10 aryl, and a process for their preparation, their use and intermediates.
摘要翻译： PCT No.PCT / EP97 / 01915 Sec。 371日期：1998年10月5日 102（e）日期1998年10月5日PCT 1996年4月25日PCT公布。出版物WO97 / 41176 日期：1997年11月6日靛蓝衍生物（1和2），其中4至7个所示的基团是氢，并且这些基团中的一个至四个是选自碳环基团，杂环基团，卤素，C 1 -C18烷基，-OR12，-CN，-NR10R11，-COR9，-NR13COR9，-NR12COOR9，-NR12CONR10R11，-NHSO2R9，-SO2R9，-SOR9，-SO2OR9，-CONR10R11，-SO2NR10R11，-N = NR14，-OCOR9和 -OCONHR9，其中可以组合两个相应的相邻基团以形成稠合的芳环，其中R9是C1-C18烷基，C6-C10芳基，苄基或杂环基，R10和R11是氢，C1-C18烷基，C3- C 12 -C 10芳基或杂芳基，或其中R 10和R 11连同其它基团R 2至R 4一起形成环，R 12为氢，C 1 -C 18烷基，C 3至C 24环烷基，C 6 -C 10芳基或杂芳基，R 13是氢，C 1 -C 18烷基，C 3至C 24环烷基，C 1 -C 4烷基芳基，C 6 -C 10芳基或杂环基，R 14是偶合基团的基团或C 6 -C 10芳基，以及它们的制备方法及其用途和中间体。

6. 发明授权

US6060601A Fluorescence-derivatisation of carbonyl compounds-novel carbonyl reagents 失效
标题翻译：羰基化合物的荧光衍生化 - 新型羰基试剂
公开(公告)号：US6060601A
公开(公告)日：2000-05-09
申请号：US121584
申请日：1998-07-23
申请人： Heinz Langhals , Wolfgang Jona
发明人： Heinz Langhals , Wolfgang Jona
IPC分类号： G01N21/78 , C07D471/06 , C09B3/18 , C09B5/62 , C09K11/06 , G01N30/88 , C07D211/18
CPC分类号： C09B5/62
摘要： Perylene hydrazide imides of the general formula I a process for the preparation thereof, the use thereof as detection reagents for carbonyl compounds, protonic acids, acylating agents and metal salts, and also perylene hydrazones II and bi- and tri-fluorophoric perylene bisimides III, the preparation thereof and methods of using them.
摘要翻译：通式I的苝酰肼是制备方法的方法，其作为羰基化合物，质子酸，酰化剂和金属盐的检测试剂的用途，以及苝腙II和双 - 和三氟苝二酰亚胺III，其制备方法和使用方法。

7. 发明授权

US4677079A Process for determining the composition of binary liquid mixture 失效
标题翻译：确定二元液体混合物组成的方法
公开(公告)号：US4677079A
公开(公告)日：1987-06-30
申请号：US496526
申请日：1983-05-24
申请人： Heinz Langhals
发明人： Heinz Langhals
IPC分类号： G01N31/16 , G01N33/00 , G01N33/18
CPC分类号： G01N31/16
摘要： The invention relates to a process for determining the composition of binary liquid mixtures. This process is characterized in that a solvatochromic compound is added to the sample to be analyzed, the solvatochromism band .lambda..sub.max is determined in the UV-spectrum, the E.sub.T -value (molar stimulation energy) of the solvatochromic substance is calculated and the concentration of the more polar component is determined in accordance with the following equationc.sub.P =c*exp(E.sub.T /E.sub.D -E.sub.T .degree./E.sub.D)-c* (1)in whichc.sub.P represents the concentration of the more polar component, the component having the greater E.sub.T 30-value being defined as the more polar component,E.sub.T represents the molar excitation energy of the solvatochromic compound,E.sub.T .degree. represents the E.sub.T -value of the pure, more apolar component,E.sub.T 30 is the E.sub.T -value using pyridinium phenol betaine andc* and E.sub.D are empirical parameters which may be taken from Tables or empirically determined.
摘要翻译：本发明涉及确定二元液体混合物的组成的方法。该方法的特征在于将溶剂化变色化合物加入到待分析的样品中，在UV光谱中测定溶剂化色素带λmax，计算溶剂化物色素的ET值（摩尔激发能），浓度根据以下等式cP = c * exp（ET / ED-ET DEG / ED）-c *（1）确定更极性的组分，其中cP表示极性较大的组分的浓度，该组分具有较大的 ET30值定义为极性较大的组分，ET表示溶剂化变色化合物的摩尔激发能，ET DEG表示纯的，非极性组分的ET值，ET30为使用吡啶酚苯酚甜菜碱和c * ED是经验参数，可参考表格或经验确定。

8. 发明申请

US20170210901A1 Automatic Sorting of Polymer Materials on the Basis of the Fluorescence Decay Time of the Intrinsic Fluorescence of the Polymer and of the Fluorescence of Marking Agents 审中-公开
公开(公告)号：US20170210901A1
公开(公告)日：2017-07-27
申请号：US15129408
申请日：2015-03-04
申请人： Heinz LANGHALS , Thorben SCHLÜCKER , Dominik ZGELA , Ludwig-maximillans-Universität München
发明人： Heinz Langhals , Thorben Schücke , Dominik Zegela
IPC分类号： C09B3/14 , C08J11/06 , B29B17/02 , B07C5/342 , G01N21/64 , C08K5/3437 , C09B5/62
CPC分类号： C09B3/14 , B07C5/342 , B29B17/02 , B29B2017/0203 , B29B2017/0279 , C08J11/06 , C08J2400/22 , C08J2400/30 , C08K5/3437 , C09B5/62 , G01N21/6408 , G01N2021/6439 , Y02W30/622
摘要： The invention relates to the identification of polymer materials on the basis of the fluorescence decay time of the intrinsic fluorescence of the polymer materials for definite sorting in a completely separated manner. The invention further relates to marking with fluorescent dyes, which, Because of the specific fluorescence decay times of the fluorescent dyes, can further increase the sorting reliability by means of redundancy and can be used to identify particular batches.

9. 发明申请

US20110079733A1 FLUORESCENT, HETEROCYCLICALLY FUSED PERYLENES 审中-公开
标题翻译：荧光素，杂环聚乙烯
公开(公告)号：US20110079733A1
公开(公告)日：2011-04-07
申请号：US12745900
申请日：2008-12-12
申请人： Heinz Langhals , Simon Kinzel , Andreas Obermeier
发明人： Heinz Langhals , Simon Kinzel , Andreas Obermeier
IPC分类号： G01N21/64 , C07D471/16 , C07D471/22
CPC分类号： C07D401/14
摘要： The reaction of aromatic nitriles with perylenetetracarboximides affords colorants which fluoresce strongly in the long-wave region and are of the formula in which one pair Q1 and Q2 or one pair Q2 and Q3, and optionally from 0 to 3 pairs Q3 and Q4, Q5 and Q6, Q6 and Q7 and/or Q7 and Q8, in each case in pairs, together form a heterocyclic ring the remaining Q1, Q4, Q5 and Q8 which do not form a heterocyclic ring are each hydrogen, and the remaining Q3, Q6 and Q7 which do not form a heterocyclic ring are each independently R5 or R6.R1 to R8 are each H, CN, halogen or optionally mono- or polysubstituted hydrocarbon groups.Establishing a suitable pH achieves a large Stokes shift in these colorants via the ESPT mechanism.
摘要翻译：芳香腈与苝四甲酰亚胺的反应提供了在长波区域强烈发荧光的着色剂，并且具有其中一对Q1和Q2或一对Q2和Q3以及任选地从0到3对Q3和Q4，Q5和 Q6，Q6和Q7和/或Q7和Q8在各种情况下成对组合形成杂环，剩下的不形成杂环的Q 1，Q 4，Q 5和Q 8各自为氢，剩余的Q3，Q6和不形成杂环的Q 7各自独立地为R 5或R 6。 R 1至R 8各自为H，CN，卤素或任选的单取代或多取代的烃基。建立合适的pH通过ESPT机制在这些着色剂中实现了大的斯托克斯转变。

10. 发明授权

US06335171B1 Immunochemical determination of substances contained on textile fibers or polymers 失效
标题翻译：纺织纤维或聚合物所含物质的免疫化学测定
公开(公告)号：US06335171B1
公开(公告)日：2002-01-01
申请号：US09329488
申请日：1999-06-10
申请人： Heinz Langhals , Rupert Brosius , Bertold Hock
发明人： Heinz Langhals , Rupert Brosius , Bertold Hock
IPC分类号： G01N3353
CPC分类号： G01N33/5308 , G01N33/36 , Y10S436/823
摘要： A method for the detection of substances contained on textile fibers or other natural or synthetic polymers is disclosed. The contained substances are identified with immunochemical methods, where the immunochemical reaction can occur on the fiber or polymer. The method is especially suitable for the determination of substances that can act as allergens.
摘要翻译：公开了用于检测纺织纤维或其它天然或合成聚合物上所含物质的方法。所含物质用免疫化学方法鉴定，其中免疫化学反应可发生在纤维或聚合物上。该方法特别适用于测定可作为过敏原的物质。

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