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1. 发明授权

US08658077B2 Method of crosslinking carboxyl-containing polymers using oligoamines 有权
标题翻译：使用低聚胺交联含羧基聚合物的方法
公开(公告)号：US08658077B2
公开(公告)日：2014-02-25
申请号：US13059465
申请日：2009-08-05
申请人： Bharat I. Chaudhary , Eric P. Wasserman
发明人： Bharat I. Chaudhary , Eric P. Wasserman
IPC分类号： H01B3/44 , C08F8/32 , C08J3/24
CPC分类号： A43B13/04 , C08F8/32 , C08F2800/20 , C08F2810/20 , C08F2810/50 , C08F210/02 , C08F220/06
摘要： Oligoamines, such as a compound of the formula H2N(CH2CH2NH)nH in which n is an integer of 2-10, crosslink polymers containing carboxyl functionality unexpectedly faster than conventional diamines such as 1,6-diaminohexane. The combination of an ethylene-acrylic acid copolymer with an oligoamine of this type is useful for, among other things, the production of crosslinked wire and cable insulation.
摘要翻译：低聚胺，例如其中n为2-10的整数的式H2N（CH2CH2NH）nH的化合物，交联含有羧基官能团的聚合物意外地比常规二胺如1,6-二氨基己烷更快。乙烯 - 丙烯酸共聚物与这种低聚胺的组合可用于制造交联的电线和电缆绝缘体。

2. 发明申请

US20110318646A1 DUCTILE POLYMER BINDERS AND BATTERY COMPONENTS USING THE SAME 有权
标题翻译： DUCTILE POLYMER BINDERS AND BATTERY COMPONENTS WITH THE SAME
公开(公告)号：US20110318646A1
公开(公告)日：2011-12-29
申请号：US13201069
申请日：2010-02-10
申请人： Susan J. Babinec , Houxiang Tang , Abhijit Ghosh-Dastidar , Eric P. Wasserman , Richard A. Galley , Michael M. Luong
发明人： Susan J. Babinec , Houxiang Tang , Abhijit Ghosh-Dastidar , Eric P. Wasserman , Richard A. Galley , Michael M. Luong
IPC分类号： H01M10/056 , H01M4/62 , C08G65/14 , C08G65/08 , C08G65/12
CPC分类号： C08G65/12 , C08G65/2654 , C08G65/2657 , C08G65/3312 , C08G2650/58 , C08L2205/05 , H01M4/621 , H01M4/622 , H01M10/052 , H01M10/0565 , H01M2004/021 , Y02E60/122
摘要： The present invention is directed at a binder for a battery electrode comprising an ethylene oxide-containing copolymer including a first monomer of ethylene oxide (EO) and at least one additional monomer selected from an alkylene-oxide that is different from the first monomer of EO, an alkyl glycidyl ether, or a combination thereof; wherein the ethylene oxide-containing copolymer has a weight average molecular weight less than about 200,000 g/mole (e.g., from about 10,000 to about 100,000), the molar fraction of the first monomer of EO (XEo) in the ethylene oxide-containing copolymer is greater than 0.80 (e.g., from about 0.80 to about 0.995), and the ethylene oxide-containing copolymer h a peak melting temperature (Tp), in ° C., for a selected XEO in the range of about 0.80 to about 0.995, which is below a maximum value of Tpmax, at the selected XEO, which is calculated using the equation Tpmax=(60−150 (1−XEO)).
摘要翻译：本发明涉及一种用于电池电极的粘合剂，其包含含环氧乙烷的共聚物，其包含环氧乙烷（EO）的第一单体和至少一种选自不同于EO的第一单体的烯化氧的另外的单体，烷基缩水甘油醚或其组合; 其中所述含环氧乙烷的共聚物的重均分子量小于约200,000g / mol（例如约10,000至约100,000），所述环氧乙烷共聚物中EO（XEo）的第一单体的摩尔分数大于0.80（例如，约0.80至约0.995），并且对于所选择的XEO，含环氧乙烷的共聚物ha的峰值熔融温度（Tp）在℃为约0.80至约0.995的范围内，其中在选定的XEO下，使用公式Tpmax =（60-150（1-XEO））来计算Tpmax的最大值。

3. 发明申请

US20100203276A1 In-Situ Methods of Generating Water Through the Dehydration of Metal Salt Hydrates for Moisture Crosslinking of Polyolefins 有权
标题翻译：通过金属盐水合物脱水产生水的现场方法用于聚烯烃的水分交联
公开(公告)号：US20100203276A1
公开(公告)日：2010-08-12
申请号：US12679539
申请日：2008-09-18
申请人： Eric P. Wasserman , Bharat I. Chaudhary , Michael B. Biscoglio
发明人： Eric P. Wasserman , Bharat I. Chaudhary , Michael B. Biscoglio
IPC分类号： B32B1/08 , C08L43/04 , C08K5/098 , B32B27/00
CPC分类号： C08F8/00 , C08J9/125 , C08J2343/04 , C08K5/057 , C08K5/098 , C08K5/57 , Y10T428/139 , C08L43/04
摘要： Compositions comprising a polymer resin comprising at least one copolymer with hydrolysable groups, a water-generating metal salt hydrate, and a catalyst that comprises a metal atom and at least two ligands taken from the set alkyjoxy and carboxylate are used to form articles that moisture-cure through in-situ generation of water via dehydration of the metal hydrate. The compositions are melt mixed to promote the dehydration and start the cure process during the mixing step. The curing compositions are formed and allowed to harden.
摘要翻译：包含包含至少一种具有可水解基团的共聚物的聚合物树脂，产水金属盐水合物和包含金属原子和至少两个取自所述烷氧基和羧酸酯的配体的催化剂的组合物用于形成湿气 - 通过金属水合物的脱水原位生成水来治愈。将组合物熔融混合以促进脱水并在混合步骤期间开始固化过程。形成固化组合物并使其硬化。

4. 发明申请

US20100197873A1 HIGHLY ACTIVE CATALYSTS FOR ALKYLENE OXIDE POLYMERIZATION 有权
标题翻译：用于烷基氧化物聚合的高活性催化剂
公开(公告)号：US20100197873A1
公开(公告)日：2010-08-05
申请号：US12597623
申请日：2008-02-28
申请人： Eric P. Wasserman , Yang Cheng , Lihao Tang
发明人： Eric P. Wasserman , Yang Cheng , Lihao Tang
IPC分类号： C08F4/52 , B01J31/02
CPC分类号： C08G65/12 , C08G65/2654
摘要： The reaction product of the reaction product of A.) a ligand of the formula (I), wherein R1, R2, R3, and R4 in each occurrence independently are the same or different hydrocarbyl substituents of 1 to 20 carbon atoms, hydrogen, halogen, or alkoxy groups of 1 to 8 carbon atoms; X in each occurrence independently is CR6 with R6 being hydrogen or an alkyl group of 1 to 8 carbon atoms; and R5 is an organic divalent group of 4 to 40 carbon atoms with the proviso that the two nodes X are not bound to the same atom or to vicinal atoms in the group R5; B.) an aluminum compound of the formula AlR7R8R9, wherein R7, R8 and R9 each independently is a C1 to C12 hydrocarbyl group, hydrogen, halogen, or an alkoxy group of 1 to 20 carbon atoms; and C.) a Lewis base selected from the group consisting of amines, phosphines, amides, nitriles, isonitriles, and alcohols is useful as a polymerization catalyst, particularly for the homopolymerization or copolymerization of an alkylene oxide.
摘要翻译：式（I）的反应产物的反应产物，其中R 1，R 2，R 3和R 4各自独立地是相同或不同的具有1-20个碳原子的烃基取代基，氢，卤素，或1〜8个碳原子的烷氧基; 每次出现X独立地是CR 6，其中R6是氢或1至8个碳原子的烷基; 并且R 5是4至40个碳原子的有机二价基团，条件是两个结点X不与基团R5中的相同原子或连接原子结合; B.）式AlR 7 R 8 R 9的铝化合物，其中R 7，R 8和R 9各自独立地为C 1至C 12烃基，氢，卤素或具有1至20个碳原子的烷氧基; 和C.）选自胺，膦，酰胺，腈，异腈和醇的路易斯碱可用作聚合催化剂，特别是用于烯化氧的均聚或共聚。

5. 发明授权

US08324311B2 Method for crosslinking polyolefins with in situ generated water 有权
标题翻译：用原位生成水交联聚烯烃的方法
公开(公告)号：US08324311B2
公开(公告)日：2012-12-04
申请号：US12667759
申请日：2008-07-07
申请人： Eric P. Wasserman , Bharat I. Chaudhary
发明人： Eric P. Wasserman , Bharat I. Chaudhary
IPC分类号： C08L41/00
CPC分类号： C08K5/092 , C08K5/175 , C08L23/0892 , C08L2312/08 , Y10T428/139 , C08L43/04
摘要： Compositions comprising a polymer resin comprising at least one copolymer with hydrolysable groups, an amino acid or diearboxylic acid water-generating organic compound, and a catalyst that comprises a metal atom and at least two ligands taken from the set alkyloxy and earhcxylate are used to form articles that moisture-cure through in-situ generation of water via ring-closing dehydration reactions.
摘要翻译：包含包含至少一种具有可水解基团的共聚物的聚合物树脂，氨基酸或二羧酸产水有机化合物的组合物和包含金属原子和至少两个取自组合的烷氧基和己二酸酯的配体的催化剂被用于形成通过闭环脱水反应原位产生水分固化的物品。

6. 发明授权

US08273678B2 Highly active catalysts for alkylene oxide polymerization 有权
标题翻译：用于烯化氧聚合的高活性催化剂
公开(公告)号：US08273678B2
公开(公告)日：2012-09-25
申请号：US12597623
申请日：2008-02-28
申请人： Eric P. Wasserman , Yang Cheng , Lihao Tang
发明人： Eric P. Wasserman , Yang Cheng , Lihao Tang
IPC分类号： B01J31/00
CPC分类号： C08G65/12 , C08G65/2654
摘要： The reaction product of the reaction product of A.) a ligand of the formula (I), wherein R1, R2, R3, and R4 in each occurrence independently are the same or different hydrocarbyl substituents of 1 to 20 carbon atoms, hydrogen, halogen, or alkoxy groups of 1 to 8 carbon atoms; X in each occurrence independently is CR6 with R6 being hydrogen or an alkyl group of 1 to 8 carbon atoms; and R5 is an organic divalent group of 4 to 40 carbon atoms with the proviso that the two nodes X are not bound to the same atom or to vicinal atoms in the group R5; B.) an aluminum compound of the formula AlR7R8R9, wherein R7, R8 and R9 each independently is a C1 to C12 hydrocarbyl group, hydrogen, halogen, or an alkoxy group of 1 to 20 carbon atoms; and C.) a Lewis base selected from the group consisting of amines, phosphines, amides, nitriles, isonitriles, and alcohols is useful as a polymerization catalyst, particularly for the homopolymerization or copolymerization of an alkylene oxide.
摘要翻译：式（I）的反应产物的反应产物，其中R 1，R 2，R 3和R 4各自独立地是相同或不同的具有1-20个碳原子的烃基取代基，氢，卤素，或1〜8个碳原子的烷氧基; 每次出现X独立地是CR 6，其中R6是氢或1至8个碳原子的烷基; 并且R 5是4至40个碳原子的有机二价基团，条件是两个结点X不与基团R5中的相同原子或连接原子结合; B.）式AlR 7 R 8 R 9的铝化合物，其中R 7，R 8和R 9各自独立地为C 1至C 12烃基，氢，卤素或具有1至20个碳原子的烷氧基; 和C.）选自胺，膦，酰胺，腈，异腈和醇的路易斯碱可用作聚合催化剂，特别是用于烯化氧的均聚或共聚。

7. 发明申请

US20110015335A1 In-Situ Method of Generating Through Ring-Closing Dehydration Reactions of Organic Compounds Water for Moisture Crosslinking of Polyolefins 有权
标题翻译：通过有机化合物的闭环脱水反应产生的原位方法聚烯烃水分交联水
公开(公告)号：US20110015335A1
公开(公告)日：2011-01-20
申请号：US12667759
申请日：2008-07-07
申请人： Eric P. Wasserman , Bharat I Chaudhary
发明人： Eric P. Wasserman , Bharat I Chaudhary
IPC分类号： C08L43/04 , C08F8/00
CPC分类号： C08K5/092 , C08K5/175 , C08L23/0892 , C08L2312/08 , Y10T428/139 , C08L43/04
摘要： Compositions comprising a polymer resin comprising at least one copolymer with hydrolysable groups, an amino acid or dicarboxylic acid water-generating organic compound, and a catalyst that comprises a metal atom and at least two ligands taken from the set alkyloxy and earhcxylate are used to form articles that moisture-cure through in-situ generation of water via ring-closing dehydration reactions.
摘要翻译：使用包含至少一种具有可水解基团的共聚物的聚合物树脂，氨基酸或二羧酸产水有机化合物的组合物和包含金属原子和至少两个取自组合的烷氧基和己二酸酯的配体的催化剂，以形成通过闭环脱水反应原位产生水分固化的物品。

8. 发明申请

US20100190955A1 POLY(OXIRANE)S AND PROCESSES AND CATALYSTS FOR MAKING THEM 审中-公开
标题翻译： POLY（OXIRANE）S及其制备方法和催化剂
公开(公告)号：US20100190955A1
公开(公告)日：2010-07-29
申请号：US12445364
申请日：2007-09-06
申请人： Eric P. Wasserman , Richard A. Galley , Woo Min Song , Abhijit Ghosh-Dastidar
发明人： Eric P. Wasserman , Richard A. Galley , Woo Min Song , Abhijit Ghosh-Dastidar
IPC分类号： C08G59/68 , B01J31/22
CPC分类号： B01J31/127 , B01J31/143 , C08G65/12
摘要： A catalyst composition for polymerizing oxiranes is provided that yields high molecular weight poly(oxiranes). The catalyst composition comprises: a hydrophobically modified particulate inorganic oxide; an aluminum alkyl complex; and a compound containing a Lewis basic free electron pair. Polymerization methods and poly(oxirane) polymers are also provided.
摘要翻译：提供用于聚合环氧乙烷的催化剂组合物，其产生高分子量聚（环氧乙烷）。催化剂组合物包括：疏水改性的颗粒无机氧化物; 铝烷基复合物; 和含有路易斯碱性自由电子对的化合物。还提供了聚合方法和聚（环氧乙烷）聚合物。

9. 发明授权

US5317036A Gas phase polymerization reactions utilizing soluble unsupported catalysts 失效
标题翻译：使用可溶性无载体催化剂的气相聚合反应
公开(公告)号：US5317036A
公开(公告)日：1994-05-31
申请号：US962119
申请日：1992-10-16
申请人： Robert C. Brady, III , Frederick J. Karol , Timothy R. Lynn , Robert J. Jorgensen , Sun-Chueh Kao , Eric P. Wasserman
发明人： Robert C. Brady, III , Frederick J. Karol , Timothy R. Lynn , Robert J. Jorgensen , Sun-Chueh Kao , Eric P. Wasserman
IPC分类号： C08F4/642 , B01J8/24 , B01J8/38 , C08F2/00 , C08F2/34 , C08F4/60 , C08F4/62 , C08F4/6592 , C08F10/00 , C08F210/18
CPC分类号： C08F2/34 , B01J8/24 , B01J8/382 , C08F210/18 , Y10S526/901 , Y10S526/943
摘要： Gas phase polymerization processes are disclosed which utilize unsupported soluble transition metal coordination catalysts. The catalysts are introduced into the reactor as a solution.
摘要翻译：公开了使用无载体可溶性过渡金属配位催化剂的气相聚合方法。将催化剂作为溶液引入反应器。

10. 发明授权

US09200084B2 Method for the preparation of a particulate reversibly crosslinked polymeric material 有权
标题翻译：用于制备颗粒可逆交联的聚合物材料的方法
公开(公告)号：US09200084B2
公开(公告)日：2015-12-01
申请号：US13700263
申请日：2010-06-08
申请人： Purnendu Mukherjee , Eric P. Wasserman
发明人： Purnendu Mukherjee , Eric P. Wasserman
IPC分类号： C08B15/00 , C08B3/10 , A61L15/32 , A61K47/48
CPC分类号： C08B3/10 , C08B15/005
摘要： The present invention relates to method for the preparation of a particulate reversibly-crosslinked polymeric material comprising: treating a particulate water-soluble hydroxyl-functional polymer in a liquid phase comprising a solvent mixture in that the hydroxyl-functional polymer is insoluble containing an organic solvent and water; a tetracarboxylic acid dianhydride represented by formula (I), 10 (I) wherein: U and V are independently selected from CH, N and P; 15 X is selected from a single bond, a saturated divalent (C1-C10) hydrocarbon group, O, S, NR, and PR, wherein R is selected from hydrogen and (C1-C4) alkyl; n and m are independently selected from 0 and 1; w is 1 or 2 with the proviso that; 20 if w is 1 then Y is X and if w is 2 then Y is selected from H and (C1-C4) alkyl, whereby there is no bond between both Y; and optionally a catalyst; to form a particulate reversibly-crosslinked polymeric material and 25 to a particulate reversibly-crosslinked polymeric material obtainable thereby.
摘要翻译：本发明涉及制备颗粒可逆交联的聚合物材料的方法，包括：在包含溶剂混合物的液相中处理颗粒状水溶性羟基官能聚合物，因为羟基官能聚合物不溶于含有机溶剂和水; 由式（I）表示的四羧酸二酐，10（I）其中：U和V独立地选自CH，N和P; 15 X选自单键，饱和二价（C1-C10）烃基，O，S，NR和PR，其中R选自氢和（C1-C4）烷基; n和m独立地选自0和1; w为1或2，条件是： 20，如果w为1，则Y为X，如果w为2，则Y选自H和（C 1 -C 4）烷基，由此两者之间不存在键; 和任选的催化剂; 以形成可逆交联的聚合物颗粒和25至可由其获得的可逆交联的聚合物颗粒。

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