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1. 发明授权

US4798911A Catalyst composition and method for selective dehydrogenation 失效
标题翻译：催化剂组合物和选择性脱氢方法
公开(公告)号：US4798911A
公开(公告)日：1989-01-17
申请号：US75375
申请日：1987-07-20
申请人： Carl M. Lentz , Bruce L. Gustafson , Paul S. Wehner
发明人： Carl M. Lentz , Bruce L. Gustafson , Paul S. Wehner
IPC分类号： B01J23/89 , C07B35/04 , C07B61/00 , C07C5/00 , C07C5/32 , C07C5/333 , C07C11/02 , C07C37/06 , C07C39/15 , C07C41/18 , C07C43/215 , C07C45/65 , C07C47/548 , C07C49/794 , C07C51/347 , C07C63/64 , C07C69/76 , C07C69/94 , C07C317/14 , C07C5/367 , C07C39/12
CPC分类号： C07C41/18 , B01J23/8926 , C07C37/001 , C07C37/06 , C07C5/325 , C07C5/3337 , C07C67/297 , C07C67/317 , C07C2101/14 , C07C2521/18 , C07C2523/44 , C07C2523/72 , C07C2523/89
摘要： A method for selective dehydrogenation of a compound, comprising contacting a compound of the formula ##STR1## wherein each R.sup.1, R.sup.2, R.sup.3 and R.sup.4 is independently selected from the group consisting of H, (C.sub.1 -C.sub.20) alkyl, (C.sub.3 -C.sub.20) cycloalkyl, (C.sub.6 -C.sub.20) aryl, (C.sub.7 -C.sub.20) alkylaryl, (C.sub.7 -C.sub.20) aralkyl groups, as well as substituted (C.sub.1 -C.sub.20) alkyl, (C.sub.3 -C.sub.20) cycloalkyl, (C.sub.6 -C.sub.20) aryl, (C.sub.7 -C.sub.20) aralkyl and (C.sub.7 -C.sub.20) arylalkyl moieties, optionally further substituted with --OR, wherein R is R.sup.1, R.sup.2, R.sup.3 or R.sup.4 ; and wherein R.sup.1 and R.sup.2 or R.sup.3 and R.sup.4 may be joined as part of a ring structure, at a dehydrogenation temperature in the presence of a catalyst comprising about 0.01 wt %-19.9 wt % Pd and about 0.01 wt %-19.9 wt % Cu on a carbon support, wherein the total amount of (Pd+Cu) on the support is about 0.02 wt % to 20 wt %, the weight ratio of Pd:Cu is about 1:1 to 10:1, and the carbon support has a surface area of at least about 100 m.sup.2 /g and is essentially free of reactive sulfur.A selective dehydrogenation catalyst having the composition described supra is disclosed as is a method of preparing the same. This catalyst is highly selective for dehydrogenating a variety of substrates while minimizing the formation of unwanted hydrogenolysis by-products.
摘要翻译：一种化合物的选择性脱氢的方法，包括使下式化合物与其中每个R 1，R 2，R 3和R 4独立地选自H，（C 1 -C 20）烷基，（C 3 -C 20）环烷基，（C 6 -C 20）芳基，（C 7 -C 20）烷基芳基，（C 7 -C 20）芳烷基以及取代的（C 1 -C 20）烷基，（C 3 -C 20）环烷基，（C 6 -C 20） C7-C20）芳烷基和（C7-C20）芳烷基部分，任选进一步被-OR取代，其中R是R 1，R 2，R 3或R 4; 并且其中R 1和R 2或R 3和R 4可以作为环结构的一部分在脱氢温度下在催化剂存在下接合，所述催化剂包含约0.01重量％-19.9重量％的Pd和约0.01重量％-19.9重量％的Cu 碳载体，其中载体上的（Pd + Cu）的总量为约0.02重量％至20重量％，Pd：Cu的重量比为约1:1至10:1，并且碳载体具有表面积至少约100m 2 / g，基本上不含活性硫。作为其制备方法，公开了具有上述组成的选择性脱氢催化剂。该催化剂对于使各种底物脱氢而具有高选择性，同时最小化不想要的氢解副产物的形成。

2. 发明授权

US4847429A Synthesis of phenylhydroquinones 失效
标题翻译：苯基氢醌的合成
公开(公告)号：US4847429A
公开(公告)日：1989-07-11
申请号：US81209
申请日：1987-08-03
申请人： Carl M. Lentz , Bruce L. Gustafson , Dale E. Van Sickle , Joseph S. Bowers, Jr.
发明人： Carl M. Lentz , Bruce L. Gustafson , Dale E. Van Sickle , Joseph S. Bowers, Jr.
IPC分类号： B01J27/12 , B01J27/125 , B01J27/16 , B01J29/06 , B01J31/02 , B01J31/04 , B01J31/08 , C07B61/00 , C07C37/06 , C07C37/11 , C07C37/14 , C07C39/15 , C07C39/17 , C07C41/18 , C07C41/30 , C07C43/205 , C07C43/21 , C07C69/017 , C07C69/28 , C07C205/00 , C07C205/21 , C07C205/36 , C07C321/00
CPC分类号： C07C37/11 , C07C37/06 , C07C37/14 , C07C2101/14
摘要： Process is disclosed for the preparation of phenylhydroquinones by the alkylation of hydroquinone (or derivatives thereof) with the cyclohexyl moieties, cyclohexanol or cyclohexene (or derivatives thereof), followed by dehydrogenation of the intermediate cyclohexylhydroquinone.
摘要翻译：公开了通过用环己基部分，环己醇或环己烯（或其衍生物）烷基化氢醌（或其衍生物），然后中间体环己基氢醌脱氢来制备苯基氢醌的方法。

3. 发明申请

US20170211992A1 VISUAL AND ELECTRONICALLY READABLE TEMPERATURE INDICATOR 审中-公开
公开(公告)号：US20170211992A1
公开(公告)日：2017-07-27
申请号：US15415301
申请日：2017-01-25
申请人： Steve Yeager , Justine Gaston , Carl M. Lentz , Randall Lane
发明人： Steve Yeager , Justine Gaston , Carl M. Lentz , Randall Lane
IPC分类号： G01K7/20 , G01K11/12 , G01K11/06
摘要： Visual and electronically readable temperature indicators and methods of making the same have an electric circuit with a microchip and a bridge within the circuit, and a facing material over the electric circuit. The bridge includes either a single layer or multiple layers that include a conductive material, a phase change material having a pre-selected melt temperature, a binder, a first colorant that is soluble in the phase change material and/or a second colorant that is a special effect pigment. In operation, at temperatures below the pre-selected melt temperature, the bridge is electrically conductive, and at a temperature at or above the pre-selected melt temperature, the phase change material melts and dilutes the conductive material, so that the bridge is electrically non-conductive, and a color change occurs that is visible to the user through the facing material such as through a transparent window or in an absorbent material.

4. 发明申请

US20120175412A1 COMPUTING SYSTEMS AND METHODS FOR ELECTRONICALLY INDICATING THE ACCEPTABILITY OF A PRODUCT 有权
标题翻译：电子系统和电子显示产品可接受性的方法
公开(公告)号：US20120175412A1
公开(公告)日：2012-07-12
申请号：US13276543
申请日：2011-10-19
申请人： Frederick R. GRABINER , Carl M. Lentz , Emily Moore , Thaddeus Prusik , Nicholas Puro , Bruce-Erik Osborn
发明人： Frederick R. GRABINER , Carl M. Lentz , Emily Moore , Thaddeus Prusik , Nicholas Puro , Bruce-Erik Osborn
IPC分类号： G06F17/30
CPC分类号： G16H20/00 , G06F19/00 , G06F19/321 , G06F19/3462 , G06F19/3475 , G06K9/4652 , G06K9/6215 , G06K2009/4666 , G06Q10/0833 , G06Q10/087 , G06Q30/0623 , G06T7/73 , G06T7/90 , G07G1/0054 , G07G1/0081 , G16H10/00 , G16H15/00 , G16H40/20 , G16H40/67
摘要： In part, the invention relates to computing systems and methods for electronically indicating the acceptability of a product. An image capture and communication device may analyze a product label that includes one or more monitors, authentication elements, and identification elements. The image capture and communication device may determine the type and features of the monitors, authentication elements, and identification elements. The image capture and communication device may transmit data based on the type and features to a host server, which may transmit data associated with the host product to the image capture and communication device in, inter alia, the form of an acceptability report.
摘要翻译：部分地，本发明涉及用于电子地指示产品的可接受性的计算系统和方法。图像捕获和通信设备可以分析包括一个或多个监视器，认证元件和识别元件的产品标签。图像捕获和通信设备可以确定监视器，认证元件和识别元件的类型和特征。图像捕获和通信设备可以基于类型和特征将数据发送到主机服务器，主机服务器可以特别地以可接受性报告的形式将与主机产品相关联的数据传送到图像捕获和通信设备。

5. 发明申请

US20120079980A1 COLOR-CHANGING EMULSIONS FOR FREEZE INDICATORS 有权
标题翻译：冷冻指示剂的颜色变化乳液
公开(公告)号：US20120079980A1
公开(公告)日：2012-04-05
申请号：US13246392
申请日：2011-09-27
申请人： Dene H. TAYLOR , Carl M. Lentz , Dawn E. Smith
发明人： Dene H. TAYLOR , Carl M. Lentz , Dawn E. Smith
IPC分类号： G01D21/00 , G01N21/75
CPC分类号： G01K11/12 , G01K3/04 , G01K11/06
摘要： A color-changing emulsion for use in a freeze indicator can employ a dispersion medium, for example, an aqueous liquid, a first reactant phase and a second reactant phase, which two reactant phases can both be dispersed in the dispersion medium. The first reactant phase includes a hydrophobic liquid and a first reactant, for example, a color precursor such as a leuco dye. The second reactant phase can include a hydrophobic liquid, and includes, or can be, a second reactant, for example, a color developer such as a leuco dye developer. The first and second reactant phases can be essentially unmixed, and can be co-reactable to provide a color change. In response to a freezing temperature, the color-changing emulsion can coagulate and change color irreversibly. An intense color change can be obtained by using, for example, a suitable leuco dye precursor and developer.
摘要翻译：用于冷冻指示剂的变色乳液可以使用分散介质，例如水性液体，第一反应物相和第二反应物相，其中两个反应物相都可以分散在分散介质中。第一反应物相包括疏水性液体和第一反应物，例如着色前体如无色染料。第二反应物相可以包括疏水性液体，并且包括或可以是第二反应物，例如彩色显影剂，例如无色染料显影剂。第一和第二反应物相可以基本上不混合，并且可以共同反应以提供颜色变化。响应于冷冻温度，变色乳液可以不可逆地凝结和变色。通过使用例如合适的无色染料前体和显影剂可以获得强烈的颜色变化。

6. 发明授权

US5277767A Electrochemical synthesis of diaryliodonium salts 失效
标题翻译：二芳基碘盐的电化学合成
公开(公告)号：US5277767A
公开(公告)日：1994-01-11
申请号：US681589
申请日：1991-04-08
申请人： Michael R. Cushman , Carl M. Lentz , David D. Cornell
发明人： Michael R. Cushman , Carl M. Lentz , David D. Cornell
IPC分类号： C25B3/10 , C25B3/02 , C25B3/00
CPC分类号： C25B3/02
摘要： Electrochemical process for preparing diaryliodonium salts using a single compartment and a carbon anode. The process has high current efficiency and, optionally, increased para, para' regioselectivity. The process proceeds in the presence of a solvent such as acetic acid and an electrolyte such as a compound of fluorine or sulfuric acid.
摘要翻译：使用单个隔室和碳阳极制备二芳基碘鎓盐的电化学工艺。该方法具有高电流效率，并且可选地增加对位，对位选择性。该过程在溶剂如乙酸和诸如氟或硫酸的化合物的电解质的存在下进行。

7. 发明授权

US08354486B2 Co-crystallizable diacetylenic monomer compositions, crystal phases and mixtures, and related methods 有权
标题翻译：可共结构的二炔单体组合物，结晶相和混合物及相关方法
公开(公告)号：US08354486B2
公开(公告)日：2013-01-15
申请号：US12730835
申请日：2010-03-24
申请人： Elizabeth Castillo Martinez , Ray H. Baughman , Lee J. Hall , Mikhail Kozlov , Dawn E. Smith , Thaddeus Prusik , Carl M. Lentz
发明人： Elizabeth Castillo Martinez , Ray H. Baughman , Lee J. Hall , Mikhail Kozlov , Dawn E. Smith , Thaddeus Prusik , Carl M. Lentz
IPC分类号： C08F238/00 , G01D21/00 , C07C275/20 , C08F2/36
CPC分类号： C07C275/20 , C08F238/02 , G01N31/229
摘要： Solid polymerizable diacetylenic monomer compositions, including compositions co-crystallized from a diversity of solvent systems under diverse cooling conditions, can exhibit diffraction patterns associated with the color development reactivities of the compositions. High reactivity compositions are disclosed and high reactivity and low reactivity phases can be identified. A low angle powder X-ray diffraction peak can indicate the presence of one or more crystal phases in a composition. A fingerprint region can exhibit fingerprint patterns of diffraction peaks associated with different reactivities. Information about polymerization of the diacetylenic monomers is disclosed using 13C nuclear magnetic resonance (“NMR”) characterization. Diacetylenic monomer compositions useful in ambient condition indicators, for example time-temperature indicators are disclosed.
摘要翻译：固体可聚合二炔单体组合物，包括在不同冷却条件下从各种溶剂体系共结晶的组合物可以显示与组合物的显色反应性相关的衍射图。公开了高反应性组合物，并且可以鉴定出高反应性和低反应性相。低角度粉末X射线衍射峰可以指示组合物中存在一个或多个结晶相。指纹区域可以显示与不同反应性相关的衍射峰的指纹图谱。使用13C核磁共振（NMR）表征公开了关于二乙炔单体的聚合的信息。公开了用于环境条件指示剂的二乙炔单体组合物，例如时间 - 温度指示剂。

8. 发明授权

US4929737A Hydrogenation of halonitroaromatic compounds 失效
标题翻译：卤代芳族化合物的氢化
公开(公告)号：US4929737A
公开(公告)日：1990-05-29
申请号：US151726
申请日：1988-02-03
申请人： Carl M. Lentz , Edward T. Mullins , Charles L. Gibson
发明人： Carl M. Lentz , Edward T. Mullins , Charles L. Gibson
IPC分类号： B01J25/00 , C07B43/04 , C07B61/00 , C07C209/36 , C07C227/04 , C07C227/08 , C07C229/60 , C07C231/12 , C07C233/80 , C07C235/24 , C07C303/36 , C07C311/39 , C07D231/52
CPC分类号： C07D231/52 , C07C209/36 , C07C209/365 , C07C227/08 , C07C231/12 , C07C233/80 , C07C235/24 , C07C311/39
摘要： Disclosed is an improved process for the preparation of haloaromatic amines by the catalytic hydrogenation of halonitroaromatic compounds in the presence of a chromium-containing Raney cobalt catalyst. The catalyst gives good hydrogenation rates while minimizing formation of dehalogenated by-products.
摘要翻译：公开了一种通过在含铬的阮内钴催化剂的存在下通过卤代硝基芳族化合物的催化氢化来制备卤代芳族胺的改进方法。催化剂提供良好的氢化速率，同时最小化脱卤副产物的形成。

9. 发明授权

US4759833A Electrolytic method of simultaneously preparing diaryliodonium salt and alkoxide salt and method of preparing ester of an aromatic acid 失效
标题翻译：同时制备二芳基碘盐和醇盐的电解方法及芳香酸酯的制备方法
公开(公告)号：US4759833A
公开(公告)日：1988-07-26
申请号：US115303
申请日：1987-11-02
申请人： Carl M. Lentz , Michael R. Cushman , James R. Overton , David D. Cornell
发明人： Carl M. Lentz , Michael R. Cushman , James R. Overton , David D. Cornell
IPC分类号： C25B3/04 , C25B3/10 , C25C1/00
CPC分类号： C25B3/04 , C25B3/10
摘要： An electrolytic method for the simultaneous preparation of a diaryliodonium salt and an alkoxide salt comprises adding to the anode compartment of an electrolytic cell, comprised of an anode, a first electrolytic solution comprising an aromatic compound, an iodoaromatic compound, a solvent and a first organic salt; adding to the cathode compartment of the cell, comprised of a cathode, a second electrolytic solution comprising a hydroxyalkyl compound and a second organic salt; and applying to the anode and the cathode an electric potential, to form diaryliodonium salt in the anode compartment and an alkoxide salt in the cathode compartment.Esters of an aromatic acid are prepared by carbonylating an admixture of the diaryliodonium salt and the alkoxide salt by the addition of carbon monoxide thereto.
摘要翻译：用于同时制备二芳基碘盐和醇盐的电解方法包括将由阳极，包含芳族化合物的第一电解溶液，碘芳香族化合物，溶剂和第一有机物构成的电解池的阳极室盐; 加入电池的阴极室，包括阴极，包含羟烷基化合物和第二有机盐的第二电解溶液; 并向阳极和阴极施加电位，以在阳极室中形成二芳基碘鎓盐和在阴极室中形成醇盐。通过向其中加入一氧化碳羰基化二芳基碘盐和醇盐的混合物来制备芳族酸的酯。

10. 发明授权

US4594445A Carbonylation process for the production of aromatic acids and derivatives thereof 失效
标题翻译：用于生产芳香酸及其衍生物的羰基化方法
公开(公告)号：US4594445A
公开(公告)日：1986-06-10
申请号：US689419
申请日：1985-01-07
申请人： Carl M. Lentz , James R. Overton , David D. Cornell
发明人： Carl M. Lentz , James R. Overton , David D. Cornell
IPC分类号： C07C69/76
CPC分类号： C07C69/76
摘要： The present invention provides a process for the preparation of aryl carboxylic acids and derivatives thereof by the carbonylation of diaryliodonium salts. The diaryliodonium salts are reacted with carbon monoxide and water or an alcohol or amine in a base reaction medium having a pK.sub.b greater than about 8.
摘要翻译：本发明提供了通过二芳基碘鎓盐的羰基化制备芳基羧酸及其衍生物的方法。二芳基碘鎓盐与一氧化碳和水或醇或胺在pKb大于约8的碱性反应介质中反应。

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