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1. 发明授权

US4769493A Process for producing tetrafluorophthalic acid 失效
标题翻译：制备四氟邻苯二甲酸的方法
公开(公告)号：US4769493A
公开(公告)日：1988-09-06
申请号：US85498
申请日：1987-08-14
申请人： Haruaki Ito , Utaro Matsushita , Toshiaki Shimizu , Nobuo Ishikawa , Masaaki Shimizu
发明人： Haruaki Ito , Utaro Matsushita , Toshiaki Shimizu , Nobuo Ishikawa , Masaaki Shimizu
IPC分类号： C07C51/00 , C07D209/48
CPC分类号： C07D209/48 , C07C51/00
摘要： A process for producing tetrafluorophthalic acid is disclosed, which comprises the steps of:(a) reacting an alkali metal fluoride and at least one imide compound represented by formula (I) or (II) ##STR1## wherein X.sup.1, X.sup.2, X.sup.3, and X.sup.4, which may be the same or different, each represents a chloride atom or a bromine atom, R.sup.1 represents a monovalent organic group, and R.sup.2 represents a divalent organic group, to provide an N-substituted tetrafluorophthalimide; and(b) hydrolyzing the tetrafluorophthalimide in the presence of an acid.
摘要翻译：公开了一种制备四氟邻苯二甲酸的方法，其包括以下步骤：（a）使碱金属氟化物与至少一种由式（I）或（II）表示的酰亚胺化合物（I））其中X1，X2，X3和X4可以相同或不同，各自表示氯原子或溴原子，R1表示一价有机基团，R2表示二价有机基团，以提供N-取代的四氟邻苯二甲酰亚胺; 和（b）在酸存在下水解四氟邻苯二甲酰亚胺。

2. 发明授权

US4542238A Optically active substance 失效
标题翻译：光学活性物质
公开(公告)号：US4542238A
公开(公告)日：1985-09-17
申请号：US665501
申请日：1984-10-29
申请人： Nobuo Ishikawa
发明人： Nobuo Ishikawa
IPC分类号： B01J27/00 , C07B61/00 , C07C51/00 , C07C59/135 , C07C67/00 , C07C59/00
CPC分类号： C07C59/135
摘要： An optically active substance consisting of perfluoro-2-alkoxy carboxylic acid or its derivative represented by the following general formula: ##STR1## where R.sub.f and R.sub.f ' are the same or different perfluoroaliphatic groups, X is a halogen or hydroxyl group, and C is a chiral carbon atom, the above carboxylic acid or its derivative being useful for an analytical reagent for optically active compounds, such as a chiral derivatizing agent for the .sup.19 F NMR or gas chromatographic analysis.
摘要翻译：由以下通式表示的全氟-2-烷氧基羧酸或其衍生物组成的光学活性物质：其中Rf和Rf'是相同或不同的全氟脂肪族基团，X是卤素或羟基，C是手性碳原子，上述羧酸或其衍生物可用于光学活性化合物的分析试剂，例如用于19F NMR或气相色谱分析的手性衍生化试剂。

3. 发明授权

US4532020A Process for preparing a .beta.-(fluoroalkyl or fluoroalkenyl)-.beta.-hydroxyalkyne 失效
标题翻译：制备β-（氟烷基或氟烯基）-β-羟基亚氨基的方法
公开(公告)号：US4532020A
公开(公告)日：1985-07-30
申请号：US586943
申请日：1984-03-07
申请人： Nobuo Ishikawa , Tomoya Kitazume
发明人： Nobuo Ishikawa , Tomoya Kitazume
IPC分类号： C07C29/44 , C07C33/42 , C07C33/48 , B01J19/10
CPC分类号： C07C29/44 , C07C33/42 , C07C33/426 , C07C33/483 , C07B2200/09
摘要： A process for preparing a .beta.-(fluoroalkyl or fluoroalkenyl)-.beta.-hydroxyalkyne represented by the formula ##STR1## wherein R.sub.f represents a fluoroalkyl or fluoroalkenyl group and R represents an aliphatic or aromatic group, comprising reacting an alkyne represented by the formulaR--C.tbd.CH (II)wherein R is the same as defined above with a fluorine containing aldehyde represented by the formulaR.sub.f CHO (III)wherein R.sub.f is the same as defined above in the presence of catalyst under ultrasonic irradiation.A process for preparing an .alpha.-(fluoroalkyl or fluoroalkenyl)allyl alcohol represented by the formula ##STR2## wherein R.sub.f represents a fluoroalkyl or fluoroalkenyl group, R represents an aliphatic or aromatic group and R' represents a hydrogen atom or an aliphatic group, comprising (1) reacting a .beta.-(fluoroalkyl or fluoroalkenyl)-.beta.-hydroxyalkyne represented by the formula ##STR3## wherein R.sub.f and R are respectively the same as defined above with a isobutylmagnesium halide represented by the formulai--C.sub.4 H.sub.9 MgXwherein X represents a halogen atom, and (2) reacting the reaction mixture thus obtained above with a halide represented by the formulaR'X'wherein X' represents a halogen atom and R' is the same as defined above.
摘要翻译：一种制备由式（I）表示的β-（氟代烷基或氟烯基）-β-羟基亚油酸的方法，其中Rf代表氟烷基或氟烯基，R代表脂族或芳族基团，包括使由其中R与上述定义相同的式RC 3BOND CH（II）与式RfCHO（III）表示的含氟醛反应其中Rf在超声波照射下在催化剂存在下与上述定义相同。由式（IV）表示的α-（氟代烷基或氟烯基）烯丙醇的制备方法，其中Rf代表氟代烷基或氟代烯基，R代表脂族或芳基，R'代表氢原子或脂族基团，其包含（1）使式（I）表示的β-（氟代烷基或氟代烯基）-β-羟基亚氨基酯反应，其中Rf和R分别与上述定义相同，用式i- C4H9MgX其中X表示卤素原子，和（2）使由上述得到的反应混合物与式R'X'表示的卤化物反应，其中X'表示卤素原子，R'与上述定义相同。

4. 发明授权

US4614742A Fluorinated isophthalonitrile compound and nonmedical fungicide containing the same 失效
标题翻译：氟化间苯二腈化合物和含有相同的非医药杀真菌剂
公开(公告)号：US4614742A
公开(公告)日：1986-09-30
申请号：US770481
申请日：1985-08-29
申请人： Nobuo Ishikawa , Akio Takaoka , Takashi Isono , Masatoshi Motoyoshi , Kazuhiro Kojima
发明人： Nobuo Ishikawa , Akio Takaoka , Takashi Isono , Masatoshi Motoyoshi , Kazuhiro Kojima
IPC分类号： A01N37/40 , A01N37/44 , A01N39/00 , A01N43/08 , A01N43/48 , A01N43/50 , A01N43/52 , A01N43/54 , A01N43/653 , C07C255/53 , C07C255/58 , C07D235/30 , C07D239/46 , C07D239/54 , C07D239/553 , C07D249/14 , C07D307/12 , C07D521/00 , A01N43/84 , A01N37/34 , C07C121/78
CPC分类号： C07D239/47 , A01N37/40 , A01N37/44 , A01N39/00 , A01N43/08 , A01N43/50 , A01N43/52 , A01N43/54 , A01N43/653 , C07C255/00 , C07C323/00 , C07D231/12 , C07D233/56 , C07D235/30 , C07D239/553 , C07D249/08 , C07D249/14 , C07D307/12
摘要： A fluorinated isophthalonitrile compound having the general formula ##STR1## wherein Y is --O, --S, or --N(R'), R and R' are independently hydrogen, an alkyl group, an alkyl group, an alkynyl group, a haloalkyl group, an alkoxyl group, alkoxyalkyl group, a phenyl group which may be substituted, a tetrahydrofurfuryl group, or a cycloalkyl group, provided that, in the case of Y=--N(R'), R and R' or Y may be a tetrahydrofurfuryl group, or a cycloalkyl group, a heterocyclic compound residue.This fluorinated isophthalonitrile compound is suitable for use as an agricultural fungicide.
摘要翻译：具有通式为其中Y为-O，-S或-N（R'）的通式（I）的氟化间苯二腈化合物，R和R'独立地为氢，烷基，烷基，炔基卤代烷基，烷氧基，烷氧基烷基，可被取代的苯基，四氢糠基或环烷基，条件是在Y = -N（R'），R和R'或 Y可以是四氢糠基，或环烷基，杂环化合物残基。该氟化的间苯二腈化合物适合用作农业杀真菌剂。

5. 发明授权

US4578503A Alkylated or alkenylated malonic acid or its derivatives having a fluorine 失效
标题翻译：烷基化或链烯基化的丙二酸或其具有氟的衍生物
公开(公告)号：US4578503A
公开(公告)日：1986-03-25
申请号：US528134
申请日：1983-08-31
申请人： Nobuo Ishikawa , Takeshi Nakai , Yoshio Inouye
发明人： Nobuo Ishikawa , Takeshi Nakai , Yoshio Inouye
IPC分类号： C07C69/65 , C07C69/716 , C07C67/317 , C07C57/36 , C07C69/612
CPC分类号： C07C69/65 , C07C69/716
摘要： An alkylated or alkenylated malonic ester having a fluorine containing aliphatic substituent and derivatives thereof as expressed by the following general formula: ##STR1## where R.sub.f is a fluorine containing aliphatic group, R is an aliphatic group, or hydrogen or alkali metal atom, and R' is an unsubstituted or substituted aliphatic group.And a method to trap the enolate ion of a malonic ester having a fluorine containing aliphatic substituent as expressed by the following general formula,R.sub.f CH(CO.sub.2 R).sub.2where R.sub.f is a fluorine containing aliphatic group and R is an aliphatic group, hydrogen or alkali metal atom, wherein said malonic ester is converted under the action of a weaker base and/or fluoride ion to a fluorine containing enolate ion to be trapped as expressed by the following general formula:R.sub.f C.sup..crclbar. (CO.sub.2 R).sub.2where R.sub.f and R are the same as above.
摘要翻译：具有含氟脂肪族取代基的烷基化或链烯基化丙二酸酯及其衍生物，由以下通式表示：其中Rf是含氟脂族基团，R是脂族基团或氢或碱金属原子，R '是未取代或取代的脂族基团。和捕获具有含氟脂肪族取代基的丙二酸酯的烯醇化物离子的方法，其由以下通式表示：RfCH（CO2R）2，其中Rf是含氟脂族基团，R是脂族基团，氢或碱金属原子，其中所述丙二酸酯在较弱碱和/或氟离子的作用下转化为要被捕获的含氟烯醇化物离子，如以下通式表示：RfC（ - ）（CO 2 R）2，其中Rf和R为与上述相同。

6. 发明授权

US4558148A Fluorinated allylic compounds and a process for preparing these compounds 失效
标题翻译：氟化烯丙基化合物和制备这些化合物的方法
公开(公告)号：US4558148A
公开(公告)日：1985-12-10
申请号：US635682
申请日：1984-07-30
申请人： Nobuo Ishikawa , Tomoya Kitazume
发明人： Nobuo Ishikawa , Tomoya Kitazume
IPC分类号： C07C29/40 , C07C33/42 , C07C33/48 , C07F7/08 , C07F7/18 , C07C33/46
CPC分类号： C07F7/0818 , C07C29/40 , C07C33/423 , C07C33/483
摘要： There are described fluorinated allylic compounds as expressed by the following general formula ##STR1## wherein R.sub.f is a fluorinated aliphatic group and R is a group expressed by a general formula ##STR2## wherein R.sup.1 is an aliphatic or aromatic hydrocarbon group and R.sup.2 and R.sup.3 are the same group or different groups as selected among hydrogen atom, aliphatic and aromatic hydrocarbon groups, and heterocyclic groups. Further, a process of preparing fluorinated allylic compounds is described which includes a process step wherein a silane metal halide as expressed by a general formula(R.sup.1).sub.3 SiCH.sub.2 MX,wherein R.sup.1 is either an aliphatic or aromatic hydrocarbon group, M is an element that belongs to the group IIa, IIIb, or VIIb of the periodic table, and X is a halogen atom, is reacted with a fluorinated carboxylic acid ester as expressed by a general formulaR.sub.f COOR',wherein R.sub.f is a fluorinated aliphatic group and R' is either an aliphatic or aromatic hydrocarbon group, to form a fluorinated carbinol as expressed by a general formula ##STR3## wherein R.sup.1 and R.sub.f are as defined above, and further a molecule of (R.sup.1).sub.3 SiOH, where R.sup.1 is as defined above, is eliminated from this carbinol to produce a fluorinated allylsilane as expressed by a general formula ##STR4## wherein R.sup.1 and R.sub.f are as defined above.
摘要翻译：描述了由以下通式表示的氟化烯丙基化合物，其中Rf是氟化脂族基团，R是由通式表示的基团，其中R 1是脂族或芳族烃基，R 2和R 3是相同的基团或选自氢原子，脂族和芳族烃基和杂环基中的不同基团。此外，描述了制备氟化烯丙基化合物的方法，其包括其中由通式（R1）3SiCH2MX表示的硅烷金属卤化物，其中R 1是脂族或芳族烃基，M是属于元素周期表IIa，IIIb或VIIb族，X为卤原子，与通式RfCOOR'表示的含氟羧酸酯反应，其中Rf为氟化脂族基，R'为脂肪族或芳香族烃基，以形成通式（Ⅰa）所表示的氟化甲醇，其中R 1和R f如上所定义，并且另外分子式（R 1）3 SiOH（其中R 1如上定义）从该甲醇以产生由通式“IMAGE”表示的氟化烯丙基硅烷，其中R 1和R f如上所定义。

7. 发明授权

US4482729A Fluoroalkyl silyl ketene acetals and a process for preparing the same 失效
标题翻译：氟烷基甲硅烷基乙烯酮缩醛及其制备方法
公开(公告)号：US4482729A
公开(公告)日：1984-11-13
申请号：US586947
申请日：1984-03-04
申请人： Nobuo Ishikawa , Takeshi Nakai
发明人： Nobuo Ishikawa , Takeshi Nakai
IPC分类号： C07F7/18 , C07F7/08
CPC分类号： C07F7/1852
摘要： A fluoroalkyl silyl ketene acetal of the formula ##STR1## wherein R.sub.f is a fluoroalkyl group, and R and R' are the same or different and each is an alkyl group, which is prepared by reacting or fluorinated carboxylic acid of the formulaR.sub.f CH.sub.2 COOR'wherein R.sub.f and R' are respectively the same as defined above with a silylating agent represented by a formulaR.sub.3 SiOTfwherein Tf represents a trifluoromethane sulfonyl group and R is the same as defined above.
摘要翻译：其中R f是氟烷基，R和R'相同或不同，并且各自是烷基，其通过使式RfCH 2 COOR'或氟化的氟化反应制备，其中式 Rf和R'分别与上述通式R3SiOTf表示的甲硅烷基化剂相同，其中Tf表示三氟甲磺酰基，R与上述定义相同。

8. 发明授权

US4873677A Charging apparatus for an electronic device 失效
标题翻译：电子设备用充电装置
公开(公告)号：US4873677A
公开(公告)日：1989-10-10
申请号：US216914
申请日：1988-07-07
申请人： Kenji Sakamoto , Nobuo Ishikawa , Motomu Hayakawa
发明人： Kenji Sakamoto , Nobuo Ishikawa , Motomu Hayakawa
IPC分类号： G04C10/00 , H02J7/02
CPC分类号： H02J7/025 , G04C10/00 , H01F38/14
摘要： An apparatus for charging a power storage device provided within an electronic device. A power source provides direct current which is alternated in direction through a pair of primary coils for inducing alternating current in a secondary coil of the electronic device. The pair of primary coils are fixed to a coil yoke all of which are supported within a casing of the apparatus. During charging of the power storage device, the electronic device is mounted to the outside surface of the casing whereby substantially all of the magnetic flux of the magnetic field produced by the pair of primary coils flows through the secondary coil and coil yoke. The frequency of the oscillating signal is preset to provide the maximum induced current which will not adversely affect the movement of the analog mechanisms within the electronic device.

9. 发明授权

US4864442A Magnetic read/write apparatus 失效
标题翻译：磁读/写装置
公开(公告)号：US4864442A
公开(公告)日：1989-09-05
申请号：US92912
申请日：1987-08-20
申请人： Osamu Miyazawa , Nobuo Ishikawa , Mamoru Miyasaka , Kenichi Hirota
发明人： Osamu Miyazawa , Nobuo Ishikawa , Mamoru Miyasaka , Kenichi Hirota
IPC分类号： G11B5/48 , G11B17/03 , G11B17/32 , G11B19/20 , G11B23/00 , G11B23/50
CPC分类号： G11B23/505 , G11B17/03 , G11B17/32 , G11B19/2009 , G11B23/0035 , G11B5/4806
摘要： In magnetic read/write apparatus having a media hub (2) made of magnetic material provided with a magnetic disk (1) and a package so as to cover the magnetic disk with a shell, to position the media hub (2) in the axial direction is performed by attaching an end of a spindle hub (17) to a media hub (2), and to position the media hub in the radial direction is performed by attaching the inner side of a center core (4) integrally formed with the media hub (2) to the periphery of the spindle hub (17). Furthermore, a driving pin (21) for contacting the media hub (2) with the spindle hub (17) is provided at the end of the media hub (2) and in the inner side of the center core (4), thereby, making it possible to provide a small-sized spindle hub and an excellent head contact.

10. 发明授权

US4741960A Magnetic recording medium having a back coat layer containing a specific type of lubricant 失效
标题翻译：具有含特定类型润滑剂的背涂层的磁记录介质
公开(公告)号：US4741960A
公开(公告)日：1988-05-03
申请号：US10957
申请日：1987-02-02
申请人： Hitoshi Takita , Nobuo Ishikawa , Shigeru Nakano
发明人： Hitoshi Takita , Nobuo Ishikawa , Shigeru Nakano
IPC分类号： G11B5/708 , C09D101/18 , C09D175/04 , C10M105/76 , C10N40/18 , G11B5/71 , G11B5/735 , G11B5/70
CPC分类号： G11B5/735 , Y10S428/90 , Y10T428/265 , Y10T428/31609 , Y10T428/31663 , Y10T428/31786
摘要： A magnetic recording medium comprising a back coat layer formed on a non-magnetic support on one side which is opposite to a side where a magnetic recording layer is formed. The back coat layer is made of a dispersion of a fluorine-modified organosiloxane in a binder resin. The organosiloxane is of the following formula ##STR1## in which R.sub.1 represents a saturated or unsaturated monohydrocarbon group having from 7 to 21 carbon atoms, R.sub.2 represents a saturated monohydrocarbon group having from 1 to 4 carbon atoms, k is an integer of from 1 to 12, l is an integer of from 2 to 6, m is an integer of 1 or 2, n is an integer of 1 or 2 provided that m+n.ltoreq.3.
摘要翻译：一种磁记录介质，包括在与形成磁记录层的一侧相对的一侧上的非磁性载体上形成的背涂层。背涂层由粘合剂树脂中的氟改性有机硅氧烷的分散体构成。有机硅氧烷具有下式（A），其中R 1表示具有7至21个碳原子的饱和或不饱和单烃基，R 2表示具有1至4个碳原子的饱和单烃基，k是 1至12，l是2至6的整数，m是1或2的整数，n是1或2的整数，条件是m + n <3。

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