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1. 发明申请

US20110136930A1 METHOD FOR PREPARING VISCOELASTIC POLYURETHANE FOAM 审中-公开
标题翻译：制备粘弹性聚氨酯泡沫的方法
公开(公告)号：US20110136930A1
公开(公告)日：2011-06-09
申请号：US13025732
申请日：2011-02-11
申请人： Denise R. Butler , Bernard E. Obi , Rogelio R. Gamboa , Robert E. O'Neill
发明人： Denise R. Butler , Bernard E. Obi , Rogelio R. Gamboa , Robert E. O'Neill
IPC分类号： C08J9/35 , C08K5/098 , C08K5/19 , C09K3/00
CPC分类号： C08G18/4816 , C08G18/163 , C08G18/165 , C08G18/1875 , C08G18/2036 , C08G18/2081 , C08G18/225 , C08G18/244 , C08G18/284 , C08G18/485 , C08G2101/0058 , C08G2101/0083 , C08G2280/00
摘要： Viscoelastic polyurethane foam is prepared by using certain additives in the foam formulation. The additives include 1) alkali metal or transition metal salts of carboxylic acids; 2) 1,3,5-tris alkyl- or 1,3,5-tris (N,N-dialkyl amino alkyl)-hexahydro-s-triazine compounds; and 3) C1-12 carboxylate salts of quaternary ammonium compounds. The additives significantly improve processing and in particular permit the use of higher isocyanate indices, which helps to improve foam physical properties.
摘要翻译：通过在泡沫配方中使用某些添加剂来制备粘弹性聚氨酯泡沫。添加剂包括1）羧酸的碱金属或过渡金属盐; 2）1,3,5-三烷基 - 或1,3,5-三（N，N-二烷基氨基烷基） - 六氢-s-三嗪化合物; 和3）季铵化合物的C1-12羧酸盐。添加剂显着地改善了加工，特别是允许使用更高的异氰酸酯指数，这有助于改善泡沫物理性能。

2. 发明申请

US20090292037A1 METHOD FOR PREPARING VISCOELASTIC POLYURETHANE FOAM 审中-公开
标题翻译：制备粘弹性聚氨酯泡沫的方法
公开(公告)号：US20090292037A1
公开(公告)日：2009-11-26
申请号：US12307988
申请日：2007-08-03
申请人： Denise R. Butler , Bernard E. Obi , Rogelio R. Gamboa , Robert E. O'Neill
发明人： Denise R. Butler , Bernard E. Obi , Rogelio R. Gamboa , Robert E. O'Neill
IPC分类号： C08G18/16 , C09K3/00
CPC分类号： C08G18/4816 , C08G18/163 , C08G18/165 , C08G18/1875 , C08G18/2036 , C08G18/2081 , C08G18/225 , C08G18/244 , C08G18/284 , C08G18/485 , C08G2101/0058 , C08G2101/0083 , C08G2280/00
摘要： Viscoelastic polyurethane foam is prepared by using certain additives in the foam formulation. The additives include 1) alkali metal or transition metal salts of carboxylic acids; 2) 1,3,5-tris alkyl- or 1,3,5-tris (N,N-dialkyl amino alkyl)-hexahydro-s-triazine compounds; and 3) Ci-12 carboxylate salts of quaternary ammonium compounds. The additives significantly improve processing and in particular permit the use of higher isocyanate indices, which helps to improve foam physical properties.
摘要翻译：通过在泡沫配方中使用某些添加剂来制备粘弹性聚氨酯泡沫。添加剂包括1）羧酸的碱金属或过渡金属盐; 2）1,3,5-三烷基 - 或1,3,5-三（N，N-二烷基氨基烷基） - 六氢-s-三嗪化合物; 和3）季铵化合物的C 12 -C 18羧酸盐。添加剂显着地改善了加工，特别是允许使用更高的异氰酸酯指数，这有助于改善泡沫物理性能。

3. 发明授权

US08686058B2 Natural resource based viscoelastic foams 有权
标题翻译：自然资源型粘弹性泡沫
公开(公告)号：US08686058B2
公开(公告)日：2014-04-01
申请号：US13054709
申请日：2009-07-15
申请人： Bernard E. Obi , Alan K. Schrock , Rogelio R. Gamboa , Asjad Shafi
发明人： Bernard E. Obi , Alan K. Schrock , Rogelio R. Gamboa , Asjad Shafi
IPC分类号： C08G18/28
CPC分类号： C08G18/4816 , C08G18/36 , C08G18/4837 , C08G18/6696 , C08G18/7621
摘要： Embodiments of the present invention disclose viscoelastic foams having a renewable natural resource contents of between about 1 and about 25 wt % of the foam. The foams may have a ratio of elastic modulus (E′) at 20° C. to 25% compression force deflection (CFD) of 25 to 125.
摘要翻译：本发明的实施方案公开了具有约1至约25重量％的可再生天然资源含量的粘弹性泡沫。泡沫可以具有在20℃至25％压缩力挠度（CFD）的25至125的弹性模量（E'）的比率。

4. 发明申请

US20130178548A1 USE OF POLY(BUTYLENE OXIDE) POLYOL TO IMPROVE DURABILITY OF MDI-POLYURETHANE FOAMS 有权
标题翻译：使用聚（丁烯氧化物）多元醇改善MDI-聚氨酯泡沫塑料的耐久性
公开(公告)号：US20130178548A1
公开(公告)日：2013-07-11
申请号：US13817749
申请日：2011-08-23
申请人： Kaoru Aou , Rogelio R. Gamboa , Bernard E. Obi
发明人： Kaoru Aou , Rogelio R. Gamboa , Bernard E. Obi
IPC分类号： C08G18/48
CPC分类号： C08G18/4854 , C08G18/283 , C08G18/48 , C08G18/4816 , C08G18/4829 , C08G18/485 , C08G2101/00 , C08G2101/0008 , C08G2101/0083
摘要： Embodiments of the present invention relate to polyurethane foams having high air flow while maintaining viscoelastic properties. In one embodiment, a reaction system for preparation of a viscoelastic polyurethane foam is provided. The reaction system comprises (a) a polyisocyanate component and (b) an isocyanate reactive component. The isocyanate reactive component comprises (i) from 35 to 74% by weight of the isocyanate reactive component of one or more propylene oxide rich (PO-rich) polyols having a combined number average equivalent weight from 200 to 500, (ii) from 24 to 50% by weight of the isocyanate reactive component of one or more ethylene oxide rich (EO-rich) polyols having a combined number average equivalent weight from 200 to 2,800, and (iii)from 2 to 10% by weight of the isocyanate reactive component of one or more butylene oxide rich (BO-rich) polyethers having a number average equivalent weight of 2,000 or more.
摘要翻译：本发明的实施方案涉及具有高空气流量同时保持粘弹性的聚氨酯泡沫体。在一个实施方案中，提供了一种用于制备粘弹性聚氨酯泡沫的反应体系。反应体系包括（a）多异氰酸酯组分和（b）异氰酸酯反应性组分。异氰酸酯反应性组分包含（i）35至74重量％的一种或多种富含氧化丙烯（PO的）多元醇的异氰酸酯反应性组分的数均当量为200至500，（ii）为24 至50重量％的一种或多种二氧化碳富含（EO富含）多元醇的异氰酸酯反应性组分，其数均当量为200至2800，以及（iii）2至10重量％的异氰酸酯反应性一种或多种具有数均当量为2,000以上的富环氧丁烷（BO-富）聚醚的组分。

5. 发明申请

US20130085200A1 HIGH AIR FLOW POLYURETHANE VISCOELASTIC FOAM 审中-公开
标题翻译：高空气流动聚氨酯粘弹性泡沫
公开(公告)号：US20130085200A1
公开(公告)日：2013-04-04
申请号：US13702273
申请日：2011-06-20
申请人： Kaoru Aou , Rogelio R. Gamboa , Bernard E. Obi , Asjad Shafi
发明人： Kaoru Aou , Rogelio R. Gamboa , Bernard E. Obi , Asjad Shafi
IPC分类号： C08G18/06
CPC分类号： C08G18/06 , C08G18/48 , C08G18/4804 , C08G18/4816 , C08G18/4829 , C08G18/4833 , C08G18/6674 , C08G18/6677 , C08G18/7621 , C08G2101/00 , C08G2101/0008 , C08G2101/0083 , C08G2280/00
摘要： Polyurethane foams and methods for making polyurethane foams are provided. The method may comprise forming a reaction mixture including a toluene diisocyanate (TDI) component, an isocyanate reactive component comprising one or more propylene oxide rich (PO-rich) polyols, one or more ethylene oxide rich (EO-rich) polyols having a combined number average equivalent weight from 100 to 500 comprising from 10% to 28% by weight of the total isocyanate reactive component, water, and a catalyst component comprising at least one catalyst, and subjecting the reaction mixture to conditions sufficient to result in the reaction mixture to expand and cure to form a viscoelastic polyurethane foam having a resilience of less than 25%, as measured according to ASTM D3574 Test H.
摘要翻译：提供聚氨酯泡沫和制备聚氨酯泡沫的方法。该方法可以包括形成包括甲苯二异氰酸酯（TDI）组分，包含一种或多种富含氧化丙烯（PO的）多元醇的异氰酸酯反应性组分，一种或多种富含氧化烯（EO）的多元醇的反应混合物，其具有组合数均当量为100至500，包括总异氰酸酯反应性组分的10重量％至28重量％，水和包含至少一种催化剂的催化剂组分，并使反应混合物达到足以产生反应混合物的条件膨胀和固化以形成弹性小于25％的粘弹性聚氨酯泡沫，根据ASTM D3574试验H测量。

6. 发明授权

US09255174B2 Use of poly(butylene oxide) polyol to improve durability of MDI-polyurethane foams 有权
标题翻译：使用聚（环氧丁烷）多元醇改善MDI聚氨酯泡沫塑料的耐久性
公开(公告)号：US09255174B2
公开(公告)日：2016-02-09
申请号：US13817749
申请日：2011-08-23
申请人： Kaoru Aou , Rogelio R. Gamboa , Bernard E. Obi
发明人： Kaoru Aou , Rogelio R. Gamboa , Bernard E. Obi
IPC分类号： C08G18/48 , C08G18/28 , C08G101/00
CPC分类号： C08G18/4854 , C08G18/283 , C08G18/48 , C08G18/4816 , C08G18/4829 , C08G18/485 , C08G2101/00 , C08G2101/0008 , C08G2101/0083
摘要： Embodiments of the present invention relate to polyurethane foams having high air flow while maintaining viscoelastic properties. In one embodiment, a reaction system for preparation of a viscoelastic polyurethane foam is provided. The reaction system comprises (a) a polyisocyanate component and (b) an isocyanate reactive component. The isocyanate reactive component comprises (i) from 35 to 74% by weight of the isocyanate reactive component of one or more propylene oxide rich (PO-rich) polyols having a combined number average equivalent weight from 200 to 500, (ii) from 24 to 50% by weight of the isocyanate reactive component of one or more ethylene oxide rich (EO-rich) polyols having a combined number average equivalent weight from 200 to 2,800, and (iii) from 2 to 10% by weight of the isocyanate reactive component of one or more butylene oxide rich (BO-rich) polyethers having a number average equivalent weight of 2,000 or more.
摘要翻译：本发明的实施方案涉及具有高空气流量同时保持粘弹性的聚氨酯泡沫体。在一个实施方案中，提供了一种用于制备粘弹性聚氨酯泡沫的反应体系。反应体系包括（a）多异氰酸酯组分和（b）异氰酸酯反应性组分。异氰酸酯反应性组分包含（i）35至74重量％的一种或多种富含氧化丙烯（PO的）多元醇的异氰酸酯反应性组分的数均当量为200至500，（ii）为24 至50重量％的一种或多种二氧化碳富含（EO富含）多元醇的异氰酸酯反应性组分，其数均当量为200至2800，以及（iii）2至10重量％的异氰酸酯反应性一种或多种具有数均当量为2,000以上的富环氧丁烷（BO-富）聚醚的组分。

7. 发明申请

US20110124762A1 NATURAL RESOURCE BASED VISCOELASTIC FOAMS 有权
标题翻译：基于自然资源的粘弹性
公开(公告)号：US20110124762A1
公开(公告)日：2011-05-26
申请号：US13054709
申请日：2009-07-15
申请人： Bernard E. Obi , Alan K. Schrock , Rogelio R. Gamboa , Asjad Shafi
发明人： Bernard E. Obi , Alan K. Schrock , Rogelio R. Gamboa , Asjad Shafi
IPC分类号： C08G18/00 , C08J9/00
CPC分类号： C08G18/4816 , C08G18/36 , C08G18/4837 , C08G18/6696 , C08G18/7621
摘要： Embodiments of the present invention disclose viscoelastic foams having a renewable natural resource contents of between about 1 and about 25 wt % of the foam. The foams may have a ratio of elastic modulus (E′) at 20° C. to 25% compression force deflection (CFD) of 25 to 125.
摘要翻译：本发明的实施方案公开了具有约1至约25重量％的可再生天然资源含量的粘弹性泡沫。泡沫可以具有在20℃至25％压缩力挠度（CFD）的25至125的弹性模量（E'）的比率。

8. 发明授权

US08791168B2 Viscoelastic foams having high air flow 有权
标题翻译：具有高气流的粘弹性泡沫
公开(公告)号：US08791168B2
公开(公告)日：2014-07-29
申请号：US12441666
申请日：2007-09-07
申请人： David A. Babb , Bernard E. Obi , Robert E. O'Neill , Alvaro Pauperio-Neto
发明人： David A. Babb , Bernard E. Obi , Robert E. O'Neill , Alvaro Pauperio-Neto
IPC分类号： C08G18/28
CPC分类号： C08G18/4891 , C08G18/165 , C08G18/1825 , C08G18/1833 , C08G18/242 , C08G18/409 , C08G18/4816 , C08G18/4829 , C08G18/4837 , C08G18/4883 , C08G18/7621 , C08G2101/005 , C08G2101/0058 , C08G2101/0083 , C08L83/00
摘要： A viscoelastic polyurethane foam is the reaction product of at least one natural oil derived polyol and at least one aromatic compound having an average of more than one isocyanate group. A viscoelastic polyurethane foam has an air flow of at least about 0.5 l/s, wherein the foam is formed in the substantial absence of copolymer polyol and has not (yet) been mechanically reticulated and is preferably prepared using at least one natural oil derived polyol, more preferably in an amount of at least about 20 weight percent of the polyols used. A process of preparing a viscoelastic foam, comprises steps of (A) forming a reaction mixture including at least one polyol, at least one polyisocyanate, water, at least one catalyst wherein a the polyol comprises at least one natural oil derived polyol; and (B) subjecting the reaction mixture to conditions sufficient to result in the reaction mixture to expand and cure to form a viscoelastic polyurethane foam. In another embodiment, a process comprises steps of (a) forming a natural oil derived polyol composition comprising at least one natural oil derived polyol and water; (b) admixing at least one gelling catalyst and at least one blowing catalyst with the natural oil derived polyol composition to form a catalyst polyol admixture; (c) supplying an isocyanate in an amount corresponding to an isocyanate index for a pMDI of at least about 65 and at most about 95 or, when the isocyanate is a TDI or MDI or combination thereof, at least about 80 and at most about 105; and (c) admixing the isocyanate with the catalyst polyol admixture.
摘要翻译：粘弹性聚氨酯泡沫是至少一种天然油衍生的多元醇与至少一种具有多于一个异氰酸酯基团的芳族化合物的反应产物。粘弹性聚氨酯泡沫具有至少约0.5l / s的空气流，其中泡沫在基本上不存在共聚物多元醇的情况下形成，并且尚未（机械地网状化），并且优选使用至少一种天然油衍生的多元醇，更优选地为所用多元醇的至少约20重量％的量。一种制备粘弹性泡沫的方法，包括以下步骤：（A）形成包含至少一种多元醇，至少一种多异氰酸酯，水，至少一种催化剂的反应混合物，其中多元醇包含至少一种天然油衍生的多元醇; 和（B）使反应混合物达到足以使反应混合物膨胀和固化以形成粘弹性聚氨酯泡沫的条件。在另一个实施方案中，方法包括以下步骤：（a）形成天然油衍生的多元醇组合物，其包含至少一种天然油衍生的多元醇和水; （b）将至少一种胶凝催化剂和至少一种发泡催化剂与天然油衍生的多元醇组合物混合以形成催化剂多元醇混合物; （c）供应对应于至少约65和至多约95的pMDI的异氰酸酯指数的异氰酸酯，或当异氰酸酯是TDI或MDI或其组合时，至少约80和至多约105 ; 和（c）将异氰酸酯与催化剂多元醇混合物混合。

9. 发明申请

US20090306237A1 VISCOELASTIC FOAMS HAVING HIGH AIR FLOW 有权
标题翻译：具有高空气流量的粘弹力
公开(公告)号：US20090306237A1
公开(公告)日：2009-12-10
申请号：US12441666
申请日：2007-09-07
申请人： David A. Babb , Bernard E. Obi , Robert E. O'Neill , Alvaro Pauperio-Neto
发明人： David A. Babb , Bernard E. Obi , Robert E. O'Neill , Alvaro Pauperio-Neto
IPC分类号： C08G18/48 , C08G18/32 , C08G18/34
CPC分类号： C08G18/4891 , C08G18/165 , C08G18/1825 , C08G18/1833 , C08G18/242 , C08G18/409 , C08G18/4816 , C08G18/4829 , C08G18/4837 , C08G18/4883 , C08G18/7621 , C08G2101/005 , C08G2101/0058 , C08G2101/0083 , C08L83/00
摘要： A viscoelastic polyurethane foam is the reaction product of at least one natural oil derived polyol and at least one aromatic compound having an average of more than one isocyanate group. A viscoelastic polyurethane foam has an air flow of at least about 0.5 l/s, wherein the foam is formed in the substantial absence of copolymer polyol and has not (yet) been mechanically reticulated and is preferably prepared using at least one natural oil derived polyol, more preferably in an amount of at least about 20 weight percent of the polyols used. A process of preparing a viscoelastic foam, comprises steps of (A) forming a reaction mixture including at least one polyol, at least one polyisocyanate, water, at least one catalyst wherein a the polyol comprises at least one natural oil derived polyol; and (B) subjecting the reaction mixture to conditions sufficient to result in the reaction mixture to expand and cure to form a viscoelastic polyurethane foam. In another embodiment, a process comprises steps of (a) forming a natural oil derived polyol composition comprising at least one natural oil derived polyol and water; (b) admixing at least one gelling catalyst and at least one blowing catalyst with the natural oil derived polyol composition to form a catalyst polyol admixture; (c) supplying an isocyanate in an amount corresponding to an isocyanate index for a pMDI of at least about 65 and at most about 95 or, when the isocyanate is a TDI or MDI or combination thereof, at least about 80 and at most about 105; and (c) admixing the isocyanate with the catalyst polyol admixture.
摘要翻译：粘弹性聚氨酯泡沫是至少一种天然油衍生的多元醇与至少一种具有多于一个异氰酸酯基团的芳族化合物的反应产物。粘弹性聚氨酯泡沫具有至少约0.5l / s的空气流，其中泡沫在基本上不存在共聚物多元醇的情况下形成，并且尚未（机械地网状化），并且优选使用至少一种天然油衍生的多元醇，更优选地为所用多元醇的至少约20重量％的量。一种制备粘弹性泡沫的方法，包括以下步骤：（A）形成包含至少一种多元醇，至少一种多异氰酸酯，水，至少一种催化剂的反应混合物，其中多元醇包含至少一种天然油衍生的多元醇; 和（B）使反应混合物达到足以使反应混合物膨胀和固化以形成粘弹性聚氨酯泡沫的条件。在另一个实施方案中，方法包括以下步骤：（a）形成天然油衍生的多元醇组合物，其包含至少一种天然油衍生的多元醇和水; （b）将至少一种胶凝催化剂和至少一种发泡催化剂与天然油衍生的多元醇组合物混合以形成催化剂多元醇混合物; （c）供应对应于至少约65和至多约95的pMDI的异氰酸酯指数的异氰酸酯，或当异氰酸酯是TDI或MDI或其组合时，至少约80和至多约105 ; 和（c）将异氰酸酯与催化剂多元醇混合物混合。

10. 发明申请

US20140179815A1 METHOD FOR PREPARING FLEXIBLE POLYURETHANE FOAM WITH HYDROLYSABLE SILANE COMPOUNDS 有权
标题翻译：用可水解的硅烷化合物制备柔性聚氨酯泡沫的方法
公开(公告)号：US20140179815A1
公开(公告)日：2014-06-26
申请号：US14236615
申请日：2012-08-16
申请人： Parvinder S. Walia , Bernard E. Obi , Venkat S. Minnikanti , William A. Koonce , Kamesh R. Vyakaranam , Ling Zhang , Sabrina Fregni
发明人： Parvinder S. Walia , Bernard E. Obi , Venkat S. Minnikanti , William A. Koonce , Kamesh R. Vyakaranam , Ling Zhang , Sabrina Fregni
IPC分类号： C08G18/28
CPC分类号： C08G18/289 , C08G18/10 , C08G18/165 , C08G18/1833 , C08G18/1841 , C08G18/2063 , C08G18/246 , C08G18/3275 , C08G18/4816 , C08G18/4841 , C08G18/6688 , C08G18/7664 , C08G18/778 , C08G2101/0008 , C08G2101/005 , C08G2101/0058 , C08G2101/0083
摘要： Flexible polyurethane foams are made using certain hydrolysable silane compounds in the foam formulation. The hydrolysable silane compounds contain at least one isocyanate-reactive group and at least one hydrolysable silane group. The presence of the hydrolysable silane compound in the foam formulation leads to improved tensile, tear and elongation properties without an adverse effect on other important foam properties such as resiliency and hysteresis loss.
摘要翻译：柔性聚氨酯泡沫在泡沫配方中使用某些可水解的硅烷化合物制成。可水解硅烷化合物含有至少一个异氰酸酯反应性基团和至少一个可水解硅烷基团。泡沫制剂中可水解硅烷化合物的存在导致拉伸，撕裂和伸长性能的改善，而对其它重要的泡沫性能如弹性和滞后损失没有不利影响。

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