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1. 发明授权

US08686058B2 Natural resource based viscoelastic foams 有权
标题翻译：自然资源型粘弹性泡沫
公开(公告)号：US08686058B2
公开(公告)日：2014-04-01
申请号：US13054709
申请日：2009-07-15
申请人： Bernard E. Obi , Alan K. Schrock , Rogelio R. Gamboa , Asjad Shafi
发明人： Bernard E. Obi , Alan K. Schrock , Rogelio R. Gamboa , Asjad Shafi
IPC分类号： C08G18/28
CPC分类号： C08G18/4816 , C08G18/36 , C08G18/4837 , C08G18/6696 , C08G18/7621
摘要： Embodiments of the present invention disclose viscoelastic foams having a renewable natural resource contents of between about 1 and about 25 wt % of the foam. The foams may have a ratio of elastic modulus (E′) at 20° C. to 25% compression force deflection (CFD) of 25 to 125.
摘要翻译：本发明的实施方案公开了具有约1至约25重量％的可再生天然资源含量的粘弹性泡沫。泡沫可以具有在20℃至25％压缩力挠度（CFD）的25至125的弹性模量（E'）的比率。

2. 发明申请

US20110124762A1 NATURAL RESOURCE BASED VISCOELASTIC FOAMS 有权
标题翻译：基于自然资源的粘弹性
公开(公告)号：US20110124762A1
公开(公告)日：2011-05-26
申请号：US13054709
申请日：2009-07-15
申请人： Bernard E. Obi , Alan K. Schrock , Rogelio R. Gamboa , Asjad Shafi
发明人： Bernard E. Obi , Alan K. Schrock , Rogelio R. Gamboa , Asjad Shafi
IPC分类号： C08G18/00 , C08J9/00
CPC分类号： C08G18/4816 , C08G18/36 , C08G18/4837 , C08G18/6696 , C08G18/7621
摘要： Embodiments of the present invention disclose viscoelastic foams having a renewable natural resource contents of between about 1 and about 25 wt % of the foam. The foams may have a ratio of elastic modulus (E′) at 20° C. to 25% compression force deflection (CFD) of 25 to 125.
摘要翻译：本发明的实施方案公开了具有约1至约25重量％的可再生天然资源含量的粘弹性泡沫。泡沫可以具有在20℃至25％压缩力挠度（CFD）的25至125的弹性模量（E'）的比率。

3. 发明申请

US20130085200A1 HIGH AIR FLOW POLYURETHANE VISCOELASTIC FOAM 审中-公开
标题翻译：高空气流动聚氨酯粘弹性泡沫
公开(公告)号：US20130085200A1
公开(公告)日：2013-04-04
申请号：US13702273
申请日：2011-06-20
申请人： Kaoru Aou , Rogelio R. Gamboa , Bernard E. Obi , Asjad Shafi
发明人： Kaoru Aou , Rogelio R. Gamboa , Bernard E. Obi , Asjad Shafi
IPC分类号： C08G18/06
CPC分类号： C08G18/06 , C08G18/48 , C08G18/4804 , C08G18/4816 , C08G18/4829 , C08G18/4833 , C08G18/6674 , C08G18/6677 , C08G18/7621 , C08G2101/00 , C08G2101/0008 , C08G2101/0083 , C08G2280/00
摘要： Polyurethane foams and methods for making polyurethane foams are provided. The method may comprise forming a reaction mixture including a toluene diisocyanate (TDI) component, an isocyanate reactive component comprising one or more propylene oxide rich (PO-rich) polyols, one or more ethylene oxide rich (EO-rich) polyols having a combined number average equivalent weight from 100 to 500 comprising from 10% to 28% by weight of the total isocyanate reactive component, water, and a catalyst component comprising at least one catalyst, and subjecting the reaction mixture to conditions sufficient to result in the reaction mixture to expand and cure to form a viscoelastic polyurethane foam having a resilience of less than 25%, as measured according to ASTM D3574 Test H.
摘要翻译：提供聚氨酯泡沫和制备聚氨酯泡沫的方法。该方法可以包括形成包括甲苯二异氰酸酯（TDI）组分，包含一种或多种富含氧化丙烯（PO的）多元醇的异氰酸酯反应性组分，一种或多种富含氧化烯（EO）的多元醇的反应混合物，其具有组合数均当量为100至500，包括总异氰酸酯反应性组分的10重量％至28重量％，水和包含至少一种催化剂的催化剂组分，并使反应混合物达到足以产生反应混合物的条件膨胀和固化以形成弹性小于25％的粘弹性聚氨酯泡沫，根据ASTM D3574试验H测量。

4. 发明申请

US20130178548A1 USE OF POLY(BUTYLENE OXIDE) POLYOL TO IMPROVE DURABILITY OF MDI-POLYURETHANE FOAMS 有权
标题翻译：使用聚（丁烯氧化物）多元醇改善MDI-聚氨酯泡沫塑料的耐久性
公开(公告)号：US20130178548A1
公开(公告)日：2013-07-11
申请号：US13817749
申请日：2011-08-23
申请人： Kaoru Aou , Rogelio R. Gamboa , Bernard E. Obi
发明人： Kaoru Aou , Rogelio R. Gamboa , Bernard E. Obi
IPC分类号： C08G18/48
CPC分类号： C08G18/4854 , C08G18/283 , C08G18/48 , C08G18/4816 , C08G18/4829 , C08G18/485 , C08G2101/00 , C08G2101/0008 , C08G2101/0083
摘要： Embodiments of the present invention relate to polyurethane foams having high air flow while maintaining viscoelastic properties. In one embodiment, a reaction system for preparation of a viscoelastic polyurethane foam is provided. The reaction system comprises (a) a polyisocyanate component and (b) an isocyanate reactive component. The isocyanate reactive component comprises (i) from 35 to 74% by weight of the isocyanate reactive component of one or more propylene oxide rich (PO-rich) polyols having a combined number average equivalent weight from 200 to 500, (ii) from 24 to 50% by weight of the isocyanate reactive component of one or more ethylene oxide rich (EO-rich) polyols having a combined number average equivalent weight from 200 to 2,800, and (iii)from 2 to 10% by weight of the isocyanate reactive component of one or more butylene oxide rich (BO-rich) polyethers having a number average equivalent weight of 2,000 or more.
摘要翻译：本发明的实施方案涉及具有高空气流量同时保持粘弹性的聚氨酯泡沫体。在一个实施方案中，提供了一种用于制备粘弹性聚氨酯泡沫的反应体系。反应体系包括（a）多异氰酸酯组分和（b）异氰酸酯反应性组分。异氰酸酯反应性组分包含（i）35至74重量％的一种或多种富含氧化丙烯（PO的）多元醇的异氰酸酯反应性组分的数均当量为200至500，（ii）为24 至50重量％的一种或多种二氧化碳富含（EO富含）多元醇的异氰酸酯反应性组分，其数均当量为200至2800，以及（iii）2至10重量％的异氰酸酯反应性一种或多种具有数均当量为2,000以上的富环氧丁烷（BO-富）聚醚的组分。

5. 发明申请

US20110136930A1 METHOD FOR PREPARING VISCOELASTIC POLYURETHANE FOAM 审中-公开
标题翻译：制备粘弹性聚氨酯泡沫的方法
公开(公告)号：US20110136930A1
公开(公告)日：2011-06-09
申请号：US13025732
申请日：2011-02-11
申请人： Denise R. Butler , Bernard E. Obi , Rogelio R. Gamboa , Robert E. O'Neill
发明人： Denise R. Butler , Bernard E. Obi , Rogelio R. Gamboa , Robert E. O'Neill
IPC分类号： C08J9/35 , C08K5/098 , C08K5/19 , C09K3/00
CPC分类号： C08G18/4816 , C08G18/163 , C08G18/165 , C08G18/1875 , C08G18/2036 , C08G18/2081 , C08G18/225 , C08G18/244 , C08G18/284 , C08G18/485 , C08G2101/0058 , C08G2101/0083 , C08G2280/00
摘要： Viscoelastic polyurethane foam is prepared by using certain additives in the foam formulation. The additives include 1) alkali metal or transition metal salts of carboxylic acids; 2) 1,3,5-tris alkyl- or 1,3,5-tris (N,N-dialkyl amino alkyl)-hexahydro-s-triazine compounds; and 3) C1-12 carboxylate salts of quaternary ammonium compounds. The additives significantly improve processing and in particular permit the use of higher isocyanate indices, which helps to improve foam physical properties.
摘要翻译：通过在泡沫配方中使用某些添加剂来制备粘弹性聚氨酯泡沫。添加剂包括1）羧酸的碱金属或过渡金属盐; 2）1,3,5-三烷基 - 或1,3,5-三（N，N-二烷基氨基烷基） - 六氢-s-三嗪化合物; 和3）季铵化合物的C1-12羧酸盐。添加剂显着地改善了加工，特别是允许使用更高的异氰酸酯指数，这有助于改善泡沫物理性能。

6. 发明授权

US09255174B2 Use of poly(butylene oxide) polyol to improve durability of MDI-polyurethane foams 有权
标题翻译：使用聚（环氧丁烷）多元醇改善MDI聚氨酯泡沫塑料的耐久性
公开(公告)号：US09255174B2
公开(公告)日：2016-02-09
申请号：US13817749
申请日：2011-08-23
申请人： Kaoru Aou , Rogelio R. Gamboa , Bernard E. Obi
发明人： Kaoru Aou , Rogelio R. Gamboa , Bernard E. Obi
IPC分类号： C08G18/48 , C08G18/28 , C08G101/00
CPC分类号： C08G18/4854 , C08G18/283 , C08G18/48 , C08G18/4816 , C08G18/4829 , C08G18/485 , C08G2101/00 , C08G2101/0008 , C08G2101/0083
摘要： Embodiments of the present invention relate to polyurethane foams having high air flow while maintaining viscoelastic properties. In one embodiment, a reaction system for preparation of a viscoelastic polyurethane foam is provided. The reaction system comprises (a) a polyisocyanate component and (b) an isocyanate reactive component. The isocyanate reactive component comprises (i) from 35 to 74% by weight of the isocyanate reactive component of one or more propylene oxide rich (PO-rich) polyols having a combined number average equivalent weight from 200 to 500, (ii) from 24 to 50% by weight of the isocyanate reactive component of one or more ethylene oxide rich (EO-rich) polyols having a combined number average equivalent weight from 200 to 2,800, and (iii) from 2 to 10% by weight of the isocyanate reactive component of one or more butylene oxide rich (BO-rich) polyethers having a number average equivalent weight of 2,000 or more.
摘要翻译：本发明的实施方案涉及具有高空气流量同时保持粘弹性的聚氨酯泡沫体。在一个实施方案中，提供了一种用于制备粘弹性聚氨酯泡沫的反应体系。反应体系包括（a）多异氰酸酯组分和（b）异氰酸酯反应性组分。异氰酸酯反应性组分包含（i）35至74重量％的一种或多种富含氧化丙烯（PO的）多元醇的异氰酸酯反应性组分的数均当量为200至500，（ii）为24 至50重量％的一种或多种二氧化碳富含（EO富含）多元醇的异氰酸酯反应性组分，其数均当量为200至2800，以及（iii）2至10重量％的异氰酸酯反应性一种或多种具有数均当量为2,000以上的富环氧丁烷（BO-富）聚醚的组分。

7. 发明申请

US20090292037A1 METHOD FOR PREPARING VISCOELASTIC POLYURETHANE FOAM 审中-公开
标题翻译：制备粘弹性聚氨酯泡沫的方法
公开(公告)号：US20090292037A1
公开(公告)日：2009-11-26
申请号：US12307988
申请日：2007-08-03
申请人： Denise R. Butler , Bernard E. Obi , Rogelio R. Gamboa , Robert E. O'Neill
发明人： Denise R. Butler , Bernard E. Obi , Rogelio R. Gamboa , Robert E. O'Neill
IPC分类号： C08G18/16 , C09K3/00
CPC分类号： C08G18/4816 , C08G18/163 , C08G18/165 , C08G18/1875 , C08G18/2036 , C08G18/2081 , C08G18/225 , C08G18/244 , C08G18/284 , C08G18/485 , C08G2101/0058 , C08G2101/0083 , C08G2280/00
摘要： Viscoelastic polyurethane foam is prepared by using certain additives in the foam formulation. The additives include 1) alkali metal or transition metal salts of carboxylic acids; 2) 1,3,5-tris alkyl- or 1,3,5-tris (N,N-dialkyl amino alkyl)-hexahydro-s-triazine compounds; and 3) Ci-12 carboxylate salts of quaternary ammonium compounds. The additives significantly improve processing and in particular permit the use of higher isocyanate indices, which helps to improve foam physical properties.
摘要翻译：通过在泡沫配方中使用某些添加剂来制备粘弹性聚氨酯泡沫。添加剂包括1）羧酸的碱金属或过渡金属盐; 2）1,3,5-三烷基 - 或1,3,5-三（N，N-二烷基氨基烷基） - 六氢-s-三嗪化合物; 和3）季铵化合物的C 12 -C 18羧酸盐。添加剂显着地改善了加工，特别是允许使用更高的异氰酸酯指数，这有助于改善泡沫物理性能。

8. 发明申请

US20140179815A1 METHOD FOR PREPARING FLEXIBLE POLYURETHANE FOAM WITH HYDROLYSABLE SILANE COMPOUNDS 有权
标题翻译：用可水解的硅烷化合物制备柔性聚氨酯泡沫的方法
公开(公告)号：US20140179815A1
公开(公告)日：2014-06-26
申请号：US14236615
申请日：2012-08-16
申请人： Parvinder S. Walia , Bernard E. Obi , Venkat S. Minnikanti , William A. Koonce , Kamesh R. Vyakaranam , Ling Zhang , Sabrina Fregni
发明人： Parvinder S. Walia , Bernard E. Obi , Venkat S. Minnikanti , William A. Koonce , Kamesh R. Vyakaranam , Ling Zhang , Sabrina Fregni
IPC分类号： C08G18/28
CPC分类号： C08G18/289 , C08G18/10 , C08G18/165 , C08G18/1833 , C08G18/1841 , C08G18/2063 , C08G18/246 , C08G18/3275 , C08G18/4816 , C08G18/4841 , C08G18/6688 , C08G18/7664 , C08G18/778 , C08G2101/0008 , C08G2101/005 , C08G2101/0058 , C08G2101/0083
摘要： Flexible polyurethane foams are made using certain hydrolysable silane compounds in the foam formulation. The hydrolysable silane compounds contain at least one isocyanate-reactive group and at least one hydrolysable silane group. The presence of the hydrolysable silane compound in the foam formulation leads to improved tensile, tear and elongation properties without an adverse effect on other important foam properties such as resiliency and hysteresis loss.
摘要翻译：柔性聚氨酯泡沫在泡沫配方中使用某些可水解的硅烷化合物制成。可水解硅烷化合物含有至少一个异氰酸酯反应性基团和至少一个可水解硅烷基团。泡沫制剂中可水解硅烷化合物的存在导致拉伸，撕裂和伸长性能的改善，而对其它重要的泡沫性能如弹性和滞后损失没有不利影响。

9. 发明申请

US20140057811A1 CURABLE COMPOSITION FOR USE AS LOST CIRCULATION MATERIAL 有权
标题翻译：可固化组合物用作失效循环材料
公开(公告)号：US20140057811A1
公开(公告)日：2014-02-27
申请号：US14004819
申请日：2012-05-03
申请人： Phillip S. Athey , Bernard E. Obi , Michael K. Poindexter
发明人： Phillip S. Athey , Bernard E. Obi , Michael K. Poindexter
IPC分类号： C09K8/035
CPC分类号： C09K8/035 , C08G18/672 , C09D175/16 , C09K8/5086 , C08G18/48
摘要： The present invention relates to compositions and methods for reducing or preventing the loss of drilling fluids and other well servicing fluids into a subterranean formation during drilling or construction of boreholes in said formation. Specifically, this invention comprises a curable composition capable of free radical polymerization for creating lost circulation material in-situ. The curable composition comprises an organic compound capable of free radical (co)polymerization represented by the formula (I): wherein x is an integer from 1 to 8; Fp comprises one or more moiety comprising a free radical polymerizable group; L is an organic moiety comprising a (substituted) aromatic or (substituted) aliphatic group comprising one or more O, N, S, or combinations thereof; and Q comprises a substituted or unsubstituted mono- or polyvalent organic radical comprising one or one or more moiety selected from alkyl, alkylene, alkenyl, cycloalkyl, cycloalkylene, aryl, aralkyl, alkaryl, poly(oxyalkylene), poly(carboalkoxyalkylene), a substituted heterocyclic radical, or an unsubstituted heterocyclic radical.
摘要翻译：本发明涉及用于减少或防止在所述地层钻孔或构造井眼期间钻井液和其它维修良好的流体进入地下地层的组合物和方法。具体地说，本发明包括能够进行自由基聚合的可固化组合物，用于原位产生流失物质。可固化组合物包含能够由式（I）表示的自由基（共）聚合的有机化合物：其中x是1至8的整数; Fp包含一个或多个包含自由基可聚合基团的部分; L是包含（取代的）芳族或（取代的）脂族基团的有机部分，其包含一个或多个O，N，S或它们的组合; 和Q包括取代或未取代的单价或多价有机基团，其包含选自烷基，亚烷基，烯基，环烷基，亚环烷基，芳基，芳烷基，烷芳基，聚（氧化烯），聚（碳烷氧基亚烷基）杂环基或未取代的杂环基。

10. 发明授权

US09688899B2 Curable composition for use as lost circulation material 有权
公开(公告)号：US09688899B2
公开(公告)日：2017-06-27
申请号：US14004819
申请日：2012-05-03
申请人： Phillip S. Athey , Bernard E. Obi , Michael K. Poindexter
发明人： Phillip S. Athey , Bernard E. Obi , Michael K. Poindexter
IPC分类号： C09K8/035 , C09K8/508 , C08G18/67 , C09D175/16
CPC分类号： C09K8/035 , C08G18/672 , C09D175/16 , C09K8/5086 , C08G18/48
摘要： The present invention relates to compositions and methods for reducing or preventing the loss of drilling fluids and other well servicing fluids into a subterranean formation during drilling or construction of boreholes in said formation. Specifically, this invention comprises a curable composition capable of free radical polymerization for creating lost circulation material in-situ. The curable composition comprises an organic compound capable of free radical (co)polymerization represented by the formula (I): wherein x is an integer from 1 to 8; Fp comprises one or more moiety comprising a free radical polymerizable group; L is an organic moiety comprising a (substituted) aromatic or (substituted) aliphatic group comprising one or more O, N, S, or combinations thereof; and Q comprises a substituted or unsubstituted mono- or polyvalent organic radical comprising one or one or more moiety selected from alkyl, alkylene, alkenyl, cycloalkyl, cycloalkylene, aryl, aralkyl, alkaryl, poly(oxyalkylene), poly(carboalkoxyalkylene), a substituted heterocyclic radical, or an unsubstituted heterocyclic radical.

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