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1. 发明授权

US08791168B2 Viscoelastic foams having high air flow 有权
标题翻译：具有高气流的粘弹性泡沫
公开(公告)号：US08791168B2
公开(公告)日：2014-07-29
申请号：US12441666
申请日：2007-09-07
申请人： David A. Babb , Bernard E. Obi , Robert E. O'Neill , Alvaro Pauperio-Neto
发明人： David A. Babb , Bernard E. Obi , Robert E. O'Neill , Alvaro Pauperio-Neto
IPC分类号： C08G18/28
CPC分类号： C08G18/4891 , C08G18/165 , C08G18/1825 , C08G18/1833 , C08G18/242 , C08G18/409 , C08G18/4816 , C08G18/4829 , C08G18/4837 , C08G18/4883 , C08G18/7621 , C08G2101/005 , C08G2101/0058 , C08G2101/0083 , C08L83/00
摘要： A viscoelastic polyurethane foam is the reaction product of at least one natural oil derived polyol and at least one aromatic compound having an average of more than one isocyanate group. A viscoelastic polyurethane foam has an air flow of at least about 0.5 l/s, wherein the foam is formed in the substantial absence of copolymer polyol and has not (yet) been mechanically reticulated and is preferably prepared using at least one natural oil derived polyol, more preferably in an amount of at least about 20 weight percent of the polyols used. A process of preparing a viscoelastic foam, comprises steps of (A) forming a reaction mixture including at least one polyol, at least one polyisocyanate, water, at least one catalyst wherein a the polyol comprises at least one natural oil derived polyol; and (B) subjecting the reaction mixture to conditions sufficient to result in the reaction mixture to expand and cure to form a viscoelastic polyurethane foam. In another embodiment, a process comprises steps of (a) forming a natural oil derived polyol composition comprising at least one natural oil derived polyol and water; (b) admixing at least one gelling catalyst and at least one blowing catalyst with the natural oil derived polyol composition to form a catalyst polyol admixture; (c) supplying an isocyanate in an amount corresponding to an isocyanate index for a pMDI of at least about 65 and at most about 95 or, when the isocyanate is a TDI or MDI or combination thereof, at least about 80 and at most about 105; and (c) admixing the isocyanate with the catalyst polyol admixture.
摘要翻译：粘弹性聚氨酯泡沫是至少一种天然油衍生的多元醇与至少一种具有多于一个异氰酸酯基团的芳族化合物的反应产物。粘弹性聚氨酯泡沫具有至少约0.5l / s的空气流，其中泡沫在基本上不存在共聚物多元醇的情况下形成，并且尚未（机械地网状化），并且优选使用至少一种天然油衍生的多元醇，更优选地为所用多元醇的至少约20重量％的量。一种制备粘弹性泡沫的方法，包括以下步骤：（A）形成包含至少一种多元醇，至少一种多异氰酸酯，水，至少一种催化剂的反应混合物，其中多元醇包含至少一种天然油衍生的多元醇; 和（B）使反应混合物达到足以使反应混合物膨胀和固化以形成粘弹性聚氨酯泡沫的条件。在另一个实施方案中，方法包括以下步骤：（a）形成天然油衍生的多元醇组合物，其包含至少一种天然油衍生的多元醇和水; （b）将至少一种胶凝催化剂和至少一种发泡催化剂与天然油衍生的多元醇组合物混合以形成催化剂多元醇混合物; （c）供应对应于至少约65和至多约95的pMDI的异氰酸酯指数的异氰酸酯，或当异氰酸酯是TDI或MDI或其组合时，至少约80和至多约105 ; 和（c）将异氰酸酯与催化剂多元醇混合物混合。

2. 发明申请

US20090306237A1 VISCOELASTIC FOAMS HAVING HIGH AIR FLOW 有权
标题翻译：具有高空气流量的粘弹力
公开(公告)号：US20090306237A1
公开(公告)日：2009-12-10
申请号：US12441666
申请日：2007-09-07
申请人： David A. Babb , Bernard E. Obi , Robert E. O'Neill , Alvaro Pauperio-Neto
发明人： David A. Babb , Bernard E. Obi , Robert E. O'Neill , Alvaro Pauperio-Neto
IPC分类号： C08G18/48 , C08G18/32 , C08G18/34
CPC分类号： C08G18/4891 , C08G18/165 , C08G18/1825 , C08G18/1833 , C08G18/242 , C08G18/409 , C08G18/4816 , C08G18/4829 , C08G18/4837 , C08G18/4883 , C08G18/7621 , C08G2101/005 , C08G2101/0058 , C08G2101/0083 , C08L83/00
摘要： A viscoelastic polyurethane foam is the reaction product of at least one natural oil derived polyol and at least one aromatic compound having an average of more than one isocyanate group. A viscoelastic polyurethane foam has an air flow of at least about 0.5 l/s, wherein the foam is formed in the substantial absence of copolymer polyol and has not (yet) been mechanically reticulated and is preferably prepared using at least one natural oil derived polyol, more preferably in an amount of at least about 20 weight percent of the polyols used. A process of preparing a viscoelastic foam, comprises steps of (A) forming a reaction mixture including at least one polyol, at least one polyisocyanate, water, at least one catalyst wherein a the polyol comprises at least one natural oil derived polyol; and (B) subjecting the reaction mixture to conditions sufficient to result in the reaction mixture to expand and cure to form a viscoelastic polyurethane foam. In another embodiment, a process comprises steps of (a) forming a natural oil derived polyol composition comprising at least one natural oil derived polyol and water; (b) admixing at least one gelling catalyst and at least one blowing catalyst with the natural oil derived polyol composition to form a catalyst polyol admixture; (c) supplying an isocyanate in an amount corresponding to an isocyanate index for a pMDI of at least about 65 and at most about 95 or, when the isocyanate is a TDI or MDI or combination thereof, at least about 80 and at most about 105; and (c) admixing the isocyanate with the catalyst polyol admixture.
摘要翻译：粘弹性聚氨酯泡沫是至少一种天然油衍生的多元醇与至少一种具有多于一个异氰酸酯基团的芳族化合物的反应产物。粘弹性聚氨酯泡沫具有至少约0.5l / s的空气流，其中泡沫在基本上不存在共聚物多元醇的情况下形成，并且尚未（机械地网状化），并且优选使用至少一种天然油衍生的多元醇，更优选地为所用多元醇的至少约20重量％的量。一种制备粘弹性泡沫的方法，包括以下步骤：（A）形成包含至少一种多元醇，至少一种多异氰酸酯，水，至少一种催化剂的反应混合物，其中多元醇包含至少一种天然油衍生的多元醇; 和（B）使反应混合物达到足以使反应混合物膨胀和固化以形成粘弹性聚氨酯泡沫的条件。在另一个实施方案中，方法包括以下步骤：（a）形成天然油衍生的多元醇组合物，其包含至少一种天然油衍生的多元醇和水; （b）将至少一种胶凝催化剂和至少一种发泡催化剂与天然油衍生的多元醇组合物混合以形成催化剂多元醇混合物; （c）供应对应于至少约65和至多约95的pMDI的异氰酸酯指数的异氰酸酯，或当异氰酸酯是TDI或MDI或其组合时，至少约80和至多约105 ; 和（c）将异氰酸酯与催化剂多元醇混合物混合。

3. 发明授权

US09040657B2 Alkylene oxide polymerization using a double metal cyanide catalyst complex and a magnesium, Group 3-Group 15 metal or lanthanide series metal compound 有权
标题翻译：使用双金属氰化物催化剂络合物和镁，第3族第15族金属或镧系金属化合物的环氧烷聚合
公开(公告)号：US09040657B2
公开(公告)日：2015-05-26
申请号：US13990697
申请日：2011-12-18
申请人： David S. Laitar , David A. Babb , Carlos M. Villa , Richard Keaton , Jean-Paul Masy
发明人： David S. Laitar , David A. Babb , Carlos M. Villa , Richard Keaton , Jean-Paul Masy
IPC分类号： C08G59/68 , C08G65/00 , C08G65/26
CPC分类号： C08G65/2663 , C07C41/01 , C07C41/02 , C08G65/269 , C08G65/34
摘要： Alkylene oxide polymerizations are performed in the presence of a double metal cyanide polymerization catalyst and certain magnesium, Group 3-Group 15 metal or lanthanide series metal compounds. The presence of the magnesium, Group 3-Group 15 metal or lanthanide series metal compound provides several benefits including more rapid catalyst activation, faster polymerization rates and the reduction in the amount of ultra high molecular weight polymers that are formed. The catalyst mixture is unexpectedly useful in making polyethers having low equivalent weights.
摘要翻译：在双金属氰化物聚合催化剂和某些镁，第3族第15族金属或镧系金属化合物的存在下进行环氧烷聚合反应。镁，第3族 - 第15族金属或镧系金属化合物的存在提供了几个益处，包括更快速的催化剂活化，更快的聚合速率和所形成的超高分子量聚合物的量的减少。催化剂混合物意外地用于制备具有低当量重量的聚醚。

4. 发明授权

US08178645B2 Room temperature curable polymers and precursors thereof 有权
标题翻译：室温固化聚合物及其前体
公开(公告)号：US08178645B2
公开(公告)日：2012-05-15
申请号：US12668609
申请日：2008-07-10
申请人： Paul J. Popa , Zenon Lysenko , David A. Babb , William A. Koonce , Gary E. Spilman
发明人： Paul J. Popa , Zenon Lysenko , David A. Babb , William A. Koonce , Gary E. Spilman
IPC分类号： C08G18/42 , C08G63/00 , C08G18/71
CPC分类号： C08G18/4288 , C08G18/4269 , C08G18/4277 , C08G18/718 , C08G2190/00 , C09J175/06
摘要： A polyester polyol, referred to hereinafter as a MHMS polyol comprises fatty acid based mer units wherein at least about 80 weight percent of the fatty acid based mer units are from methyl 9 (10) hydroxymethylstearate, or is prepared from an oil having fatty acids or fatty acid esters which are at least about 80 weight percent oleic acid or esters thereof and which has an average hydroxyl functionality of from 1.5 to 4. A reaction product, referred to herein after as MHMS alkoxysilane prepolymer, is produced from at least one such MHMS polyol and at least one isocyanate functional silane. This prepolymer is moisture cured to form a silylated MHMS polymer.
摘要翻译：以下称为MHMS多元醇的聚酯多元醇包括脂肪酸基mer单元，其中至少约80重量％的脂肪酸基mer单元为9（10）羟甲基硬脂酸甲酯，或由具有脂肪酸或至少约80重量％的油酸或其酯，并且其平均羟基官能度为1.5-4的脂肪酸酯。本文中称为MHMS烷氧基硅烷预聚物的反应产物由至少一种这样的MHMS 多元醇和至少一种异氰酸酯官能的硅烷。将该预聚物水分固化以形成甲硅烷基化的MHMS聚合物。

5. 发明授权

US07960444B2 Vegetable oil based polyols and polyurethanes made therefrom 有权
标题翻译：植物油基多元醇和由其制成的聚氨酯
公开(公告)号：US07960444B2
公开(公告)日：2011-06-14
申请号：US10553767
申请日：2004-04-21
申请人： Zenon Lysenko , Alan K. Schrock , David A. Babb , Aaron Sanders , John Tsavalas , H. Ray Jouett , Larry Chambers , Charles Keillor , James H. Gilchrist
发明人： Zenon Lysenko , Alan K. Schrock , David A. Babb , Aaron Sanders , John Tsavalas , H. Ray Jouett , Larry Chambers , Charles Keillor , James H. Gilchrist
IPC分类号： C08G18/00 , C08G18/04 , C07C57/02
CPC分类号： C08G18/36 , C08G18/4018 , C08G18/4072 , C08G18/4288 , C08G18/4804 , C08G18/4841 , C08G18/4891 , C08G18/6696 , C08G2101/0008 , C08G2101/0025 , C08G2101/005 , C08G2101/0083
摘要： Polyols useful in the manufacture of polyurethanes are disclosed. The polyols are prepared by reacting a vegetable oil based (hydroxymethyl containing) monomer with a polyol, polyamine or aminoalcohol under vacuum.
摘要翻译：公开了可用于制造聚氨酯的多元醇。通过在真空下使基于植物油的（含羟甲基）单体与多元醇，多胺或氨基醇反应来制备多元醇。

6. 发明申请

US20110015293A1 POLYETHER NATURAL OIL POLYOLS AND POLYMERS THEREOF 审中-公开
标题翻译：聚醚天然油多元醇及其聚合物
公开(公告)号：US20110015293A1
公开(公告)日：2011-01-20
申请号：US12933293
申请日：2009-03-20
申请人： Hongming Ma , Jorge Jimenez , Dwight D. Latham , David A. Babb , Imran Munshi , Christopher Noakes
发明人： Hongming Ma , Jorge Jimenez , Dwight D. Latham , David A. Babb , Imran Munshi , Christopher Noakes
IPC分类号： C08J9/00 , C07C59/147 , C08G18/72
CPC分类号： C08G18/4804 , C08G18/4891 , C08G2101/0008 , C08G2101/005 , C08G2101/0083
摘要： A polyether NOP comprises at least two natural oil moieties separated by a molecular structure having at least about 19 ether groups or by a polyether molecular structure having an equivalent weight of at least about 480, said polyol referred to hereinafter as a polyether NOP. The polyether NOP is preferably prepared by a process comprising admixing at least one polyether initiator having an equivalent weight of at least about 480 or at least about 19 ether groups per active hydrogen group with at least one natural oil or derivative thereof under reaction conditions such that at least one polyether NOP is formed. The invention includes reaction products of the polyether NOP or combinations thereof, optionally and preferably in admixture with at least one other polyol which preferably includes at least one polyether polyol and at least one monomer reactive therewith, preferably at least one polyisocyanate to form a polyurethane, preferably in the form of a foam, especially a high resilience foam. The invention includes articles comprising at least one polyether NOP, at least one polymer thereof, or at least one foam thereof.
摘要翻译：聚醚NOP包含至少两个通过具有至少约19个醚基团的分子结构分开的天然油部分，或通过当量为至少约480的聚醚分子结构，所述多元醇在下文中称为聚醚NOP。聚醚NOP优选通过包括在反应条件下将每个活性氢基团当量至少约480或至少约19个醚基团的至少一种聚醚引发剂与至少一种天然油或其衍生物混合的方法制备，使得形成至少一种聚醚NOP。本发明包括聚醚NOP或其组合的反应产物，任选和优选与至少一种其它多元醇混合，其中多元醇优选包括至少一种聚醚多元醇和至少一种与其反应的单体，优选至少一种多异氰酸酯以形成聚氨酯，优选为泡沫形式，特别是高弹性泡沫。本发明包括包含至少一种聚醚NOP，至少一种聚合物或其至少一种泡沫的制品。

7. 发明申请

US20100298610A1 ALDEHYDE COMPOSITIONS DERIVED FROM SEED OILS 有权
标题翻译：从种子油中衍生的醛类组合物
公开(公告)号：US20100298610A1
公开(公告)日：2010-11-25
申请号：US12565446
申请日：2009-09-23
申请人： Zenon Lysenko , Donald L. Morrison , David A. Babb , Donald L. Bunning , Christopher W. Derstine , James H. Gilchrist , H. Ray Jouett , Kurt D. Olson , Wei-Jun Peng , Joe D. Phillips , Brian M. Roesch , Aaron W. Sanders , Alan K. Schrock , Pulikkottil J. Thomas , Jeffrey S. Kanel
发明人： Zenon Lysenko , Donald L. Morrison , David A. Babb , Donald L. Bunning , Christopher W. Derstine , James H. Gilchrist , H. Ray Jouett , Kurt D. Olson , Wei-Jun Peng , Joe D. Phillips , Brian M. Roesch , Aaron W. Sanders , Alan K. Schrock , Pulikkottil J. Thomas , Jeffrey S. Kanel
IPC分类号： C07C47/02
CPC分类号： C08G18/4891 , C07C67/31 , C07C67/347 , C07C69/675 , C07C69/716 , C07C69/732 , C07C69/738 , C08G18/4072 , C08G18/4804 , C08G18/4841 , C08G2101/0008 , C08G2101/005 , C08G2101/0083
摘要： An aldehyde composition derived by hydroformylation of a transesterified seed oil and containing a mixture of formyl-substituted fatty acids or fatty acid esters having the following composition by weight: greater than about 10 to less than about 95 percent monoformyl, greater than about 1 to less than about 65 percent diformyl, and greater than about 0.1 to less than about 10 percent triformyl-substituted fatty acids or fatty acid esters, and having a diformyl to triformyl weight ratio of greater than about 5/1; preferably, greater than about 3 to less than about 20 percent saturates; and preferably, greater than about 1 to less than about 20 percent unsaturates.
摘要翻译：通过酯交换种子油的加氢甲酰化衍生的醛组合物，并含有具有以下重量组成的甲酰取代的脂肪酸或脂肪酸酯的混合物：大于约10至小于约95％的单甲基，大于约1至少并且具有大于约65％的二甲酰基和大于约0.1至小于约10％的三甲酰基取代的脂肪酸或脂肪酸酯，并且具有大于约5/1的二甲酰基 - 三甲酰基重量比; 优选大于约3至小于约20％的饱和物; 并且优选大于约1至小于约20％的不饱和度。

8. 发明授权

US06627573B2 Expanded anionic compounds comprising hydroxyl or quiescent reactive functionality and catalyst activators therefrom 失效
标题翻译：包括羟基或静止反应性官能团的膨胀的阴离子化合物及其催化剂活化剂
公开(公告)号：US06627573B2
公开(公告)日：2003-09-30
申请号：US09904422
申请日：2001-07-12
申请人： David A. Babb , Richard E. Campbell, Jr. , David R. Neithamer , Grant B. Jacobsen , Edmund M. Carnahan
发明人： David A. Babb , Richard E. Campbell, Jr. , David R. Neithamer , Grant B. Jacobsen , Edmund M. Carnahan
IPC分类号： B01J3000
CPC分类号： C08F10/00 , C07F5/027 , C07F5/062 , C07F5/066 , C07F7/0803 , C08F4/65912 , C08F4/65916 , C08F4/6592 , C08F4/65927 , C08F210/16 , C08F4/61908 , C08F4/65908 , C08F210/14 , C08F2500/12
摘要： A compound useful as a cocatalyst or cocatalyst component, especially for use as an addition polymerization catalyst compound, corresponding to the formula: (A*+a)b(Z*J*j)−cd, wherein: A* is a cation of from 1 to 80, preferably 1 to 60 atoms, not counting hydrogen atoms, said A* having a charge +a, Z* is an anion group of from 1 to 50, preferably 1 to 30 atoms, not counting hydrogen atoms, further containing two or more Lewis base sites; J* independently each occurrence is a Lewis acid of from 1 to 80, preferably 1 to 60 atoms, not counting hydrogen atoms, coordinated to at least one Lewis base site of Z*, and optionally two or more such J* groups may be joined together in a moiety having multiple Lewis acidic functionality, j is a number from 2 to 12 and a, b, c, and d are integers from 1 to 3, with the proviso that a×b is equal to c×d, and provided further that one or more of A*, Z* or J* comprises a hydroxyl group or a polar group containing quiescent reactive functionality.
摘要翻译：用作助催化剂或助催化剂组分的化合物，特别是用作加成聚合催化剂化合物，其对应于下式：其中：A *是不计氢原子的1至80个，优选1至60个原子的阳离子，所述化合物 A *具有电荷+ a，Z *是1至50个，优选1至30个原子的阴离子基团，不计算氢原子，进一步含有两个或更多个路易斯碱基位点; J *各自独立地为路易斯酸 1至80个，优选1至60个原子，不计数氢原子，与Z *的至少一个路易斯碱碱基位点配位，并且任选地两个或多个这样的J *基团可以连接在具有多个路易斯酸官能团的部分中， j是2至12的数字，a，b，c和d是1至3的整数，条件是axb等于cxd，进一步提供A *，Z *或J *中的一个或多个包括羟基或含有静止反应性官能团的极性基团。

9. 发明授权

US5206422A Process for preparation of fluorinated carbonyl compounds 失效
标题翻译：氟化羰基化合物的制备方法
公开(公告)号：US5206422A
公开(公告)日：1993-04-27
申请号：US775326
申请日：1991-10-11
申请人： David A. Babb
发明人： David A. Babb
IPC分类号： C07C51/58 , C07C67/313
CPC分类号： C07C51/58 , C07C67/313
摘要： A process for the preparation of fluorinated carbonyl compounds from a fluorinated methyl or ethyl ether using tin tetrachloride as a catalyst. The fluorinated ether is contacted with the tin tetrachloride catalyst at a temperature between 0.degree. C. and 250.degree. C.
摘要翻译：一种使用四氯化锡作为催化剂由氟化甲基或乙醚制备氟化羰基化合物的方法。氟化醚与四氯化锡催化剂在0℃至250℃的温度下接触。

10. 发明授权

US5159038A Perfluorocyclobutane ring-containing polymers 失效
标题翻译：含全氟环丁烷环的聚合物
公开(公告)号：US5159038A
公开(公告)日：1992-10-27
申请号：US673882
申请日：1991-03-22
申请人： David A. Babb , W. Frank Richey , Katherine S. Clement , Bobby R. Ezzell
发明人： David A. Babb , W. Frank Richey , Katherine S. Clement , Bobby R. Ezzell
IPC分类号： C07C17/26 , C07C43/17 , C07C43/225 , C07C65/21 , C07C65/24 , C08F16/32 , C10M105/54 , C10M107/38
CPC分类号： C10M107/38 , C07C17/269 , C07C43/17 , C07C43/225 , C07C65/21 , C07C65/24 , C08F16/32 , C10M105/54 , C07C2103/18
摘要： A process for preparing a polymer having perfluorocyclobutane rings by the steps of (a) contacting monomers having at least two dimerizable perfluorovinyl groups; and (b) exposing the monomers to sufficient heat and for a sufficient time that a polymer containing perfluorocyclobutane rings is formed. The invention includes polymers having a backbone comprising hydrocarbyl groups, perfluorocyclobutane rings and non-carbon atoms and polymers of at least 10,000 molecular weight having repeating units [O-(CFR.sub.f).sub.n -O-perfluorocyclobutane].
摘要翻译：一种通过以下步骤制备具有全氟环丁烷环的聚合物的方法：（a）使具有至少两个可二聚的全氟乙烯基的单体接触; 和（b）将单体暴露于足够的热量并持续足够的时间，形成含有全氟环丁烷环的聚合物。本发明包括具有包含烃基，全氟环丁烷环和非碳原子的主链的聚合物和具有至少10,000分子量的具有重复单元[O-（CFRf）n-O-全氟环丁烷]的聚合物。

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