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1. 发明授权

US4286959A Disperse dye formulations 失效
标题翻译：分散染料配方
公开(公告)号：US4286959A
公开(公告)日：1981-09-01
申请号：US18765
申请日：1979-03-08
申请人： Dieter Horn , Ewald Daubach , Erwin Hahn , Herbert Uhrig , Richard Hoene , Herbert Naarmann
发明人： Dieter Horn , Ewald Daubach , Erwin Hahn , Herbert Uhrig , Richard Hoene , Herbert Naarmann
IPC分类号： C09B67/00 , C09B67/38 , D06P1/00 , D06P3/54 , C09B67/22
CPC分类号： D06P3/54 , C09B67/008 , C09B67/0092 , D06P1/0016
摘要： The invention seeks to provide a free-flowing formulation of one or more disperse dyes, with which packages can be dyed homogeneously by the HT process without filtering out of the dye, and which is suitable for the thermosol dyeing process. According to the invention such a formulation comprises one or more disperse dyes (a) enclosed in a matrix of one or more polymers (b) which are soluble, or colloidally soluble, both in water and in an organic solvent, in the form of a solid solution in a state of molecular dispersion or of extremely fine subdivision so that in an X-ray spectrum the dye appears amorphous.The formulations may contain additional assistants conventionally present when dyeing hydrophobic fibers. The formulations contain the disperse dye in an extremely fine state of subdivision. Because of the latter, the formulations give level package dyeings, without filtration of the dye, and very level dyeings when used by the thermofixing process.
摘要翻译：本发明寻求提供一种或多种分散染料的自由流动配方，通过该方法可以通过HT方法将包装均匀地染色，而不过滤出染料，并且适用于热溶胶染色方法。根据本发明，这种制剂包含一种或多种分散染料（a），其包封在一种或多种聚合物（b）的基质中，所述聚合物（b）在水和有机溶剂中都是可溶于或胶体可溶的，形式为在分子分散状态或极细细分的状态下的固溶体，使得在X射线光谱中，染料看起来是无定形的。当染色疏水性纤维时，制剂可以含有通常存在的其它助剂。制剂含有极细细分的分散染料。由于后者，制剂在不过滤染料的情况下给予水平的包装染色，而当用热固定方法使用时，会产生非常高的染色。

2. 发明授权

US4213900A Spray-drying method for the preparation of water-dispersible pulverulent disperse dye formulations 失效
标题翻译：用于制备水分散性粉末分散染料配方的喷雾干燥方法
公开(公告)号：US4213900A
公开(公告)日：1980-07-22
申请号：US925527
申请日：1978-07-17
申请人： Ewald Daubach , Dieter Horn , Erwin Hahn , Herbert Uhrig
发明人： Ewald Daubach , Dieter Horn , Erwin Hahn , Herbert Uhrig
IPC分类号： C09B67/20 , C09B67/06 , C09B67/38 , D06P1/16 , C09B5/24 , C09B6/00 , C09B46/00
CPC分类号： C09B67/0003 , C09B67/008 , D06P1/16 , Y10S534/01
摘要： Easily water-dispersible pulverulent formulations of disperse dyes are prepared by spray-drying a dye solution which comprises(a) one or more disperse dyes,(b) one or more water-soluble anionic dispersants,(c) from 0 to 20% by weight, based on (a+b+c+d), of other surfactants and(d) from 0 to 20% by weight, based on (a+b+c+d) of agents which serve as protective colloids (the proportion of (c+d) being at most 20% by weight).Suitable solvents (e) are formic acid, formamide, N-methylformamide, butyrolactone, ethylene glycol and propylene glycol, which may in addition contain up to 100% by weight, based on (e), of N,N-dimethylformamide or acetic acid or mixtures of these. The formulations obtained by the above process contain the dye in very fine dispersion.
摘要翻译：通过喷雾干燥染料溶液来制备分散染料的易水分散性粉剂，其包含（a）一种或多种分散染料，（b）一种或多种水溶性阴离子分散剂，（c）0-20％基于（a + b + c + d）的其他表面活性剂和（d）0至20重量％，基于（a + b + c + d）作为保护胶体的试剂（比例（c + d）为20重量％以下）。合适的溶剂（e）是甲酸，甲酰胺，N-甲基甲酰胺，丁内酯，乙二醇和丙二醇，其还可以含有至多100重量％（e）的N，N-二甲基甲酰胺或乙酸或这些的混合物。通过上述方法获得的制剂含有非常细的分散体中的染料。

3. 发明授权

US3947287A Aqueous pigment dispersions 失效
标题翻译：水性颜料分散体
公开(公告)号：US3947287A
公开(公告)日：1976-03-30
申请号：US424175
申请日：1973-12-12
申请人： Horst Belde , Knut Oppenlaender , Ewald Daubach , Rolf Fikentscher
发明人： Horst Belde , Knut Oppenlaender , Ewald Daubach , Rolf Fikentscher
IPC分类号： B01F17/42 , C08G65/26 , C08L71/02 , C09B67/20 , C09B67/46 , C09D101/02 , C09C3/08
CPC分类号： C09B67/0089 , C08G65/2609 , C08L71/02 , C09B67/0066 , C09D101/02
摘要： An aqueous pigment dispersion which contains (a) pigment, (b) a water-soluble surfactant and water and a water-retaining agent in which (b) is a reaction product of a polyhydroxyl compound with from 3 to 50 moles of propylene oxide and from 2 to 70 moles of ethylene oxide per equivalent of hydroxyl. The dispersions give bright and deep-shade emulsion paints or distempers containing cellulose ethers.
摘要翻译：一种水性颜料分散体，其包含（a）颜料，（b）水溶性表面活性剂和水和保水剂，其中（b）是多羟基化合物与3-50摩尔环氧丙烷的反应产物和每当量羟基2-70摩尔环氧乙烷。分散体产生含有纤维素醚的明亮和深色乳液漆或碲化物。

4. 发明授权

US3966488A Flowable aqueous pigment formulations containing dipropylene glycol 失效
标题翻译：含有二丙二醇的可流动的含水颜料配方
公开(公告)号：US3966488A
公开(公告)日：1976-06-29
申请号：US438032
申请日：1974-01-30
申请人： Hans Langenfelder , Ewald Daubach , Horst Belde
发明人： Hans Langenfelder , Ewald Daubach , Horst Belde
IPC分类号： C09B67/20 , C04B31/40
CPC分类号： C09B67/006
摘要： Aqueous pigment formulations containing glycol and having good flow, good water retention and good flocculation resistance which contain dipropylene glycol as a flow improver. The formulations are particularly suitable for pigmenting aqueous polymer dispersions and textile pigment printing and dope dyeing.
摘要翻译：含有二醇的水性颜料配方，具有良好的流动性，良好的保水性和良好的抗絮凝性，其含有二丙二醇作为流动改进剂。该制剂特别适用于着色聚合物水分散体和纺织品颜料印花和染料染色。

5. 发明授权

US3960486A Powdered, highly concentrated and stably dispersible dye formulations 失效
标题翻译：粉末状，高浓度和稳定分散的染料配方
公开(公告)号：US3960486A
公开(公告)日：1976-06-01
申请号：US506560
申请日：1974-09-16
申请人： Ewald Daubach , Heinz Saukel , Leonhard Von Rambach
发明人： Ewald Daubach , Heinz Saukel , Leonhard Von Rambach
IPC分类号： C09B67/46 , C09B67/00 , D06P1/44 , D06P1/68
CPC分类号： C09B67/0092 , D06P1/445 , Y10S8/904 , Y10S8/907 , Y10S8/908
摘要： Powdered, highly concentrated and stably dispersible dye formulations which are substantially devoid of dye agglomerates, which contain dyes which are not soluble in water such as disperse dyes or vat dyes, anionactive dispersing agents and (as stabilizing agent) from 2 to 30% by weight based on the dye of a polyethylene oxide having a molecular weight of from 200 to 1000 or a reaction product which has been obtained froma. C.sub.6 to C.sub.20 fatty alcohols;B. alkylphenols of C.sub.4 to C.sub.12 in the alkyl;C. C.sub.14 to C.sub.20 fatty amines;D. castor oil or hydrogenated castor oil;E. C.sub.14 to C.sub.20 fatty acids; orF. natural resin acidswith from 2 to 80 moles of ethylene oxide per mole of OH or NH.sub.2 groups; or fromalkylenediamines of two to five carbon atoms with from 25 to 120 moles of propylene oxide and ethylene oxide per mole of NH.sub.2 groups. The formulations are stable in storage at 60.degree.C and remain devoid of dye agglomerates.
摘要翻译：粉末状，高度浓缩和稳定分散的染料配方，其基本上不含染料附聚物，其含有不溶于水的染料，例如分散染料或还原染料，阴离子活性分散剂和（作为稳定剂）为2至30重量％基于分子量为200〜1000的聚环氧乙烷的染料或由A.C6〜C20脂肪醇得到的反应产物; B.烷基中C4至C12的烷基酚; C14至C20脂肪胺; 蓖麻油或加氢蓖麻油; E. C14至C20脂肪酸; 或F.具有2至80个OH或NH 2基团的每个氧化乙烯的摩尔的天然树脂酸; 或者由二氧化钛的二烷基二胺与二氧化碳和乙二醇氧化物的二氧化碳和二氧化碳的二氧化碳组成的二氧化碳。该制剂在60℃储存时稳定，并且不含染料附聚物。

6. 发明授权

US3956270A .beta.-Modified azo dye 失效
标题翻译： {62-改性偶氮染料
公开(公告)号：US3956270A
公开(公告)日：1976-05-11
申请号：US403640
申请日：1973-10-04
申请人： Leonhard von Rambach , Ewald Daubach , Bertold Honigmann
发明人： Leonhard von Rambach , Ewald Daubach , Bertold Honigmann
IPC分类号： C09B67/48 , C09B29/08 , C09B67/00 , C09B46/00
CPC分类号： C09B29/0825 , C09B29/08 , C09B67/0029
摘要： A new .beta.-modification of the dye of the formula: ##SPC1##Which is eminently suitable for dyeing polyesters in particular and which is surprisingly more stable under dyeing conditions than the modification already known.
摘要翻译：染料的新型β-改性配方：

7. 发明授权

US4464203A Highly concentrated, dust-free, solid and readily dispersible pigment formulations and their use 失效
标题翻译：高度集中，无尘，固体和易分散的颜料配方及其用途
公开(公告)号：US4464203A
公开(公告)日：1984-08-07
申请号：US448049
申请日：1982-12-08
申请人： Horst Belde , Eduard Hartmann , Ewald Daubach
发明人： Horst Belde , Eduard Hartmann , Ewald Daubach
IPC分类号： C09B67/00 , C09B67/20 , C09B67/46 , C09D17/00 , C09C3/08
CPC分类号： C09B67/006 , C09B67/009 , C09B67/0092 , C09D17/003
摘要： Highly concentrated, dust-free, solid and readily dispersible pigment formulations contain(a) from 70 to 95% by weight of one or more finely divided pigments,(b) from 5 to 30% by weight of one or more surfactants which possess 20-45% by weight of ethylene oxide units, have a mean molecular weight of from 4,000 to 15,000 and are obtained by reacting an amine of the formula ##STR1## where R is C.sub.2 -C.sub.6 -alkylene, R.sup.1 is H or C.sub.1 -C.sub.4 -alkyl and n is 1, 2, 3, 4 or 5, or R is 1,3-phenylene, 1,4-phenylene or 4,4'-diphenylenemethane, R.sup.1 is H and n is 1, with propylene oxide and then reacting the product with ethylene oxide, and(c) from 0 to 5% by weight of waxes and/or antifoams, with or without(d) other agents conventionally used in pigment formulations, the percentages being based on (a+b+c).The formulations are very useful for pigmenting aqueous, alcoholic or aqueous/alcoholic printing inks and surface coatings, and printing pastes for textiles.
摘要翻译：高浓度，无尘，固体和容易分散的颜料制剂含有（a）70至95重量％的一种或多种细碎颜料，（b）5至30重量％的一种或多种表面活性剂，其具有20 -45重量％的环氧乙烷单元，其平均分子量为4,000至15,000，并且通过使下式的胺反应得到：其中R是C 2 -C 6 - 亚烷基，R 1是H或C 1 -C 4 - 烷基，n为1,2,3,4或5，或R为1,3-亚苯基，1,4-亚苯基或4,4'-二苯基甲烷，R1为H且n为1，与环氧丙烷反应，然后使具有环氧乙烷的产物，和（c）0至5重量％的蜡和/或消泡剂，具有或不具有常规用于颜料制剂中的其它试剂，百分比基于（a + b + c）。该配方对于着色水性，醇类或水性/醇类印刷油墨和表面涂料以及用于纺织品的印刷浆料是非常有用的。

8. 发明授权

US4218218A Stable finely dispersed aqueous formulations of disperse dyes and optical brighteners, and their use 失效
标题翻译：分散染料和荧光增白剂的稳定的细分散水性配方及其用途
公开(公告)号：US4218218A
公开(公告)日：1980-08-19
申请号：US948347
申请日：1978-10-04
申请人： Ewald Daubach , Manfred Herrmann , Knut Oppenlaender , Karl Stork
发明人： Ewald Daubach , Manfred Herrmann , Knut Oppenlaender , Karl Stork
IPC分类号： B01F17/00 , C07C37/14 , C07C305/10 , C08G65/26 , C08G65/326 , C09B67/38 , C09B67/46 , D06L3/12 , D06P1/613 , C09B29/00 , D06P1/18
CPC分类号： B01F17/0057 , C07C305/10 , C07C37/14 , C08G65/2612 , C08G65/326 , C09B67/008 , C09B67/0086 , D06L3/1264 , D06P1/6135 , Y10S516/03
摘要： The invention relates to an aqueous disperse dye or optical brightener formulation which comprises(a) from 5 to 55 percent by weight, based on (a+c), of one or more finely divided dyes, optical brighteners or mixtures of these,(b) from 10 to 200 percent by weight, based on (a), of a water-soluble surfactant of the formula ##STR1## where X is from 0 to a mean value of 125, Y is from a mean value of 37 to a mean value of 250, but if X is >37, Y:X is at least 1:1, Z is 0 or 1 and Me.sym. is an alkali metal ion, or mixtures of such surfactants,(c) from 45 to 95 percent by weight, based on (a+c) of water or of a mixture of water and a water-retaining agent, with or without(d) further additives conventionally present in aqueous formulations.
摘要翻译：本发明涉及一种含水分散染料或荧光增白剂制剂，其包含（a）基于（a + c）5至55重量％的一种或多种细分散的染料，荧光增白剂或它们的混合物，（b ）基于（a）10至200重量％的下式的水溶性表面活性剂：其中R 1，R 2，R 3，R 3， Z（Me（+））Z其中X为0至平均值125，Y为平均值为37至平均值250，但如果X为> 37，则Y：X至少为1： 1，Z为0或1，Me（+）为碱金属离子或这些表面活性剂的混合物，（c）基于（a + c）水或水混合物的45至95重量％和（d）常规存在于水性制剂中的另外的添加剂的保水剂。

9. 发明授权

US4189445A Surface-active phenolic derivatives 失效
标题翻译：表面活性酚衍生物
公开(公告)号：US4189445A
公开(公告)日：1980-02-19
申请号：US948349
申请日：1978-10-04
申请人： Knut Oppenlaender , Karl Stork , Ewald Daubach , Manfred Herrmann
发明人： Knut Oppenlaender , Karl Stork , Ewald Daubach , Manfred Herrmann
IPC分类号： B01F17/00 , C07C37/14 , C07C305/10 , C08G65/26 , C08G65/326 , C09B67/38 , C09B67/46 , D06L3/12 , D06P1/613 , C07C43/20 , C07C141/14
CPC分类号： B01F17/0057 , C07C305/10 , C07C37/14 , C08G65/2612 , C08G65/326 , C09B67/008 , C09B67/0086 , D06L3/1264 , D06P1/6135 , Y10S516/03
摘要： Oxyalkylated bisphenols are obtained from 2,2-(p,p'-bishydroxydiphenyl)-propane and styrene in the presence of an acid catalyst and are then oxyalkylated, after which they may or may not be sulfated.
摘要翻译：烷氧基化双酚在酸催化剂存在下由2,2-（p，p'-二羟基二苯基） - 丙烷和苯乙烯获得，然后进行烷氧基化，之后它们可以被硫酸化也可以不被硫酸化。

10. 发明授权

US4021226A Herbicides 失效
标题翻译：除草剂
公开(公告)号：US4021226A
公开(公告)日：1977-05-03
申请号：US620712
申请日：1975-10-08
申请人： Helmut Preugschas , Ewald Daubach , Roman Fischer , Manfred Herrmann
发明人： Helmut Preugschas , Ewald Daubach , Roman Fischer , Manfred Herrmann
IPC分类号： A01N25/22 , A01N25/04 , A01N25/30 , A01N43/58 , A01P13/00 , A01N9/22
CPC分类号： A01N25/04 , A01N25/30
摘要： New and valuable herbicide based on 1-phenyl-4-amino-5-chloro (or -5-bromo)-pyridazone-(6) in the form of an aqueous suspension.
摘要翻译：以含水悬浮液形式的基于1-苯基-4-氨基-5-氯（或5-溴） - 哒嗪酮（6）的新的和有价值的除草剂。

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