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    • 5. 发明授权
    • Method and apparatus for monitoring laser weld quality via plasma size
measurements
    • 通过等离子体尺寸测量来监测激光焊接质量的方法和装置
    • US5961859A
    • 1999-10-05
    • US956881
    • 1997-10-23
    • Mau-Song ChouChristopher C. ShihBryan W. Shirk
    • Mau-Song ChouChristopher C. ShihBryan W. Shirk
    • B23K31/00B23K26/00B23K26/02B23K26/03B23K26/20
    • B23K26/032
    • A method and apparatus for monitoring the quality of a laser process such as a welding process comprises monitoring the light emitted from the weld plasma above the surface of the workpiece being irradiated by the laser beam. The size of the plasma is determined from the light emission and compared to a predetermined value of the size as determined under process and workpiece conditions that produce welds of acceptable quality. Variations of the monitored plasma size greater than a preselected value can represent unacceptable welds. Such variations can be caused by changes in the laser beam power, the workpiece speed, laser focusing problems, insufficient shield gas flow, workpiece deformation and weld contamination. The process monitors the light emission from a selected range of wavelengths that correspond to the major emission peaks of the light spectrum. The process enables in-process control.
    • 用于监测诸如焊接工艺的激光工艺的质量的方法和装置包括监测从被激光束照射的工件表面上的焊接等离子体发射的光。 等离子体的尺寸由光发射确定,并且与在产生可接受质量的焊缝的工艺条件和工件条件下确定的尺寸的预定值进行比较。 所监测的等离子体尺寸大于预选值的变化可以表示不可接受的焊缝。 这种变化可以由激光束功率,工件速度,激光聚焦问题,屏蔽气体流量不足,工件变形和焊接污染的变化引起。 该过程监测来自对应于光谱的主要发射峰的所选波长范围的光发射。 该过程使得能够进行过程控制。
    • 6. 发明授权
    • Process to recover azide values from azide-based gas generating materials
    • 从叠氮化物气体发生材料中回收叠氮化物值的方法
    • US5433932A
    • 1995-07-18
    • US3557
    • 1993-01-13
    • John F. ClausenChristopher C. Shih
    • John F. ClausenChristopher C. Shih
    • A62D3/00A62B35/04B60R21/16C01B11/18C01B21/08C06B21/00B01D9/02
    • C06B21/0091C01B11/18C01B21/08Y10S149/124
    • In a process for recovering an alkali metal azide from a waste gas generating material containing the alkali metal azide and a metal oxide reactable with the azide, the gas generating material is mixed with a solvent for the alkali metal azide. This produces a slurry comprising (i) a solution comprising the solvent and the alkali metal azide, and (ii) the metal oxide. The slurry is separated into a liquid stream comprising primarily the solution and a sludge stream comprising primarily the metal oxide. The liquid stream is filtered in a filter to produce a filtrate which is substantially free of metal oxide and is then concentrated by evaporation of the solvent to produce crystals of the alkali metal azide. The separation may be carried out by a filter or centrifuge to produce a filter or centrifuge cake. The sludge obtained from the slurry is reslurried to recover additional azide, and the resulting slurry is again separated into a sludge and a liquid stream by a filter or centrifuge. The filtrate or centrate is recycled and can be used for dissolution of additional waste gas generating material.
    • 在从含有碱金属叠氮化物的废气产生材料和与叠氮化物反应的金属氧化物中回收碱金属叠氮化物的方法中,气体发生材料与碱金属叠氮化物的溶剂混合。 这产生浆料,其包含(i)包含溶剂和碱金属叠氮化物的溶液,和(ii)金属氧化物。 将浆料分离成主要包含溶液的液体物流和主要包含金属氧化物的污泥流。 将液体流在过滤器中过滤以产生基本上不含金属氧化物的滤液,然后通过蒸发溶剂浓缩以产生碱金属叠氮化物的晶体。 分离可以通过过滤器或离心机进行以产生过滤器或离心饼。 将从浆料获得的污泥重新浆化以回收另外的叠氮化物,并且通过过滤器或离心机将所得浆料再次分离成污泥和液体流。 滤液或浓缩液循环使用,可用于其他废气产生材料的溶解。