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1. 发明申请

US20100298610A1 ALDEHYDE COMPOSITIONS DERIVED FROM SEED OILS 有权
标题翻译：从种子油中衍生的醛类组合物
公开(公告)号：US20100298610A1
公开(公告)日：2010-11-25
申请号：US12565446
申请日：2009-09-23
申请人： Zenon Lysenko , Donald L. Morrison , David A. Babb , Donald L. Bunning , Christopher W. Derstine , James H. Gilchrist , H. Ray Jouett , Kurt D. Olson , Wei-Jun Peng , Joe D. Phillips , Brian M. Roesch , Aaron W. Sanders , Alan K. Schrock , Pulikkottil J. Thomas , Jeffrey S. Kanel
发明人： Zenon Lysenko , Donald L. Morrison , David A. Babb , Donald L. Bunning , Christopher W. Derstine , James H. Gilchrist , H. Ray Jouett , Kurt D. Olson , Wei-Jun Peng , Joe D. Phillips , Brian M. Roesch , Aaron W. Sanders , Alan K. Schrock , Pulikkottil J. Thomas , Jeffrey S. Kanel
IPC分类号： C07C47/02
CPC分类号： C08G18/4891 , C07C67/31 , C07C67/347 , C07C69/675 , C07C69/716 , C07C69/732 , C07C69/738 , C08G18/4072 , C08G18/4804 , C08G18/4841 , C08G2101/0008 , C08G2101/005 , C08G2101/0083
摘要： An aldehyde composition derived by hydroformylation of a transesterified seed oil and containing a mixture of formyl-substituted fatty acids or fatty acid esters having the following composition by weight: greater than about 10 to less than about 95 percent monoformyl, greater than about 1 to less than about 65 percent diformyl, and greater than about 0.1 to less than about 10 percent triformyl-substituted fatty acids or fatty acid esters, and having a diformyl to triformyl weight ratio of greater than about 5/1; preferably, greater than about 3 to less than about 20 percent saturates; and preferably, greater than about 1 to less than about 20 percent unsaturates.
摘要翻译：通过酯交换种子油的加氢甲酰化衍生的醛组合物，并含有具有以下重量组成的甲酰取代的脂肪酸或脂肪酸酯的混合物：大于约10至小于约95％的单甲基，大于约1至少并且具有大于约65％的二甲酰基和大于约0.1至小于约10％的三甲酰基取代的脂肪酸或脂肪酸酯，并且具有大于约5/1的二甲酰基 - 三甲酰基重量比; 优选大于约3至小于约20％的饱和物; 并且优选大于约1至小于约20％的不饱和度。

2. 发明申请

US20080221363A1 Process for the Monosulfonation of Aromatic Phosphines, and Zwitterionic Product Derived Therefrom 有权
标题翻译：芳香膦单磺化方法及其衍生的两性离子产物
公开(公告)号：US20080221363A1
公开(公告)日：2008-09-11
申请号：US12064064
申请日：2006-09-14
申请人： Donald L. Morrison , Kurt D. Olson , Walter C. Reed , Anthony G. Abatjoglou
发明人： Donald L. Morrison , Kurt D. Olson , Walter C. Reed , Anthony G. Abatjoglou
IPC分类号： C07F9/54
CPC分类号： C07F9/5022 , C07F9/5442 , C07F9/5449
摘要： A method of preparing an aromatic phosphine monosulfonate in zwitterionic form, such as dicyclohexylphenylphosphine monosulfonate zwitterion, involving contacting an aromatic phosphine with a sulfonating agent to provide a reaction mixture containing aromatic phosphine monosulfonate in acid form and unconverted sulfonating agent; quenching or removing substantially all of the unconverted sulfonating agent; partially neutralizing the aromatic phosphine monosulfonate in acid form to phase separate aromatic phosphine monosulfonate in zwitterionic form as a solid or neat liquid layer; and collecting the zwitterion as a solid or neat liquid. The zwitterion may be neutralized to form the corresponding aromatic phosphine monosulfonate metal salt, which is useful in preparing catalysts for hydroformylation processes.
摘要翻译：一种以两性离子形式制备芳族膦单磺酸盐如二环己基苯基膦单磺酸盐两性离子的方法，包括使芳族膦与磺化剂接触以提供含有酸形式的芳族膦单磺酸盐和未转化的磺化剂的反应混合物; 淬火或去除基本上所有未转化的磺化剂; 部分中和酸形式的芳族膦单磺酸盐作为固体或纯液体层以两性离子形式相分离芳香族膦单磺酸盐; 并收集两性离子作为固体或纯净液体。两性离子可以被中和形成相应的芳族膦单磺酸盐金属盐，其可用于制备用于加氢甲酰化方法的催化剂。

3. 发明授权

US07485759B2 Minimization of ligand degradation products, or reversion of same to useful phosphine ligands 有权
标题翻译：配体降解产物的最小化，或者将其还原成有用的膦配体
公开(公告)号：US07485759B2
公开(公告)日：2009-02-03
申请号：US12018841
申请日：2008-01-24
申请人： John R. Briggs , Wei-Jun Peng , Brian M. Roesch , Anthony G. Abatjoglou , Donald L. Morrison
发明人： John R. Briggs , Wei-Jun Peng , Brian M. Roesch , Anthony G. Abatjoglou , Donald L. Morrison
IPC分类号： C07C45/50
CPC分类号： C07F9/5022 , C07C29/16 , C07C45/50 , C07C45/62 , C07C67/38 , C07C33/03 , C07C69/738 , C07C47/21 , C07C47/02
摘要： A process for the minimization of phosphonium ion ligand degradation products formed during reaction of a polyunsaturated olefin or an unconjugated functionalized olefin in the presence of a transition metal-triorganophosphine ligand complex catalyst to form as a product, by-product, or intermediate product a conjugated functionalized olefin having a carbon-carbon double bond conjugated to an α-electron-withdrawing group, such as, an α,β-unsaturated aldehyde, ketone, ester, acid, or nitrile. The minimization process involves conducting the reaction under selected conditions of conversion, temperature, pressure, or a combination thereof; and/or by selecting a triorganophosphine ligand with a specified steric and/or electronic property. Further, a process for reversion of phosphonium ion ligand degradation product(s) back to useful triorganophosphine ligand(s), the reversion involving treating a reaction product fluid containing the degradation product(s) with an inert gas, hydrogen, synthesis gas, or a mixture thereof under conditions sufficient to regenerate the triorganophosphine ligand(s).
摘要翻译：一种在过渡金属 - 三有机膦配体催化剂存在下，在多不饱和烯烃或非共轭官能化烯烃反应期间形成的鏻离子配体降解产物最小化的方法，以形成产物，副产物或中间产物，共轭具有与α-吸电子基团例如α，β-不饱和醛，酮，酯，酸或腈共轭的碳 - 碳双键的官能化烯烃。最小化方法包括在选择的转化条件，温度，压力或其组合下进行反应; 和/或通过选择具有特定空间和/或电子性质的三有机膦配体。此外，将鏻离子配位体降解产物还原回有用的三有机膦配体的方法，涉及用惰性气体，氢气，合成气体或其混合物处理含有降解产物的反应产物流体的逆转其混合物在足以再生三有机膦配体的条件下进行。

4. 发明授权

US07119216B2 Metathesis of unsaturated fatty acid esters or unsaturated fatty acids with lower olefins 有权
标题翻译：不饱和脂肪酸酯或不饱和脂肪酸与低级烯烃的复分解
公开(公告)号：US07119216B2
公开(公告)日：2006-10-10
申请号：US10469321
申请日：2002-02-27
申请人： Thomas H. Newman , Cynthia L. Rand , Kenneth A. Burdett , Bob R. Maughon , Donald L. Morrison , Eric P. Wasserman
发明人： Thomas H. Newman , Cynthia L. Rand , Kenneth A. Burdett , Bob R. Maughon , Donald L. Morrison , Eric P. Wasserman
IPC分类号： C11C3/00
CPC分类号： C07C51/353 , B01J31/1658 , B01J31/2208 , B01J31/2265 , B01J31/2273 , B01J31/24 , B01J31/2404 , B01J31/28 , B01J2231/543 , B01J2531/821 , B01J2531/825 , C07C7/04 , C07C7/12 , C07C67/333 , Y02P20/127 , C07C11/02 , C07C57/03 , C07C69/533
摘要： An olefin metathesis process involving contacting an unsaturated fatty acid ester or unsaturated fatty acid, such as methyloleate or oleic acid, with a lower olefin, preferably ethylene, in the presence of a metathesis catalyst so as to prepare a first product olefin, preferably, a reduced chain α-olefin, such as methyl-9-decenoate or 9-decenoic acid, respectively. The metathesis catalyst contains ruthenium or osmium and a chelating ligand, preferably, a chelating ligand containing a carbene moiety and a second donor moiety of a Group 15 or 16 element Optionally, the catalyst can be supported on a catalyst support, such as, a cross-linked polymeric resin.
摘要翻译：一种烯烃复分解方法，包括使不饱和脂肪酸酯或不饱和脂肪酸如羟甲基或油酸与复分解催化剂存在下使低级烯烃（优选乙烯）接触，以制备第一产物烯烃，优选为还原链α-烯烃，如9-癸烯酸甲酯或9-癸烯酸。复分解催化剂含有钌或锇和螯合配体，优选含有卡宾部分和第15或16族元素的第二供体部分的螯合配体任选地，催化剂可负载在催化剂载体上，例如十字连接的聚合物树脂。

5. 发明授权

US07754924B2 Process for the monosulfonation of aromatic phosphines, and zwitterionic product derived therefrom 有权
标题翻译：芳香膦单磺化的方法和由其衍生的两性离子产物
公开(公告)号：US07754924B2
公开(公告)日：2010-07-13
申请号：US12064064
申请日：2006-09-14
申请人： Donald L. Morrison , Kurt D. Olson , Walter C. Reed , Anthony G. Abatjoglou
发明人： Donald L. Morrison , Kurt D. Olson , Walter C. Reed , Anthony G. Abatjoglou
IPC分类号： C07F5/02
CPC分类号： C07F9/5022 , C07F9/5442 , C07F9/5449
摘要： A method of preparing an aromatic phosphine monosulfonate in zwitterionic form, such as dicyclohexylphenylphosphine monosulfonate zwitterion, involving contacting an aromatic phosphine with a sulfonating agent to provide a reaction mixture containing aromatic phosphine monosulfonate in acid form and unconverted sulfonating agent; quenching or removing substantially all of the unconverted sulfonating agent; partially neutralizing the aromatic phosphine monosulfonate in acid form to phase separate aromatic phosphine monosulfonate in zwitterionic form as a solid or neat liquid layer; and collecting the zwitterion as a solid or neat liquid. The zwitterion may be neutralized to form the corresponding aromatic phosphine monosulfonate metal salt, which is useful in preparing catalysts for hydroformylation processes.
摘要翻译：一种以两性离子形式制备芳族膦单磺酸盐如二环己基苯基膦单磺酸盐两性离子的方法，包括使芳族膦与磺化剂接触以提供含有酸形式的芳族膦单磺酸盐和未转化的磺化剂的反应混合物; 淬火或去除基本上所有未转化的磺化剂; 部分中和酸形式的芳族膦单磺酸盐作为固体或纯液体层以两性离子形式相分离芳香族膦单磺酸盐; 并收集两性离子作为固体或纯净液体。两性离子可以被中和形成相应的芳族膦单磺酸盐金属盐，其可用于制备用于加氢甲酰化方法的催化剂。

6. 发明授权

US07351868B2 Minimization of ligand degradation products, of reversion of same to useful phosphine ligands 有权
标题翻译：最小化配体降解产物，将其转化为有用的膦配体
公开(公告)号：US07351868B2
公开(公告)日：2008-04-01
申请号：US10562602
申请日：2004-06-28
申请人： John R. Briggs , Wei-Jun Peng , Brian M. Roesch , Anthony G. Abatjoglou , Donald L. Morrison
发明人： John R. Briggs , Wei-Jun Peng , Brian M. Roesch , Anthony G. Abatjoglou , Donald L. Morrison
IPC分类号： C07C45/49 , C07F9/02
CPC分类号： C07F9/5022 , C07C29/16 , C07C45/50 , C07C45/62 , C07C67/38 , C07C33/03 , C07C69/738 , C07C47/21 , C07C47/02
摘要： A process for the minimization of phosphonium ion ligand degradation products formed during reaction of a polyunsaturated olefin or an unconjugated functionalized olefin in the presence of a transition metal-triorganophosphine ligand complex catalyst to form as a product, by-product, or intermediate product a conjugated functionalized olefin having a carbon-carbon double bond conjugated to an a-electronwithdrawing group, such as, an a,β-unsaturated aldehyde, ketone, ester, acid, or nitrile. The minimization process involves conducting the reaction under selected conditions of conversion, temperature, pressure, or a combination thereof; and/or by selecting a triorganophosphine ligand with a specified steric and/or electronic property. Further, a process for reversion of phosphonium ion ligand degradation product(s) back to useful triorganophosphine ligand(s), the reversion involving treating a reaction product fluid containing the degradation product(s) with an inert gas, hydrogen, synthesis gas, or a mixture thereof under conditions sufficient to regenerate the triorganophosphine ligand(s).
摘要翻译：一种在过渡金属 - 三有机膦配体催化剂存在下，在多不饱和烯烃或非共轭官能化烯烃反应期间形成的鏻离子配体降解产物最小化的方法，以形成产物，副产物或中间产物，共轭具有与α-电子取向基团例如a不饱和醛，酮，酯，酸或腈共轭的碳 - 碳双键的官能化烯烃。最小化方法包括在选择的转化条件，温度，压力或其组合下进行反应; 和/或通过选择具有特定空间和/或电子性质的三有机膦配体。此外，将鏻离子配位体降解产物还原回有用的三有机膦配体的方法，涉及用惰性气体，氢气，合成气体或其混合物处理含有降解产物的反应产物流体的逆转其混合物在足以再生三有机膦配体的条件下进行。

7. 发明申请

US20090118548A1 HYDROFORMYLATION PROCESS AND PRODUCT SEPARATION WITH IMPROVED RECOVERY OF RHODIUM 有权
标题翻译：氢氧化工艺和产品分离与改进的RHODIUM恢复
公开(公告)号：US20090118548A1
公开(公告)日：2009-05-07
申请号：US12299853
申请日：2007-04-17
申请人： Wei-Jun Peng , Kurt D. Olson , Donald L. Morrison , Brian M. Roesch , Donald L. Bunning , Jeffrey G. Hippler , Vincent J. Stricker
发明人： Wei-Jun Peng , Kurt D. Olson , Donald L. Morrison , Brian M. Roesch , Donald L. Bunning , Jeffrey G. Hippler , Vincent J. Stricker
IPC分类号： C07C45/50
CPC分类号： C07C45/80 , C07C45/50 , C07C67/347 , Y02P20/584 , C07C69/738 , C07C69/716 , C07C47/02
摘要： A non-aqueous hydroformylation process with liquid catalyst recycle involving a hydroformylation step and one or more stages of phase separation to recover a high molecular weight aldehyde product with efficient recovery of rhodium catalyst. The process includes a hydroformylation step to prepare a non-aqueous hydroformylation reaction product composition comprising one or more aldehyde products, one or more conjugated polyolefins, a rhodium-organophosphorus ligand complex, free organophosphorus ligand, and an organic solubilizing agent for said complex and said free ligand, and thereafter one or more stages of phase separation using added water under a carbon monoxide gas, hydrogen gas, or a mixture thereof. The process requires a specific range of total pressure for the hydroformylation, a specific range of total pressure for at least one of the separation stages, and a minimum sum of the total pressure of the hydroformylation step and the total pressure of the separation stage containing said gas.
摘要翻译：具有液体催化剂循环的非水羰基化方法，其涉及加氢甲酰化步骤和一个或多个相分离阶段以回收高分子量醛产物并有效回收铑催化剂。该方法包括加氢甲酰化步骤，以制备包含一种或多种醛产物，一种或多种共轭聚烯烃，铑 - 有机磷配体络合物，游离有机磷配体和用于所述络合物的有机增溶剂的非水羰基化反应产物组合物和所述游离配体，然后在一氧化碳气体，氢气或其混合物中使用加入的水进行一个或多个相分离阶段。该方法需要加氢甲酰化的总压力的特定范围，至少一个分离阶段的总压力的特定范围，以及加氢甲酰化步骤的总压力和含有所述分离阶段的分离阶段的总压力的最小总和加油站。

8. 发明授权

US4690193A Rolling shutter construction 失效
标题翻译：卷帘构造
公开(公告)号：US4690193A
公开(公告)日：1987-09-01
申请号：US763453
申请日：1985-08-07
申请人： Donald L. Morrison , Stephen Bartok
发明人： Donald L. Morrison , Stephen Bartok
IPC分类号： E06B9/165 , E06B9/16
CPC分类号： E06B9/165
摘要： A rolling shutter characterized by an array of edge-adjacent, parallel shutter slats and full shutter width, clear shutter segments or links articulately interconnecting respective pairs of adjacent shutter slats. The links are telescopically movable in the slats to permit relative movement of the slats between spaced-apart and juxtaposed positions. When spaced apart, the slats form therebetween a gap which exposes the clear link which permits passage of light over substantially the full extent of the gap. The clear links also provide a double hinge-like joint between adjacent slats. The shutter slats are also uniquely reinforced and have an improved exterior appearance.
摘要翻译：一种滚动快门，其特征在于具有边缘相邻的平行快门板条和全快门宽度的阵列，清晰的快门部分或链接铰接地互连相应的相邻的快门板条对。连杆在板条中可伸缩移动，以允许板条在间隔开和并列位置之间相对移动。当间隔开时，板条之间形成有间隙，该间隙暴露清除链节，允许光在空隙的基本上全部范围内通过。清晰的连接还提供了相邻板条之间的双铰链状接头。快门板条也是独特的加强，并具有改进的外观。

9. 发明授权

US4124228A Pressure-balanced fluid coupling 失效
标题翻译：压力平衡流体联轴器
公开(公告)号：US4124228A
公开(公告)日：1978-11-07
申请号：US780598
申请日：1977-03-24
申请人： Donald L. Morrison
发明人： Donald L. Morrison
IPC分类号： F16L37/23 , F16L37/34 , F16L29/00 , F16L37/22
CPC分类号： F16L37/23 , F16L37/34 , Y10T137/87949
摘要： A fluid coupling of the type which couples automatically on the engagement of two coupling members and which uncouples automatically on the application of a predetermined minimum axial separation force, as is useful in refueling operations between moving vehicles. One coupling member has an annular groove about its outer surface, and the other carries at least one locking ball which may be held in engagement with the groove by a lock ring having graduations in internal diameter. Applying a tensile force between the coupling members compresses a spring and simultaneously displaces the lock ring with respect to the ball until an unlocked position is reached, allowing uncoupling by release of the ball from the groove. Uncoupling may also be effected manually and independently of the tensile force applied, and there is a convenient adjustment of the threshold force necessary for uncoupling. The coupling preferably includes automatically operable valves to prevent loss of fluid on uncoupling, and is almost completely pressure balanced, to provide for consistent and reliable operation and very little change in operating characteristics over a wide range of fluid pressures.
摘要翻译：这种类型的流体联轴器在两个联接构件的接合上自动联接，并且在施加预定的最小轴向分离力时自动脱开，如在移动车辆之间的加油操作中有用的。一个联接构件具有围绕其外表面的环形槽，而另一个承载至少一个锁定球，其可以通过具有内径刻度的锁定环保持与凹槽接合。在联接构件之间施加张力压缩弹簧并同时使锁环相对于球移动，直到达到解锁位置，从而允许通过从凹槽释放球而脱开联接。解偶合也可以手动地实现，而不受施加的张力的影响，并且对于解偶联所需的阈值力有方便的调整。联接器优选地包括可自动操作的阀，以防止解耦时的流体损失，并且几乎完全是压力平衡的，以提供一致和可靠的操作，并且在宽范围的流体压力下操作特性的变化很小。

10. 发明授权

US08124812B2 Aldehyde compositions derived from seed oils 有权
标题翻译：衍生自种子油的醛组合物
公开(公告)号：US08124812B2
公开(公告)日：2012-02-28
申请号：US12565446
申请日：2009-09-23
申请人： Zenon Lysenko , Donald L. Morrison , David A. Babb , Donald L. Bunning , Christopher W. Derstine , James H. Gilchrist , H. Ray Jouett , Jeffrey S. Kanel , Kurt D. Olson , Wei-Jun Peng , Joe D. Phillips , Brian M. Roesch , Aaron W. Sanders , Alan K. Schrock , Pulikkottil J. Thomas
发明人： Zenon Lysenko , Donald L. Morrison , David A. Babb , Donald L. Bunning , Christopher W. Derstine , James H. Gilchrist , H. Ray Jouett , Jeffrey S. Kanel , Kurt D. Olson , Wei-Jun Peng , Joe D. Phillips , Brian M. Roesch , Aaron W. Sanders , Alan K. Schrock , Pulikkottil J. Thomas
IPC分类号： C07C47/02 , C07C45/50 , C07C29/14 , C07C59/147
CPC分类号： C08G18/4891 , C07C67/31 , C07C67/347 , C07C69/675 , C07C69/716 , C07C69/732 , C07C69/738 , C08G18/4072 , C08G18/4804 , C08G18/4841 , C08G2101/0008 , C08G2101/005 , C08G2101/0083
摘要： An aldehyde composition derived by hydroformylation of a transesterified seed oil and containing a mixture of formyl-substituted fatty acids or fatty acid esters having the following composition by weight: greater than about 10 to less than about 95 percent monoformyl, greater than about 1 to less than about 65 percent diformyl, and greater than about 0.1 to less than about 10 percent triformyl-substituted fatty acids or fatty acid esters, and having a diformyl to triformyl weight ratio of greater than about 5/1; preferably, greater than about 3 to less than about 20 percent saturates; and preferably, greater than about 1 to less than about 20 percent unsaturates.
摘要翻译：通过酯交换种子油的加氢甲酰化衍生的醛组合物，并含有具有以下重量组成的甲酰取代的脂肪酸或脂肪酸酯的混合物：大于约10至小于约95％的单甲基，大于约1至少并且具有大于约65％的二甲酰基和大于约0.1至小于约10％的三甲酰基取代的脂肪酸或脂肪酸酯，并且具有大于约5/1的二甲酰基 - 三甲酰基重量比; 优选大于约3至小于约20％的饱和物; 并且优选大于约1至小于约20％的不饱和度。

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