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1. 发明公开

US20240026171A1 Near-Infrared (NIR) transparent neutral black perylene solid solutions 审中-公开
公开(公告)号：US20240026171A1
公开(公告)日：2024-01-25
申请号：US18256559
申请日：2021-12-20
申请人： SUN CHEMICAL B.V.
发明人： Nikolay VINOKUROV , Paul Pascal ROQUETTE , Paul BROWN , Till VOGEL , Andres Carlos GARCIA ESPINO
IPC分类号： C09D7/41 , C09B67/22 , C09B3/18 , C09D5/33 , C09D5/00 , C09D5/36
CPC分类号： C09D7/41 , C09B67/0034 , C09B3/18 , C09D5/004 , C09D5/002 , C09D5/36
摘要： The present invention relates to a solid solution comprising (a) at least one compound according to formula (I) and (b) at least one compound according to formula (II), or at least one compound according to formula (III), or a mixture of at least one compound according to formula (II) and at least one compound according to formula (III) wherein R1 and R2 may, independently of one another, stand for —(CH2)n—X, wherein X stands for hydrogen, methyl, a C1-C5 alkoxyl, hydroxy, phenyl, C1-C5 alkylphenyl, C1-C5 alkoxyphenyl, hydroxyphenyl, halogenated phenyl, pyridyl, C1-C5 alkylpyridyl, C1-C5 alkoxypyridyl, halogenated pyridyl, pyridylvinyl or naphthyl; wherein n stands for 0, 1, 2, 3, 4 or 5; R3 and R4 may, independently of one another, stand for phenylene, C1-C5 alkylphenylene, C1-C5 alkoxyphenylene, hydroxyphenylene, halogenated phenylene, pyridinediyl, C1-C5 alkylpyridinediyl, C1-C5 alkoxy-pyridinediyl, halogenated pyridinediyl, anthraquinonediyl or naphthalenediyl, wherein the 2 nitrogen atoms bound to R4 according to formula (II) and (III) form a 5-membered or a 6-membered heterocycle with 2 atoms of an aromatic ring of R3; wherein the 2 nitrogen atoms bound to R4 according to formula (II) and (III) form a 5-membered or a 6-membered heterocycle with 2 atoms of an aromatic ring of R4; X1 to X8 may, independently from one another, stand for hydrogen, C1-C5 alkyl, C1-C5 alkoxy, hydroxy, phenyl or halide. The present invention further relates to a process for producing the solid solution. Furthermore, the present invention relates to a solid solution obtainable or obtained according to said process and to the use of the inventive solid solution, in particular as a NIR transparent black colorant in a NIR non-absorbing component.

2. 发明授权

US6039769A Process for the preparation of highly chromatic perylene pigments 有权
公开(公告)号：US6039769A
公开(公告)日：2000-03-21
申请号：US211728
申请日：1998-12-15
申请人： Gregory R. Schulz , Michael J. Greene
发明人： Gregory R. Schulz , Michael J. Greene
IPC分类号： C09B5/62 , C07D207/26 , C09B3/18 , C09B57/08 , C09B67/22 , C09B67/20
CPC分类号： C07D207/26 , C09B57/08 , C09B67/0034
摘要： This invention relates to a process for preparing perylene pigment compositions by reaction of(a) a perylene tetracarboxylic compound;(b) about 0.01 to about 20% by weight, relative to the perylene tetracarboxylic compound, of a non-pigmentary cyclic anhydride or imide of formula (I) ##STR1## wherein W is O or NR.sup.1 (where R.sup.1 is hydrogen, a metal, or optionally substituted alkyl, cycloalkyl, aralkyl, or aryl), R.sup.2, R.sup.3, and R.sup.4 are various combinations of substituents and/or fused-on rings, and the dotted line is an optional double bond representing R.sup.2 --C.dbd.C--R.sup.3 ;(c) ammonia or a primary alkyl, aralkyl, or aryl amine; optionally in the presence of(d) a solvent and/or(e) one or more dispersants.

3. 发明授权

US5981773A Preparation of perylene-3,4-dicarboxylic anhydrides 失效
标题翻译：苝-3,4-二羧酸酐的制备
公开(公告)号：US5981773A
公开(公告)日：1999-11-09
申请号：US7195
申请日：1998-01-14
申请人： Heinz Langhals , Petra Christa Von Unold , Markus Speckbacher
发明人： Heinz Langhals , Petra Christa Von Unold , Markus Speckbacher
IPC分类号： C07C51/38 , C07C63/44 , C07D221/18 , C07D311/78 , C09B3/18 , C09B5/62
CPC分类号： C09B5/62 , C07C51/38 , C07C63/44 , C07D221/18 , C09B3/18
摘要： A process for forming perylene-3, 4-dicarboxylic anhydrides by reacting a corresponding perylene-3,4:9, 10-tetracarboxylic dianhydride with a sterically hindered amine, as a base, at an elevated temperature.
摘要翻译：通过相应的苝-3,4：9,10-四羧酸二酐与空间位阻胺作为碱在高温下反应形成苝-3,4-二羧酸酐的方法。

4. 发明授权

US5948910A Water-soluble perylene dyestuffs, their preparation and their use 失效
标题翻译：水溶性苝染料，其制备及其用途
公开(公告)号：US5948910A
公开(公告)日：1999-09-07
申请号：US935098
申请日：1997-09-25
申请人： Wolfgang Bauer , Dieter Baumgart , Dieter Schnaitmann , Klaus-Peter Kreutzer , Walter Zoller
发明人： Wolfgang Bauer , Dieter Baumgart , Dieter Schnaitmann , Klaus-Peter Kreutzer , Walter Zoller
IPC分类号： C09B57/08 , C09B5/62 , C09D11/328 , D21H21/28 , C09B3/18 , C07D401/14
CPC分类号： C09D11/328 , C09B5/62 , D21H21/28
摘要： Water-soluble perylene dyestuffs, their preparation and their useThe present Application relates to water-soluble perylene dyestuffs of the formula ##STR1## in which R.sup.1 and R.sup.2 independently of one another are the radicals A--X--COOM or A--X--SO.sub.3 M;R.sup.3 and R.sup.4 independently of one another are the radicals R.sup.1 or R.sup.2, or are OR.sup.5 or NR.sup.6 R.sup.7 ;A is NR.sup.8 or S;X is a straight-chain or branched alkylene radical, a straight-chain or branched alkylene radical which is substituted by hydroxyl, carboxyl or amino, an arylene radical or an arylene radical which is optionally substituted by hydroxyl, carboxyl or sulfo;R.sup.5, R.sup.6 and R.sup.7 independently of one another are hydrogen, (C.sub.1 -C.sub.4)-alkyl or (C.sub.1 -C.sub.4)-alkyl which is substitituted by one or more hydroxyl, 2-hydroxyethoxy, (C.sub.1 -C.sub.4)-alkoxy or amino groups;R.sup.8 is hydrogen, methyl or ethyl andM is a monovalent cation or one equivalent of a polyvalent cation,processes for their preparation, their use for dyeing and printing naturally occurring and synthetic fiber materials, and recording liquids, in particular for the ink-jet process, and liquid formulations for dyeing paper in the pulp which comprise the dyestuffs according to the invention.
摘要翻译：水溶性苝染料及其制备及其用途本申请涉及下式的水溶性苝染料，其中R1和R2彼此独立地为基团A-X-COOM或A-X-SO3M; R 3和R 4彼此独立地是基团R 1或R 2，或者是OR 5或NR 6 R 7; A是NR8或S; X是直链或支链亚烷基，被羟基，羧基或氨基取代的直链或支链亚烷基，任选被羟基，羧基或磺基取代的亚芳基或亚芳基; R5，R6和R7彼此独立地是氢，（C1-C4） - 烷基或被一个或多个羟基，2-羟基乙氧基，（C1-C4） - 烷氧基或氨基取代的（C1-C4） - 烷基 ; R8是氢，甲基或乙基，M是一价阳离子或一当量的多价阳离子，其制备方法，它们用于染色和印刷天然存在的和合成的纤维材料，以及记录液体，特别是用于喷墨工艺和用于在包含根据本发明的染料的纸浆中染色纸的液体制剂。

5. 发明授权

US09199928B2 Fluorescent dye for pH sensor 有权
标题翻译：荧光染料用于pH传感器
公开(公告)号：US09199928B2
公开(公告)日：2015-12-01
申请号：US14115191
申请日：2012-03-28
申请人： Daniel Riechers , Eberhard Wuenn
发明人： Daniel Riechers , Eberhard Wuenn
IPC分类号： G01N31/16 , C07C311/29 , C09K11/06 , G01N21/64 , G01N21/80 , C09B3/18
CPC分类号： C07C311/29 , C07C2603/50 , C09B3/18 , C09K11/06 , C09K2211/1011 , G01N21/6428 , G01N21/643 , G01N21/80
摘要： The present invention relates to a new type of fluorescent with the following formula (I), its preparation process, and also an optical pH sensor which comprises this fluorescent dye immobilized on an analyte-permeable carrier.
摘要翻译：本发明涉及具有下式（I）的新型荧光剂及其制备方法，以及包含固定在分析物可渗透载体上的该荧光染料的光学pH传感器。

6. 发明申请

US20050001202A1 Perylenetetracarboxylic acid dibenzimidazole sulfoderivatives containing oxo-groups in the perylene core which form part of a para-quinoid system of bonds, lyotropic liquid crystal systems and anisotropic films containing the same, and methods for making the same 有权
标题翻译：苝四羧酸二苯并咪唑磺化衍生物在苝核心中形成一部分对醌类系统的键合，溶致液晶体系和含有它们的各向异性膜及其制备方法
公开(公告)号：US20050001202A1
公开(公告)日：2005-01-06
申请号：US10833595
申请日：2004-04-27
申请人： Elena Sidorenko , Victor Nazarov
发明人： Elena Sidorenko , Victor Nazarov
IPC分类号： C07D471/22 , C07D491/22 , C07D495/22 , C09B3/18 , C09K19/34 , G02F1/1335 , C07D471/14 , C09K19/02
CPC分类号： C09K19/60 , C07D471/22 , C07D491/22 , C07D495/22 , C09B3/18 , C09K19/348 , C09K19/606 , Y10T428/10
摘要： Anisotropic films based on sulfoderivatives of perylenetetracarboxylic acid dibenzimidazole (PTCA DBI) which contain oxo groups pendant to a perylene core. The oxo-groups, in combination with portions of the perylene core, form a quinoid system of bonds. The oxo substituted PTCA DBI sulfoderivatives form liquid crystal systems possessing high optical properties. Said liquid crystal systems can be applied onto various substrates to obtain optically isotropic or anisotropic, at least partially crystalline, films applicable in various fields.
摘要翻译：基于苝四羧酸二苯并咪唑（PTCA DBI）的磺化衍生物的各向异性膜，其含有垂饰于苝核心的氧代基团。氧代基团与苝核心部分组合形成键式的醌型体系。氧代取代的PTCA DBI磺基衍生物形成具有高光学性质的液晶体系。所述液晶体系可以应用到各种基底上，以获得适用于各种领域的光学各向同性或各向异性的至少部分结晶的膜。

7. 发明授权

US5756744A Unsymmetrical perylene dimers 失效
标题翻译：不对称苝二聚体
公开(公告)号：US5756744A
公开(公告)日：1998-05-26
申请号：US902458
申请日：1997-07-29
申请人： James M. Duff , C. Geoffrey Allen , Ah-Mee Hor , Gordon K. Hamer
发明人： James M. Duff , C. Geoffrey Allen , Ah-Mee Hor , Gordon K. Hamer
IPC分类号： C07D471/00 , C07D519/00 , C09B3/18 , G03G5/06 , C07D471/02 , C07D471/06
CPC分类号： C07D519/00 , C09B5/62 , G03G5/0659 , G03G5/0661
摘要： Photoconductive imaging members comprised of unsymmetrical dimeric perylene as a charge generator, wherein said perylene is of the following formula ##STR1## wherein R is hydrogen, alkyl, cycloalkyl, substituted alkyl, aryl, substituted aryl, aralkyl or substituted aralkyl group, and X--Y is an unsymmetrical bridging moiety of alkylene, substituted alkylene, arylene, substituted arylene, aralkylene or substituted aralkylene.
摘要翻译：由不对称的二聚苝作为电荷产生剂组成的光导成像构件，其中所述苝具有下列通式1，取代的烷基，芳基，取代的芳基，芳烷基或取代的芳烷基，XY是亚烷基的取代的亚烷基，亚芳基，取代的亚芳基，亚芳基或取代的亚芳基。

8. 发明授权

US4618694A Perylene compounds 失效
标题翻译：苝化合物
公开(公告)号：US4618694A
公开(公告)日：1986-10-21
申请号：US690524
申请日：1985-01-11
申请人： Rudiger Iden , Gunther Seybold
发明人： Rudiger Iden , Gunther Seybold
IPC分类号： C08K5/00 , C07C67/00 , C07C253/00 , C07C255/57 , C08J5/18 , C08K5/16 , C08L33/00 , C08L33/02 , C08L77/00 , C08L101/00 , C09B3/14 , C09B3/18 , G02F1/35 , G02F1/355 , G02F1/361 , H01L31/055 , C07C121/64
CPC分类号： C09B3/18 , H01L31/055 , Y02E10/52
摘要： The present invention relates to a method for concentrating light by means of fluorescent compounds in plastic sheets or films, wherein perylene compounds are used for this purpose.
摘要翻译：本发明涉及一种通过荧光化合物在塑料片或薄膜中浓缩光的方法，其中苝化合物用于此目的。

9. 发明授权

US4217455A Preparation of transparent and easily dispersible perylene-3,4,9,10-tetracarboxylic acid diimide pigments of high tinctorial strength 失效
标题翻译：具有高着色强度的透明易分散的苝-3,4,9,10-四羧酸二酰亚胺颜料的制备
公开(公告)号：US4217455A
公开(公告)日：1980-08-12
申请号：US3980
申请日：1979-01-16
申请人： Helmut Hoch , Heinrich Hiller
发明人： Helmut Hoch , Heinrich Hiller
IPC分类号： C09B5/62 , C09B67/20 , C09B67/28 , C09B3/18 , C07D471/06 , C09B67/00
CPC分类号： C09B5/62 , C09B67/0077
摘要： A process for the preparation of transparent pigmentary forms, of high tinctorial strength, of perylene-3,4,9,10-tetracarboxylic acid bis-p-phenetidide and bis-p-chloroanilide, in which the diimide concerned is converted to the leuco compound, and the latter, with or without prior isolation, is then oxidized in aqueous suspension in the presence of surfactants or while exposed to shearing forces in the presence or absence of surfactants, after which the pigment is isolated.The pigments give highly transparent very pure colorations when used unreduced, while in white reductions they give very deep colorations with substantially more yellowish hues than those given by the prior art pigments.
摘要翻译：制备高着色强度的苝-3,4,9,10-四羧酸双对苯乙二胺和双对氯苯胺的透明颜料形式的方法，其中将所述二酰亚胺转化为无色化合物，然后在有或者没有预先分离的情况下，在表面活性剂的存在下，或者在存在或不存在表面活性剂时暴露于剪切力，然后在水性悬浮液中氧化，之后分离颜料。当使用未还原时，颜料赋予高度透明的非常纯的着色，而在白色减少中，它们给出非常深的着色，其色调比现有技术颜料给出的色泽显着更淡黄色。

10. 发明授权

US3872103A Manufacture of deep-shade 3,4,9,10-perylenetetracarboxylic acid dianhydride pigments 失效
标题翻译：深层沙粒的制备3,4,9,10-戊二酸二羧酸二水合物
公开(公告)号：US3872103A
公开(公告)日：1975-03-18
申请号：US40909173
申请日：1973-10-24
申请人： BASF AG
发明人： FABIAN WOLFGANG
IPC分类号： C09B5/62 , C09B3/18 , C09B67/00 , C09B67/20 , C07D9/00
CPC分类号： C09B68/24 , C09B3/18 , C09B67/00 , C09B68/443
摘要： A process for the manufacture of deep-shade perylene-3,4,9,10tetracarboxylic acid dianhydride pigments, wherein finely ground crude pigment of which the average primary particle size is from 0.01 to 1 Mu is treated with a primary or tertiary aromatic amine which is liquid at the treatment temperature, or with a strongly polar aprotic solvent, as swelling agent, until the pigment has acquired the optimum color strength. After removal of the swelling agent, a deep-shade, pure pigment is obtained, which is suitable for all pigmentation purposes.
摘要翻译：用于制造深色苝-3,4,9,10-四羧酸二酐颜料的方法，其中平均一次粒径为0.01-1μm的精细研磨的粗颜料用伯或叔芳族化合物胺，在处理温度下为液体，或用强极性非质子溶剂作为溶胀剂，直到颜料获得最佳色强度。除去溶胀剂后，得到深色，纯色素，适用于所有的色素沉淀。

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