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1. 发明授权

US10173900B2 Preparation of polymeric resins and carbon materials 有权
公开(公告)号：US10173900B2
公开(公告)日：2019-01-08
申请号：US13763460
申请日：2013-02-08
申请人： Georgia-Pacific Chemicals LLC , EnerG2 Technologies, Inc.
发明人： Joseph F. Ludvik , Xing Dong , Shahid P. Qureshi , John B. Hines , Gerald Knazek , Renette E. Richard , Katharine Geramita , Benjamin E. Kron , Henry R. Costantino , Aaron M. Feaver , Avery Sakshaug , Leah A. Thompkins , Alan Tzu-Yang Chang
IPC分类号： C08G8/32 , C01B32/336 , H01M4/133 , H01M4/1393 , H01M4/587 , H01M4/62 , H01G11/24 , H01G11/34 , H01G11/42 , H01M10/0525
摘要： The present application is directed to methods for preparation of polymer particles in gel form and carbon materials made therefrom. The carbon materials can have enhanced electrochemical properties and find utility in any number of electrical devices, for example, as electrode material in ultracapacitors or batteries.

2. 发明申请

US20130209348A1 PREPARATION OF POLYMERIC RESINS AND CARBON MATERIALS 审中-公开
标题翻译：聚合树脂和碳材料的制备
公开(公告)号：US20130209348A1
公开(公告)日：2013-08-15
申请号：US13763460
申请日：2013-02-08
申请人： Georgia-Pacific Chemicals LLC , EnerG2 Technologies, Inc.
发明人： Joseph F. Ludvik , Xing Dong , Shahid P. Qureshi , John B. Hines , Gerald Knazek , Renette E. Richard , Katharine Geramita , Benjamin E. Kron , Henry R. Costantino , Aaron M. Feaver , Avery Sakshaug , Leah A. Thompkins , Alan Tzu-Yang Chang
IPC分类号： C01B31/10 , C01B31/02
CPC分类号： C01B32/336 , H01G11/24 , H01G11/34 , H01G11/42 , H01M4/133 , H01M4/1393 , H01M4/587 , H01M4/625 , H01M10/0525 , Y02E60/13
摘要： The present application is directed to methods for preparation of polymer particles in gel form and carbon materials made therefrom. The carbon materials can have enhanced electrochemical properties and find utility in any number of electrical devices, for example, as electrode material in ultracapacitors or batteries.
摘要翻译：本申请涉及制备凝胶形式的聚合物颗粒和由其制备的碳材料的方法。碳材料可以具有增强的电化学性质，并且可用于任何数量的电气装置，例如作为超级电容器或电池中的电极材料。

3. 发明授权

US09133337B2 Methods for making polymer particulates in gel form 有权
标题翻译：以凝胶形式制备聚合物微粒的方法
公开(公告)号：US09133337B2
公开(公告)日：2015-09-15
申请号：US13763561
申请日：2013-02-08
申请人： Georgia-Pacific Chemicals, LLC
发明人： Joseph F. Ludvik , Xing Dong
IPC分类号： C08L71/00 , C08F2/22
CPC分类号： C08L71/00 , C04B24/12 , C04B24/36 , C05C3/00 , C08F2/22 , C08G14/06 , C08G14/12 , C09B67/00 , F26B3/00
摘要： Methods for making polymer particles in gel form via an emulsion and/or suspension process are provided. The method can include preparing a reactant mixture comprising a carrier fluid and a monomer component containing one or more phenolic compounds and optionally one or more crosslinking compounds, a mixture of Maillard reactants, or a combination thereof. The monomer component can polymerize to form the polymer particles in gel form. The reactant mixture can be located within a reactor having one or more inner surfaces in contact with the reactant mixture during polymerization of the monomer component. The one or more inner surfaces limit a release of metal, metal ions, or a combination thereof into the reactant mixture to produce the polymer particles in gel form containing less than 1 wt % metal atoms, metal ions, or a combination thereof, based on the total weight of the polymer particles in gel form.
摘要翻译：提供了通过乳液和/或悬浮方法制备凝胶形式的聚合物颗粒的方法。该方法可以包括制备包含载体流体和含有一种或多种酚类化合物和任选的一种或多种交联化合物的单体组分，美拉德反应物的混合物或其组合的反应物混合物。单体组分可以聚合形成凝胶形式的聚合物颗粒。反应物混合物可以位于具有在单体组分聚合期间具有与反应物混合物接触的一个或多个内表面的反应器内。一个或多个内表面将金属，金属离子或其组合的释放限制在反应物混合物中，以基于以下方式产生包含小于1重量％的金属原子，金属离子或其组合的凝胶形式的聚合物颗粒凝胶形式的聚合物颗粒的总重量。

4. 发明授权

US10399055B2 Methods for producing precursor solutions and sol-gels for nano-engineered carbon materials and nano-engineered carbon materials created therefrom 有权
公开(公告)号：US10399055B2
公开(公告)日：2019-09-03
申请号：US15959433
申请日：2018-04-23
申请人： Georgia-Pacific Chemicals LLC
发明人： Sudhir M. Mulik , Joseph F. Ludvik , Robert W. Fleming , Christopher M. Lee
IPC分类号： B01J13/00 , C01B32/00 , C01B32/05
摘要： Methods of manufacturing nano-engineered carbon materials, such as carbon aerogels and carbon xerogels, and methods of manufacturing precursor solutions and sol-gels for making the same are provided. A method for manufacturing a precursor solution comprises programmed-addition of a cross-linking agent to a component mixture comprising a resorcinol compound. A method for manufacturing a sol-gel comprises subjecting a precursor solutions to at least one heat treatment. Methods for producing nano-engineered carbon materials from precursor solutions and sol-gels are also provided. Methods for using the nano-engineered carbon materials are also disclosed. The resulting nano-engineered carbon materials can be useful in a range of products including, supercapacitor applications, high-surface-area electrodes, fuel cells, and desalination systems.

5. 发明申请

US20180236424A1 METHODS FOR PRODUCING PRECURSOR SOLUTIONS AND SOL-GELS FOR NANO-ENGINEERED CARBON MATERIALS AND NANO-ENGINEERED CARBON MATERIALS CREATED THEREFROM 审中-公开
公开(公告)号：US20180236424A1
公开(公告)日：2018-08-23
申请号：US15959433
申请日：2018-04-23
申请人： Georgia-Pacific Chemicals LLC
发明人： Sudhir M. Mulik , Joseph F. Ludvik , Robert W. Fleming , Christopher M. Lee
IPC分类号： B01J13/00 , C01B32/05 , C01B32/00
CPC分类号： B01J13/0091 , C01B32/00 , C01B32/05
摘要： Methods of manufacturing nano-engineered carbon materials, such as carbon aerogels and carbon xerogels, and methods of manufacturing precursor solutions and sol-gels for making the same are provided. A method for manufacturing a precursor solution comprises programmed-addition of a cross-linking agent to a component mixture comprising a resorcinol compound. A method for manufacturing a sol-gel comprises subjecting a precursor solutions to at least one heat treatment. Methods for producing nano-engineered carbon materials from precursor solutions and sol-gels are also provided. Methods for using the nano-engineered carbon materials are also disclosed. The resulting nano-engineered carbon materials can be useful in a range of products including, supercapacitor applications, high-surface-area electrodes, fuel cells, and desalination systems.

6. 发明授权

US09968900B2 Methods for producing precursor solutions and sol-gels for nano-engineered carbon materials and nano-engineered carbon materials created therefrom 有权
公开(公告)号：US09968900B2
公开(公告)日：2018-05-15
申请号：US14679400
申请日：2015-04-06
申请人： Georgia-Pacific Chemicals LLC
发明人： Sudhir M. Mulik , Joseph F. Ludvik , Robert W. Fleming , Christopher M. Lee
IPC分类号： C01B31/02 , B01J13/00 , C01B32/00 , C01B32/05
CPC分类号： B01J13/0091 , C01B32/00 , C01B32/05
摘要： Methods of manufacturing nano-engineered carbon materials, such as carbon aerogels and carbon xerogels, and methods of manufacturing precursor solutions and sol-gels for making the same are provided. A method for manufacturing a precursor solution comprises programmed-addition of a cross-linking agent to a component mixture comprising a resorcinol compound. A method for manufacturing a sol-gel comprises subjecting a precursor solutions to at least one heat treatment. Methods for producing nano-engineered carbon materials from precursor solutions and sol-gels are also provided. Methods for using the nano-engineered carbon materials are also disclosed. The resulting nano-engineered carbon materials can be useful in a range of products including, supercapacitor applications, high-surface-area electrodes, fuel cells, and desalination systems.

7. 发明申请

US20150238917A1 METHODS FOR PRODUCING PRECURSOR SOLUTIONS AND SOL-GELS FOR NANO-ENGINEERED CARBON MATERIALS AND NANO-ENGINEERED CARBON MATERIALS CREATED THEREFROM 有权
标题翻译：用于生产纳米工程碳材料的前驱体溶液和溶胶的方法和由其制备的纳米工程碳材料
公开(公告)号：US20150238917A1
公开(公告)日：2015-08-27
申请号：US14679400
申请日：2015-04-06
申请人： Georgia-Pacific Chemicals LLC
发明人： Sudhir M. Mulik , Joseph F. Ludvik , Robert W. Fleming , Christopher M. Lee
IPC分类号： B01J13/00 , C01B31/02
CPC分类号： B01J13/0091 , C01B32/00 , C01B32/05
摘要： Methods of manufacturing nano-engineered carbon materials, such as carbon aerogels and carbon xerogels, and methods of manufacturing precursor solutions and sol-gels for making the same are provided. A method for manufacturing a precursor solution comprises programmed-addition of a cross-linking agent to a component mixture comprising a resorcinol compound. A method for manufacturing a sol-gel comprises subjecting a precursor solutions to at least one heat treatment. Methods for producing nano-engineered carbon materials from precursor solutions and sol-gels are also provided. Methods for using the nano-engineered carbon materials are also disclosed. The resulting nano-engineered carbon materials can be useful in a range of products including, supercapacitor applications, high-surface-area electrodes, fuel cells, and desalination systems.
摘要翻译：提供了制造纳米工程碳材料的方法，例如碳气凝胶和碳干凝胶，以及制造前体溶液和溶胶凝胶制造方法。制备前体溶液的方法包括将交联剂程序加成到包含间苯二酚化合物的组分混合物中。溶胶凝胶的制造方法包括使前体溶液进行至少一种热处理。还提供了从前体溶液和溶胶 - 凝胶制备纳米工程碳材料的方法。还公开了使用纳米工程碳材料的方法。所得的纳米工程碳材料可用于一系列产品，包括超级电容器应用，高表面积电极，燃料电池和脱盐系统。

8. 发明申请

US20130211005A1 METHODS FOR MAKING POLYMER PARTICULATES IN GEL FORM 审中-公开
标题翻译：在凝胶形式中制备聚合物颗粒的方法
公开(公告)号：US20130211005A1
公开(公告)日：2013-08-15
申请号：US13763561
申请日：2013-02-08
申请人： Georgia-Pacific Chemicals, LLC
发明人： Joseph F. Ludvik , Xing Dong
IPC分类号： C08L71/00
CPC分类号： C08L71/00 , C04B24/12 , C04B24/36 , C05C3/00 , C08F2/22 , C08G14/06 , C08G14/12 , C09B67/00 , F26B3/00
摘要： Methods for making polymer particles in gel form via an emulsion and/or suspension process are provided. The method can include preparing a reactant mixture comprising a carrier fluid and a monomer component containing one or more phenolic compounds and optionally one or more crosslinking compounds, a mixture of Maillard reactants, or a combination thereof. The monomer component can polymerize to form the polymer particles in gel form. The reactant mixture can be located within a reactor having one or more inner surfaces in contact with the reactant mixture during polymerization of the monomer component. The one or more inner surfaces limit a release of metal, metal ions, or a combination thereof into the reactant mixture to produce the polymer particles in gel form containing less than 1 wt % metal atoms, metal ions, or a combination thereof, based on the total weight of the polymer particles in gel form.
摘要翻译：提供了通过乳液和/或悬浮方法制备凝胶形式的聚合物颗粒的方法。该方法可以包括制备包含载体流体和含有一种或多种酚类化合物和任选的一种或多种交联化合物的单体组分，美拉德反应物的混合物或其组合的反应物混合物。单体组分可以聚合形成凝胶形式的聚合物颗粒。反应物混合物可以位于具有在单体组分聚合期间具有与反应物混合物接触的一个或多个内表面的反应器内。一个或多个内表面将金属，金属离子或其组合的释放限制在反应物混合物中，以基于以下方式产生包含小于1重量％的金属原子，金属离子或其组合的凝胶形式的聚合物颗粒凝胶形式的聚合物颗粒的总重量。

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