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1. 发明授权

US09714172B2 Preparation of polymeric resins and carbon materials 有权
公开(公告)号：US09714172B2
公开(公告)日：2017-07-25
申请号：US14647322
申请日：2013-11-26
申请人： Georgia-Pacific Chemicals LLC , Energ2 Technologies, Inc.
发明人： Katharine Geramita , Benjamin E. Kron , Henry R. Costantino , Aaron M. Feaver , Avery Sakshaug , Leah A. Thompkins , Alan Tzu-Yang Chang , Xing Dong , Shahid P. Qureshi , John B. Hines , Gerald A. Knazek , Joseph Frank Ludvik
IPC分类号： C01B31/02 , C01B31/08 , H01M4/583 , H01G11/34 , H01G11/38 , H01G11/04 , B01J6/00 , C01B31/00 , H01M4/587 , H01M4/96
CPC分类号： C01B32/30 , B01J6/00 , C01B32/00 , C01B32/05 , C01B32/312 , C01P2004/51 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/17 , H01G11/04 , H01G11/32 , H01G11/34 , H01G11/38 , H01G11/84 , H01M4/583 , H01M4/587 , H01M4/96
摘要： Methods for making carbon materials are provided. In at least one specific embodiment, the method can include combining one or more polymer precursors with one or more liquids to produce a mixture. The mixture can be an emulsion, dispersion, or a suspension. The liquid can include hexane, pentane, cyclopentane, benzene, toluene, o-xylene, m-xylene, p-xylene, diethyl ether, ethylmethylketone, dichloromethane, tetrahydrofuran, mineral oils, paraffin oils, vegetable derived oils, or any mixture thereof. The method can also include aging the mixture at a temperature and time sufficient for the polymer precursor to react and form polymer gel particles having a volume average particle size (Dv,50) of the polymer particles in gel form greater than or equal to 1 mm. The method can also include heating the polymer gel particles to produce a carbon material.

2. 发明申请

US20140148560A1 PREPARATION OF PHENOL-FORMALDEHYDE RESIN BEADS USING SUSPENSION OR EMULSION POLYMERIZATION 有权
标题翻译：使用悬浮或乳液聚合制备酚醛树脂珠粒
公开(公告)号：US20140148560A1
公开(公告)日：2014-05-29
申请号：US14092267
申请日：2013-11-27
申请人： Georgia-Pacific Chemicals LLC
发明人： Shahid P. Qureshi , Xing Dong , Charles C. Chan , Joseph Frank Ludvik
IPC分类号： C08G8/32
CPC分类号： C08G8/32 , C08G8/10 , C08G8/22 , C08G85/004 , C08J9/16 , C08J9/28 , C08J2201/026 , C08J2201/0482 , C08J2201/0502 , C08J2205/02 , C08J2361/06
摘要： Methods for making polymer particles in gel form via an emulsion and/or suspension polymerization are provided. In at least one specific embodiment, the method can include reacting a first reaction mixture comprising a phenolic monomer, an aldehyde monomer, and a first catalyst to produce a prepolymer. The method can also include combining the prepolymer with a carrier fluid and a second catalyst to produce a second reaction mixture. The second catalyst can include a dicarboxylic acid, an anhydride, a dihydroxybenzene, or any mixture thereof. The method can also include polymerizing the prepolymer to form polymer particles in gel form.
摘要翻译：提供了通过乳液和/或悬浮聚合制备凝胶形式的聚合物颗粒的方法。在至少一个具体实施方案中，该方法可以包括使包含酚单体，醛单体和第一催化剂的第一反应混合物反应以产生预聚物。该方法还可以包括将预聚物与载体流体和第二催化剂组合以产生第二反应混合物。第二催化剂可以包括二羧酸，酸酐，二羟基苯或其任何混合物。该方法还可包括聚合预聚物以形成凝胶形式的聚合物颗粒。

3. 发明申请

US20130211005A1 METHODS FOR MAKING POLYMER PARTICULATES IN GEL FORM 审中-公开
标题翻译：在凝胶形式中制备聚合物颗粒的方法
公开(公告)号：US20130211005A1
公开(公告)日：2013-08-15
申请号：US13763561
申请日：2013-02-08
申请人： Georgia-Pacific Chemicals, LLC
发明人： Joseph F. Ludvik , Xing Dong
IPC分类号： C08L71/00
CPC分类号： C08L71/00 , C04B24/12 , C04B24/36 , C05C3/00 , C08F2/22 , C08G14/06 , C08G14/12 , C09B67/00 , F26B3/00
摘要： Methods for making polymer particles in gel form via an emulsion and/or suspension process are provided. The method can include preparing a reactant mixture comprising a carrier fluid and a monomer component containing one or more phenolic compounds and optionally one or more crosslinking compounds, a mixture of Maillard reactants, or a combination thereof. The monomer component can polymerize to form the polymer particles in gel form. The reactant mixture can be located within a reactor having one or more inner surfaces in contact with the reactant mixture during polymerization of the monomer component. The one or more inner surfaces limit a release of metal, metal ions, or a combination thereof into the reactant mixture to produce the polymer particles in gel form containing less than 1 wt % metal atoms, metal ions, or a combination thereof, based on the total weight of the polymer particles in gel form.
摘要翻译：提供了通过乳液和/或悬浮方法制备凝胶形式的聚合物颗粒的方法。该方法可以包括制备包含载体流体和含有一种或多种酚类化合物和任选的一种或多种交联化合物的单体组分，美拉德反应物的混合物或其组合的反应物混合物。单体组分可以聚合形成凝胶形式的聚合物颗粒。反应物混合物可以位于具有在单体组分聚合期间具有与反应物混合物接触的一个或多个内表面的反应器内。一个或多个内表面将金属，金属离子或其组合的释放限制在反应物混合物中，以基于以下方式产生包含小于1重量％的金属原子，金属离子或其组合的凝胶形式的聚合物颗粒凝胶形式的聚合物颗粒的总重量。

4. 发明申请

US20130209348A1 PREPARATION OF POLYMERIC RESINS AND CARBON MATERIALS 审中-公开
标题翻译：聚合树脂和碳材料的制备
公开(公告)号：US20130209348A1
公开(公告)日：2013-08-15
申请号：US13763460
申请日：2013-02-08
申请人： Georgia-Pacific Chemicals LLC , EnerG2 Technologies, Inc.
发明人： Joseph F. Ludvik , Xing Dong , Shahid P. Qureshi , John B. Hines , Gerald Knazek , Renette E. Richard , Katharine Geramita , Benjamin E. Kron , Henry R. Costantino , Aaron M. Feaver , Avery Sakshaug , Leah A. Thompkins , Alan Tzu-Yang Chang
IPC分类号： C01B31/10 , C01B31/02
CPC分类号： C01B32/336 , H01G11/24 , H01G11/34 , H01G11/42 , H01M4/133 , H01M4/1393 , H01M4/587 , H01M4/625 , H01M10/0525 , Y02E60/13
摘要： The present application is directed to methods for preparation of polymer particles in gel form and carbon materials made therefrom. The carbon materials can have enhanced electrochemical properties and find utility in any number of electrical devices, for example, as electrode material in ultracapacitors or batteries.
摘要翻译：本申请涉及制备凝胶形式的聚合物颗粒和由其制备的碳材料的方法。碳材料可以具有增强的电化学性质，并且可用于任何数量的电气装置，例如作为超级电容器或电池中的电极材料。

5. 发明授权

US10273328B2 Emulsion and suspension polymerization processes, and improved electrochemical performance for carbon derived from same 有权
公开(公告)号：US10273328B2
公开(公告)日：2019-04-30
申请号：US15289499
申请日：2016-10-10
申请人： Georgia-Pacific Chemicals LLC
发明人： Benjamin E. Kron , Katharine Geramita , Henry R. Costantino , Joseph Frank Ludvik , Xing Dong , Shahid P. Qureshi , Gerald A. Knazek
IPC分类号： C01B31/08 , C08G61/10 , C08G8/10 , C08G8/20 , C08G8/22 , C01B32/05 , C01B32/30 , C01B32/336
摘要： The present application is directed to methods for preparation of polymer particles in gel form and carbon materials made therefrom. The carbon materials comprise enhanced electrochemical properties and find utility in any number of electrical devices, for example, as electrode material in ultracapacitors or batteries. The methods herein can also be employed generally to improve emulsion and/or suspension polymerization processes by improved control of diffusion of acidic and basic species between the polymer and secondary phases.

6. 发明授权

US09133337B2 Methods for making polymer particulates in gel form 有权
标题翻译：以凝胶形式制备聚合物微粒的方法
公开(公告)号：US09133337B2
公开(公告)日：2015-09-15
申请号：US13763561
申请日：2013-02-08
申请人： Georgia-Pacific Chemicals, LLC
发明人： Joseph F. Ludvik , Xing Dong
IPC分类号： C08L71/00 , C08F2/22
CPC分类号： C08L71/00 , C04B24/12 , C04B24/36 , C05C3/00 , C08F2/22 , C08G14/06 , C08G14/12 , C09B67/00 , F26B3/00
摘要： Methods for making polymer particles in gel form via an emulsion and/or suspension process are provided. The method can include preparing a reactant mixture comprising a carrier fluid and a monomer component containing one or more phenolic compounds and optionally one or more crosslinking compounds, a mixture of Maillard reactants, or a combination thereof. The monomer component can polymerize to form the polymer particles in gel form. The reactant mixture can be located within a reactor having one or more inner surfaces in contact with the reactant mixture during polymerization of the monomer component. The one or more inner surfaces limit a release of metal, metal ions, or a combination thereof into the reactant mixture to produce the polymer particles in gel form containing less than 1 wt % metal atoms, metal ions, or a combination thereof, based on the total weight of the polymer particles in gel form.
摘要翻译：提供了通过乳液和/或悬浮方法制备凝胶形式的聚合物颗粒的方法。该方法可以包括制备包含载体流体和含有一种或多种酚类化合物和任选的一种或多种交联化合物的单体组分，美拉德反应物的混合物或其组合的反应物混合物。单体组分可以聚合形成凝胶形式的聚合物颗粒。反应物混合物可以位于具有在单体组分聚合期间具有与反应物混合物接触的一个或多个内表面的反应器内。一个或多个内表面将金属，金属离子或其组合的释放限制在反应物混合物中，以基于以下方式产生包含小于1重量％的金属原子，金属离子或其组合的凝胶形式的聚合物颗粒凝胶形式的聚合物颗粒的总重量。

7. 发明申请

US20170316888A1 PREPARATION OF POLYMERIC RESINS AND CARBON MATERIALS 审中-公开
公开(公告)号：US20170316888A1
公开(公告)日：2017-11-02
申请号：US15649546
申请日：2017-07-13
申请人： Georgia-Pacific Chemicals LLC , Energ2 Technologies, Inc.
发明人： Katharine Geramita , Benjamin E. Kron , Henry R. Costantino , Aaron M. Feaver , Avery Sakshaug , Leah A. Thompkins , Alan Tzu-Yang Chang , Xing Dong , Shahid P. Qureshi , John B. Hines , Gerald A. Knazek , Joseph Frank Ludvik
IPC分类号： H01G11/04 , H01G11/34 , H01M4/583 , B01J6/00 , H01G11/38 , H01M4/96 , H01M4/587
CPC分类号： C01B32/30 , B01J6/00 , C01B32/00 , C01B32/05 , C01B32/312 , C01P2004/51 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/17 , H01G11/04 , H01G11/32 , H01G11/34 , H01G11/38 , H01G11/84 , H01M4/583 , H01M4/587 , H01M4/96 , Y02E60/13
摘要： Methods for making carbon materials are provided. In at least one specific embodiment, the method can include combining one or more polymer precursors with one or more liquids to produce a mixture. The mixture can be an emulsion, dispersion, or a suspension. The liquid can include hexane, pentane, cyclopentane, benzene, toluene, o-xylene, m-xylene, p-xylene, diethyl ether, ethylmethylketone, dichloromethane, tetrahydrofuran, mineral oils, paraffin oils, vegetable derived oils, or any mixture thereof. The method can also include aging the mixture at a temperature and time sufficient for the polymer precursor to react and form polymer gel particles having a volume average particle size (Dv,50) of the polymer particles in gel form greater than or equal to 1 mm. The method can also include heating the polymer gel particles to produce a carbon material.

8. 发明申请

US20170190826A1 METHODS FOR MAKING WET GELS AND DRIED GELS THEREFROM 有权
公开(公告)号：US20170190826A1
公开(公告)日：2017-07-06
申请号：US15462414
申请日：2017-03-17
申请人： Georgia-Pacific Chemicals LLC
发明人： Xing Dong , Shahid P. Qureshi , Christopher M. Lee , Kelly A. Shoemake , Joseph Frank Ludvik
IPC分类号： C08G8/28 , C08G8/32 , C08G81/00 , C08J9/28
CPC分类号： C08G8/28 , C01B32/30 , C08G8/32 , C08G16/0225 , C08G16/0256 , C08G81/00 , C08J2201/0504 , C08J2205/022
摘要： Methods for making wet gels and dried gels therefrom are provided. The method for making a wet gel can include combining a hydroxybenzene compound, an aldehyde compound, and an additive to produce a reaction mixture. The additive can include a carboxylic acid, an anhydride, a homopolymer, a copolymer, or any mixture thereof. At least the hydroxybenzene compound and the aldehyde compound can be reacted to produce a wet gel. The reaction mixture can include about 10 wt % to about 65 wt % of the hydroxybenzene compound, about 5 wt % to about 25 wt % of the aldehyde compound, up to about 85 wt % of the carboxylic acid, up to about 40 wt % of the anhydride, up to about 40 wt % of the homopolymer, and up to about 40 wt % of the copolymer, where weight percent values are based on the combined weight of the hydroxybenzene compound, the aldehyde compound, and the additive.

9. 发明申请

US20170029281A1 EMULSION AND SUSPENSION POLYMERIZATION PROCESSES, AND IMPROVED ELECTROCHEMICAL PERFORMANCE FOR CARBON DERIVED FROM SAME 审中-公开
标题翻译：乳化和悬浮聚合方法，以及从其衍生的碳的改进的电化学性能
公开(公告)号：US20170029281A1
公开(公告)日：2017-02-02
申请号：US15289499
申请日：2016-10-10
申请人： Georgia-Pacific Chemicals LLC
发明人： Benjamin E. Kron , Katharine Geramita , Henry R. Costantino , Joseph Frank Ludvik , Xing Dong , Shahid P. Qureshi , Gerald A. Knazek
IPC分类号： C01B31/10 , C08G8/22
CPC分类号： C08G61/10 , C01B32/05 , C01B32/30 , C01B32/336 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/40 , C01P2006/80 , C08G8/10 , C08G8/20 , C08G8/22 , C08G2220/00
摘要： The present application is directed to methods for preparation of polymer particles in gel form and carbon materials made therefrom. The carbon materials comprise enhanced electrochemical properties and find utility in any number of electrical devices, for example, as electrode material in ultracapacitors or batteries. The methods herein can also be employed generally to improve emulsion and/or suspension polymerization processes by improved control of diffusion of acidic and basic species between the polymer and secondary phases.
摘要翻译：本申请涉及制备凝胶形式的聚合物颗粒和由其制备的碳材料的方法。碳材料包括增强的电化学性质，并且可用于任何数量的电气装置，例如作为超级电容器或电池中的电极材料。本文的方法也可以通常用于通过改进控制聚合物和第二相之间的酸性和碱性物质的扩散来改进乳液和/或悬浮聚合方法。

10. 发明申请

US20150087731A1 METHODS FOR MAKING WET GELS AND DRIED GELS THEREFROM 有权
标题翻译：用于制造湿凝胶和干凝胶的方法
公开(公告)号：US20150087731A1
公开(公告)日：2015-03-26
申请号：US14489633
申请日：2014-09-18
申请人： Georgia-Pacific Chemicals LLC
发明人： Xing Dong , Shahid P. Qureshi , Christopher M. Lee , Kelly A. Shoemake , Joseph Frank Ludvik
IPC分类号： C08G8/28 , C08J9/28 , C08G8/32
CPC分类号： C08G8/28 , C01B32/30 , C08G8/32 , C08G16/0225 , C08G16/0256 , C08G81/00 , C08J2201/0504 , C08J2205/022
摘要： Methods for making wet gels and dried gels therefrom are provided. The method for making a wet gel can include combining a hydroxybenzene compound, an aldehyde compound, and an additive to produce a reaction mixture. The additive can include a carboxylic acid, an anhydride, a homopolymer, a copolymer, or any mixture thereof. At least the hydroxybenzene compound and the aldehyde compound can be reacted to produce a wet gel. The reaction mixture can include about 10 wt % to about 65 wt % of the hydroxybenzene compound, about 5 wt % to about 25 wt % of the aldehyde compound, up to about 85 wt % of the carboxylic acid, up to about 40 wt % of the anhydride, up to about 40 wt % of the homopolymer, and up to about 40 wt % of the copolymer, where weight percent values are based on the combined weight of the hydroxybenzene compound, the aldehyde compound, and the additive.
摘要翻译：提供了制备湿凝胶和干凝胶的方法。制备湿凝胶的方法可以包括组合羟基苯化合物，醛化合物和添加剂以产生反应混合物。添加剂可以包括羧酸，酸酐，均聚物，共聚物或其任何混合物。至少可以使羟基苯化合物和醛化合物反应以产生湿凝胶。反应混合物可包括约10重量％至约65重量％的羟基苯化合物，约5重量％至约25重量％的醛化合物，至多约85重量％的羧酸，至多约40重量％的酸酐，最多约40重量％的均聚物和至多约40重量％的共聚物，其中重量百分数值是基于羟基苯化合物，醛化合物和添加剂的总重量。

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