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1. 发明授权

US5231171A Reactive dyes having an allylsulfonyl or propargylesulfonyl group 失效
标题翻译：具有聚乙二醇醚或丙烷磺酸基团的反应性染料
公开(公告)号：US5231171A
公开(公告)日：1993-07-27
申请号：US806262
申请日：1991-12-13
申请人： Claus Marschner , Matthias Niedenbrueck , Bernd Siegel , Manfred Patsch , Klaus Pandl
发明人： Claus Marschner , Matthias Niedenbrueck , Bernd Siegel , Manfred Patsch , Klaus Pandl
IPC分类号： C09B62/44 , C09B62/443 , C09B62/78
CPC分类号： C09B62/4401 , C09B62/443 , C09B62/78
摘要： Reactive dyes useful for dyeing or printing hydroxyl- or nitrogen-containing substrates have the formula ##STR1## where Rg is a radical of the formula ##STR2## Ar is the radical of a benzene or naphthalene ring, Z.sup.1 and Z.sup.2 are each hydrogen, substituted or unsubstituted C.sub.1 -C.sub.4 -alkyl, substituted or unsubstituted phenyl, C.sub.1 -C.sub.4 -alkoxy, carboxyl, C.sub.1 -C.sub.4 -alkoxycarbonyl, cyano, halogen or hydroxysulfonyl,Z.sup.3, Z.sup.4 and Z.sup.5 are each hydrogen, substituted or unsubstituted C.sub.1 -C.sub.4 -alkyl or substituted or unsubstituted phenyl,U is a group which is detachable under alkaline reaction conditions,X is in case a) the radical of a chromophore or in case b) the radical of a coupling component to which may additionally be attached, via an azo bridge, the radical of a diazo component and which may have additional reactive groups, andL is in case a) a bridge member or in case b) an azo bridge.
摘要翻译：可用于染色或印刷含羟基或含氮底物的活性染料具有式（I）其中R g是下式的基团：其中R a是苯或萘环的基团，Z 1和Z 2分别为氢，取代或未取代的C 1 -C 4 - 烷基，取代或未取代的苯基，C 1 -C 4 - 烷氧基，羧基，C 1 -C 4 - 烷氧基羰基，氰基，卤素或羟基磺酰基，Z 3，Z 4和Z 5各自为氢， C 4 - 烷基或取代或未取代的苯基，U是在碱性反应条件下可分离的基团，X是在a）发色团的基团的情况下，或在b）可以另外附着的偶合组分的基团的情况下，通过偶氮桥，重氮组分的基团并且可以具有额外的反应性基团，并且L是在a）桥构件的情况下或在b）偶氮桥中的情况下。

2. 发明授权

US5149789A Reactive dyes with two or three nitrogen-containing haloheterocycles as reactive system 失效
标题翻译：具有两种或三种含有硝酸的氢化物作为反应体系的反应性染料
公开(公告)号：US5149789A
公开(公告)日：1992-09-22
申请号：US490710
申请日：1990-03-08
申请人： Joerg L. Jessen , Klaus Pandl , Hermann Loeffler , Bernd Siegel , Manfred Patsch
发明人： Joerg L. Jessen , Klaus Pandl , Hermann Loeffler , Bernd Siegel , Manfred Patsch
IPC分类号： C09B50/00 , C09B62/04 , C09B62/08 , D06P3/10 , D06P3/66
CPC分类号： C09B62/043
摘要： Reactive dyes of the formula ##STR1## where 1 is 0 or 1,n is 0 or 1,E is nitrogen or C--Cl,A is the radical of an azo dye attached to the triazine ring via an imino or C.sub.1 -C.sub.4 -alkylimino group,B--if E is nitrogen--is the radical of an azo dye or of a formazan dye which in either case is bonded to the triazine ring via an imino or C.sub.1 -C.sub.4 -alkylimino group or else--if n is 0--is fluorine, chlorine or unsubstituted or substituted amino, or --if E is C--C1--is fluorine, chlorine or methyl,X.sup.1 and X.sup.2 are independently of the other fluorine or chlorine,X.sup.3 is fluorine or chlorine or else--if E is C--Cl--methylsulfonyl andZ.sup.1 and Z.sup.2 are independently of the other a radical of the formula ##STR2## where L.sup.3 and L.sup.4 are independently of the other hydrogen or unsubstituted or substituted C.sub.1 -C.sub.4 -alkyl,with the proviso that l and n are not simultaneously 0 and that, if E is C--Cl or if n is 0 and Z.sup.1 is the radical of the formula ##STR3## where L.sup.3 and L.sup.4 are each as defined above, A may also be the radical of a formazan dye which is bonded to the triazine ring via an imino or C.sub.1 -C.sub.4 -alkylimino group, are useful for dyeing or printing hydroxyl- or nitrogen-containing substrates.
摘要翻译：式1的反应性染料，其中1为0或1，n为0或1，E为氮或C-Cl，A为通过亚氨基或C 1 -C 4烷基连接到三嗪环上的偶氮染料的基团，烷基亚氨基，B-如果E是氮 - 是偶氮染料或甲an染料的基团，其在任一情况下通过亚氨基或C 1 -C 4 - 烷基亚氨基键合到三嗪环，否则 - 如果n是0- 是氟，氯或未取代或取代的氨基，或 - 如果E是C-C1 - 是氟，氯或甲基，则X1和X2独立于其他氟或氯，X3是氟或氯，或者 - 如果E是C -Cl-甲基磺酰基，Z 1和Z 2独立地为下式的基团：其中L 3和L 4独立于另一个氢或未取代或取代的C 1 -C 4 - 烷基，其中条件是l和n不同时为0，并且如果E是C-Cl或如果n是0，并且Z1是式“IMAGE”的基团，其中L3和L4各自如上所定义，A也可以是t 通过亚氨基或C 1 -C 4烷基亚胺基与三嗪环结合的甲an染料的基团可用于染色或印刷含羟基或含氮基底。

3. 发明授权

US5380941A Preparation of aromatic ureas which contain a thioether or sulfonyl group 失效
标题翻译：含有硫醚或磺酰基的芳香脲的制备
公开(公告)号：US5380941A
公开(公告)日：1995-01-10
申请号：US130176
申请日：1993-10-01
申请人： Bernd Siegel , Manfred Patsch
发明人： Bernd Siegel , Manfred Patsch
IPC分类号： C07C315/04 , C07C317/04 , C07C317/28 , C07C319/20 , C07C323/12 , C07C323/44 , C07D295/20 , C07C275/28 , C07C273/18
CPC分类号： C07C323/44 , C07C317/28
摘要： A process for preparing ureas of the formula ##STR1## where the ring A can be substituted and benzo-fused andn is 0 or 2,R.sup.4 and R.sup.5 are hydrogen, C.sub.1 -C.sub.4 -alkyl or phenyl,L is unsubstituted or substituted C.sub.2 -C.sub.4 -alkylene, or NR.sup.5 and L are together the radical of the formula ##STR2## and Z is hydroxyl or a radical which can be eliminated under alkaline reaction conditions,by reacting a phenylurea of the formula ##STR3## where R.sup.4 and the ring A each have the abovementioned meanings, with an amine of the formula ##STR4## where n, R.sup.5, L and Z each have the abovementioned meanings, at from 80.degree. to 180.degree. C. in the presence or absence of an inert diluent is described.
摘要翻译：其中环A可以被取代和苯并稠合并且n是0或2，R4和R5是氢，C1-C4-烷基或苯基，L是未取代的或取代的C2- C 4 - 亚烷基，或NR 5和L一起是式“基团”，Z是羟基或可以在碱性反应条件下被除去的基团，通过使式（Ia）的苯基脲与环A 各自具有上述含义，在存在或不存在惰性稀释剂的情况下，使用式为“IMAGE”的胺，其中n，R5，L和Z各自具有上述含义，80至180℃。

4. 发明授权

US5276148A Phenylazobenzenes or naphthylazobenzenes having a plurality of fiber-reactive groups 失效
标题翻译：具有多个纤维反应性基团的苯基偶氮苯或萘基偶氮苯
公开(公告)号：US5276148A
公开(公告)日：1994-01-04
申请号：US886835
申请日：1992-05-22
申请人： Bernd Siegel , Manfred Patsch
发明人： Bernd Siegel , Manfred Patsch
IPC分类号： C09B62/51 , C09B62/44 , C09B62/447 , C09B62/507 , C09B62/513 , C09B62/006 , D06P1/38
CPC分类号： C09B62/4401 , C09B62/447 , C09B62/507
摘要： Reactive dyes of the formula ##STR1## where n is 0 or 1,R.sup.1, R.sup.2 and R.sup.3 are each hydrogen, C.sub.1 -C.sub.4 -alkyl or phenyl,A is unsubstituted or substituted C.sub.2 -C.sub.8 -alkylene,Y is vinyl or a radical of the formula --CH.sub.2 --CH.sub.2 --Q, whereQ is a group which can be eliminated under alkaline reaction conditions,D.sup.1 is phenyl or naphthyl, where these radicals may be substituted,D.sup.2 is phenylene or naphthylene, where these radicals may be substituted, andZ is a reactive radical,with the proviso thata) n is zero when D.sup.1 is substituted by unsubstituted or substituted phenylazo or by unsubstituted or substituted naphthylazo andb) the reactive radical Z is not devised from the triazine series when n is zero and D.sup.1 is dihydroxysulfonylphenyl or trihydroxysulfonylnaphthyl,are used for dyeing and printing organic substrates containing hydroxyl groups or nitrogen atoms.
摘要翻译：其中n为0或1，R1，R2和R3的式为“IMAGE”的活性染料为氢，C1-C4-烷基或苯基，A为未取代或取代的C2-C8-亚烷基，Y为乙烯基或式为-CH 2 -CH 2 -Q，其中Q为可在碱性反应条件下除去的基团，D1为苯基或萘基，其中这些基团可以被取代，D2为亚苯基或亚萘基，其中这些基团可以被取代，和 Z是反应性基团，条件是当D1被未取代或取代的苯偶氮或未取代或取代的萘基偶氮取代时，a）n为零; b）当n为零时，并未设计出来自三嗪系列的反应性基团Z 是二羟基磺酰基苯基或三羟基磺酰基萘，用于染色和印刷含有羟基或氮原子的有机底物。

5. 发明授权

US5449762A Phenylazo- or naphthylazobenzenes having thioether groups 失效
标题翻译：具有硫醚基团的苯基或萘基偶氮苯
公开(公告)号：US5449762A
公开(公告)日：1995-09-12
申请号：US382180
申请日：1995-02-01
申请人： Matthias Wiesenfeldt , Bernd Siegel , Manfred Patsch
发明人： Matthias Wiesenfeldt , Bernd Siegel , Manfred Patsch
IPC分类号： C09B62/513 , C07D251/50 , C09B62/09 , C09B62/44 , D06P1/38
CPC分类号： C09B62/09 , C07D251/50 , C09B62/4411 , C09B62/4415
摘要： Reactive dyes of the formula I ##STR1## where n is 0 or 1R.sup.1, R.sup.2 and R.sup.3 are in each case hydrogen, C.sub.1 -C.sub.4 -alkyl or phenyl,R.sup.4 is fluorine, chlorine, bromine, C.sub.1 -C.sub.4 -alkylsulfonyl, phenylsulfonyl or a radical of the formula ##STR2## L is a bridge member, A is unsubstituted or substituted C.sub.2 -C.sub.8 -alkylene,Y is vinyl or a radical of the formula --CH.sub.2 --CH.sub.2 --Q, Q being a group which can be removed under alkaline reaction conditions, andD is phenyl or naphthyl, it being possible for these radicals to be substituted, and a process for preparing reactive dyes by oxidation of the abovementioned compounds are described.
摘要翻译：式I的反应性染料，其中n为0或1，R 1，R 2和R 3各自为氢，C 1 -C 4 - 烷基或苯基，R 4为氟，氯，溴，C 1 -C 4 - 烷基磺酰基，苯基磺酰基或下式的基团是桥连基团，A是未取代的或取代的C 2 -C 8 - 亚烷基，Y是乙烯基或式-CH 2 -CH 2 -Q基，Q是可以在碱性反应条件下除去，D是苯基或萘基，这些基团可以被取代，并描述了通过氧化上述化合物制备活性染料的方法。

6. 发明授权

US5245020A Reactive dyes with two or three nitrogen-containing haloheterocycles as reactive system 失效
标题翻译：具有两个或三个含氮卤素杂环的活性染料作为反应体系
公开(公告)号：US5245020A
公开(公告)日：1993-09-14
申请号：US853518
申请日：1992-03-18
申请人： Joerg L. Jessen , Klaus Pandl , Hermann Loeffler , Bernd Siegel , Manfred Patsch
发明人： Joerg L. Jessen , Klaus Pandl , Hermann Loeffler , Bernd Siegel , Manfred Patsch
IPC分类号： C09B62/04
CPC分类号： C09B62/043
摘要： Reactive dyes of the formula ##STR1## where l is 0 or 1,n is 0 or 1,E is nitrogen or C--ClA is the radical of an azo dye attached to the triazine ring via an imino or C.sub.1 -C.sub.4 -alkylimido group,B--if E is nitrogen--is the radical of an azo dye or of a formazan dye which in either case is bonded to the triazine ring via an imino of C.sub.1 -C.sub.4 -alkylimino group or else--if n is 0--is fluorine, chlorine or unsubstituted or substituted amino, or--if E is C--Cl--is fluorine, chlorine or methyl,X.sup.1 and X.sup.2 are independently of the other fluorine or chlorine,X.sup.3 is fluorine or chlorine or else--if E is C--Cl--methylsulfonyl andZ.sup.1 and Z.sup.2 are independently of the the other a radical of the formula ##STR2## where L.sup.3 and L.sup.4 are independently of the other hydrogen or unsubstituted or substituted C.sub.1 -C.sub.4 -alkyl,with the proviso that l and n are not simultaneously 0 and that, if E is C--Cl or if n is 0 and Z.sup.1 is the radical of the formula ##STR3## where L.sup.3 and L.sup.4 are each as defined above, A may also be the radical of a formazan dye which is bonded to the triazine ring via an imino or C.sub.1 -C.sub.4 -alkylimino group, are useful for dyeing or printing hydroxyl- or nitrogen-containing substrates.
摘要翻译：其中l为0或1的反应性染料，其中l为0或1，n为0或1，E为氮或C-Cl为经由亚氨基或C 1 -C 4烷基亚氨基连接到三嗪环上的偶氮染料的基团基团，B-如果E是氮，则是偶氮染料或甲an染料的基团，在任一情况下，通过C 1 -C 4 - 烷基亚氨基的亚氨基键合到三嗪环，或者 - 如果n是0- 氟，氯或未取代或取代的氨基，或 - 如果E是C-Cl-是氟，氯或甲基，则X1和X2独立于其它氟或氯，X3是氟或氯，或者 - 如果E是C- Cl-甲基磺酰基，Z 1和Z 2独立地为下式的基团：其中L 3和L 4独立于另一个氢或未取代或取代的C 1 -C 4 - 烷基，条件是 l和n不同时为0，并且如果E是C-Cl，或者如果n是0，并且Z1是式“IMAGE”的基团，其中L3和L4各自如上定义，则A也可以是通过亚氨基或C 1 -C 4烷基亚胺基与三嗪环结合的甲an染料的基团可用于染色或印刷含羟基或含氮基底。

7. 发明授权

US5225595A Arylsulfonyl compounds with unsaturated radicals 失效
标题翻译：具有不饱和基团的芳基磺酰基化合物
公开(公告)号：US5225595A
公开(公告)日：1993-07-06
申请号：US971270
申请日：1992-11-04
申请人： Bernd Siegel , Claus Marschner , Manfred Patsch
发明人： Bernd Siegel , Claus Marschner , Manfred Patsch
IPC分类号： C07C317/14 , C07C317/32 , C07C317/36 , C07C317/40 , C09B62/447 , C09B62/82
CPC分类号： C07C317/14 , C07C317/32 , C07C317/36 , C07C317/40 , C09B62/447 , C09B62/82
摘要： Sulfonyl compounds of the formula ##STR1## where Ar is the radical of a benzene or naphthalene ring,R.sup.1 and R.sup.2 are each hydrogen, substituted or unsubstituted C.sub.1 -C.sub.4 -alkyl, substituted or unsubstituted phenyl, C.sub.1 -C.sub.4 -alkoxy, carboxyl, C.sub.1 -C.sub.4 -alkoxycarbonyl, cyano, halogen or hydroxysulfonyl,R.sup.3 is nitro, amino, C.sub.1 -C.sub.4 -alkanoylamino or benzoylamino, andR.sup.4 is a radical of the formula ##STR2## where X.sup.1, X.sup.2 and X.sup.3 are each hydrogen, substituted or unsubstituted C.sub.1 -C.sub.4 -alkyl or substituted or unsubstituted phenyl, andX.sup.4 is a group which is detachable under alkaline conditions,either in the free form or in the form of their salts, are useful for synthesizing reactive dyes.
摘要翻译：式（I）的磺酰化合物其中Ar是苯或萘环的基团，R 1和R 2各自为氢，取代或未取代的C 1 -C 4 - 烷基，取代或未取代的苯基，C 1 -C 4 - 烷氧基，羧基，C 1 -C 4 - 烷氧基羰基，氰基，卤素或羟基磺酰基，R 3是硝基，氨基，C 1 -C 4 - 烷酰基氨基或苯甲酰基氨基，R 4是下式的基团：其中X 1，X 2和X 3各自为氢，取代或未取代的C1-C4烷基或取代或未取代的苯基，X4是在碱性条件下以游离形式或其盐形式可分离的基团，可用于合成活性染料。

8. 发明授权

US5091516A Phenyl- or naphthylazobenzenes with multiple reactive groups and intermediates therefor 失效
标题翻译：具有多种反应性组合的苯乙烯或萘二甲酸酐及其中间体
公开(公告)号：US5091516A
公开(公告)日：1992-02-25
申请号：US608842
申请日：1990-11-05
申请人： Bernd Siegel , Manfred Patsch
发明人： Bernd Siegel , Manfred Patsch
IPC分类号： C09B62/008 , C07C317/28 , C09B62/44
CPC分类号： C09B62/4413 , C07C317/28
摘要： Reactive dyes useful for dyeing or printing hydroxyl- or amino-containing organic substrates have the formula ##STR1## where R.sup.1, R.sup.2 and R.sup.3 are each hydrogen, C.sub.1 -C.sub.4 -alkyl or phenyl,R.sup.4 is C.sub.1 -C.sub.4 -alkoxy, phenoxy or a radical of the formula NL.sup.1 L.sup.2, where L.sup.1 and L.sup.2 are each substituted or unsubstituted C.sub.1 -C.sub.4 -alkyl or substituted or unsubstituted phenyl, or L.sup.1 and L.sup.2 together combine with the nitrogen atom joining them to form a heterocyclic radical, or L.sup.1 may also be hydrogen,R.sup.5 is fluorine, chlorine, bromine, C.sub.1 -C.sub.4 -alkylsulfonyl, phenylsulfonyl or a radical of the formula ##STR2## A is substituted or unsubstituted C.sub.2 -C.sub.8 -alkylene, Y is vinyl or a radical of the formula --CH.sub.2 --CH.sub.2 --Q, where Q is a group which is detachable under alkaline reaction conditions, andD is phenyl or naphthyl, which may both be substituted,and are preparable from phenylenediamine intermediates of the formula ##STR3## where X is hydroxyl or halogen and R.sup.1, R.sup.2, R.sup.3 and A are each as defined above.
摘要翻译：可用于染色或印刷含羟基或氨基的有机底物的活性染料具有式“IMAGE”，其中R 1，R 2和R 3各自为氢，C 1 -C 4烷基或苯基，R 4为C 1 -C 4 - 烷氧基，苯氧基或式NL1L2的基团，其中L1和L2各自为取代或未取代的C1-C4-烷基或取代或未取代的苯基，或L1和L2与连接它们的氮原子一起形成杂环基，或者L1也可以是氢 R 5是氟，氯，溴，C 1 -C 4 - 烷基磺酰基，苯基磺酰基或下式基团A是取代或未取代的C 2 -C 8 - 亚烷基，Y是乙烯基或式-CH 2 -CH 2 - Q，其中Q是在碱性反应条件下可分离的基团，D是可以被取代的苯基或萘基，并且可由式为“IMAGE”的苯二胺中间体制备，其中X是羟基或卤素，R 1，R 2 ，R3和A各自如上所定义。

9. 发明授权

US5428140A Preparation of phenylazo- or naphthylazobenzenes having thioether groups 失效
标题翻译：具有硫醚基团的苯偶氮或萘基偶氮苯的制备
公开(公告)号：US5428140A
公开(公告)日：1995-06-27
申请号：US254764
申请日：1994-06-06
申请人： Matthias Wiesenfeldt , Bernd Siegel , Manfred Patsch
发明人： Matthias Wiesenfeldt , Bernd Siegel , Manfred Patsch
IPC分类号： C09B62/513 , C07D251/50 , C09B62/09 , C09B62/44 , C09B43/06 , C09B62/08 , C09B62/507
CPC分类号： C09B62/09 , C07D251/50 , C09B62/4411 , C09B62/4415
摘要： Reactive dyes of the formula ##STR1## where n is 0 or 1R.sup.1, R.sup.2 and R.sup.3 are in each case hydrogen, C.sub.1 -C.sub.4 -alkyl or phenyl,R.sup.4 is fluorine, chlorine, bromine, C.sub.1 -C.sub.4 -alkylsulfonyl, phenylsulfonyl or a radical of the formula ##STR2## L is a bridge member, A is unsubstitued or substituted C.sub.2 -C.sub.8 -alkylene,Y is vinyl or a radical of the formula --CH.sub.2 --CH.sub.2 --Q, Q being a group which can be removed under alkaline reaction conditions, andD is phenyl or naphthyl, it being possible for these radicals to be substituted,and a process for preparing reactive dyes by oxidation of the abovementioned compounds are described.
摘要翻译：其中n为0或1个R 1，R 2和R 3各自为氢，C 1 -C 4 - 烷基或苯基，R 4为氟，氯，溴，C 1 -C 4 - 烷基磺酰基，苯基磺酰基或下式基团L是桥连构件，A是未取代的或取代的C 2 -C 8 - 亚烷基，Y是乙烯基或式-CH 2 -CH 2 -Q基，Q是可以在碱性反应条件下除去，D是苯基或萘基，这些基团可以被取代，并描述了通过氧化上述化合物制备活性染料的方法。

10. 发明授权

US5182371A Doubled phenyl- or naphthyl-azobenzenes having a plurality of reactive groups and intermediates thereof 失效
标题翻译：具有多重反应性组合的双酚 - 亚苄基酯及其中间体
公开(公告)号：US5182371A
公开(公告)日：1993-01-26
申请号：US835484
申请日：1992-02-14
申请人： Bernd Siegel , Manfred Patsch
发明人： Bernd Siegel , Manfred Patsch
IPC分类号： C09B62/513 , C07C317/18 , C07C317/28 , C09B62/44
CPC分类号： C07C317/28 , C09B62/4415
摘要： The reactive dyes have the formula ##STR1## where n is 0 or 1,R.sup.1, R.sup.2 and R.sup.3 are each hydrogen, C.sub.1 -C.sub.4 -alkyl or phenyl,R.sup.4 is fluorine, chlorine, bromine, C.sub.1 -C.sub.4 -alkylsulfonyl, phenylsulfonyl or a radical of the formula ##STR2## L is a bridgemember, A is substituted or unsubstituted C.sub.2 -C.sub.8 -alkylene,Y is vinyl or a radical of the formula --CH.sub.2 --CH.sub.2 --Q, where Q is a group which is detachable under alkaline reaction conditions, andD is phenyl or naphthyl, which may each be substituted.The present dyes are useful in dyeing or printing hydroxyl- or nitrogen-containing fibres.
摘要翻译：活性染料具有式（I）其中n为0或1，R1，R2和R3分别为氢，C1-C4-烷基或苯基，R4为氟，氯，溴，C1-C4 - 烷基磺酰基，苯基磺酰基或下式的基团L是桥连基团，A是取代或未取代的C 2 -C 8 - 亚烷基，Y是乙烯基或式-CH 2 -CH 2 -Q基团，其中Q是基团其在碱性反应条件下是可分离的，D是苯基或萘基，其各自可被取代。本染料可用于染色或印刷含羟基或含氮纤维。

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