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    • 3. 发明授权
    • Thermosensitive recording medium
    • 热敏记录介质
    • US08492308B2
    • 2013-07-23
    • US12674296
    • 2008-08-21
    • Tatsuyuki KuriharaTatsuo NagaiYoshimi MidorikawaAkihito OginoMamoru SugaYoshimune Aosaki
    • Tatsuyuki KuriharaTatsuo NagaiYoshimi MidorikawaAkihito OginoMamoru SugaYoshimune Aosaki
    • B41M5/333
    • B41M5/3336B41M5/3335B41M5/426B41M5/44B41M2205/04B41M2205/38B41M2205/40
    • The present invention provides a thermosensitive recording medium with excellent color developing sensitivity, moist heat resistance and plasticizer resistance, as well as excellent heat resistance, background coloring, light resistance and the like in the printed image.A diphenyl sulfone derivative containing a hydroxyl group on one end and an alkoxy group on the other end has a higher melting point than the one containing hydroxyl groups on both ends. As a result, the thermosensitive recording medium obtained using the diphenyl sulfone derivative as the color developing agent in the thermosensitive color developing layer has excellent heat resistance. However the color developing sensitivity of the thermosensitive recording medium generally declines simultaneously, when a color developing agent with a high melting point is ordinarily used. The thermosensitive recording medium of the present invention that uses a combination of the diphenyl sulfone derivative and a specific phenol derivative in the thermosensitive color developing layer has a good color developing sensitivity and an improved balance among the properties such as moist heat resistance, plasticizer resistance and the like.
    • 本发明提供了在印刷图像中具有优异的显色灵敏度,耐湿热性和耐增塑剂性以及优异的耐热性,背景着色,耐光性等的热敏记录介质。 一端含有羟基,另一端含有烷氧基的二苯砜衍生物的熔点比两末端羟基的熔点高。 结果,在热敏显色层中使用二苯砜衍生物作为彩色显影剂获得的热敏记录介质具有优异的耐热性。 然而,当通常使用具有高熔点的彩色显影剂时,热敏记录介质的显色灵敏度通常会同时下降。 在热敏显色层中使用二苯砜衍生物和特定苯酚衍生物的组合的本发明的热敏记录介质具有良好的显色灵敏度,并且在诸如耐湿热性,耐增塑剂性和 类似。
    • 4. 发明申请
    • THERMOSENSITIVE RECORDING MEDIUM
    • 耐热记录介质
    • US20110130281A1
    • 2011-06-02
    • US12674296
    • 2008-08-21
    • Tatsuyuki KuriharaTatsuo NagaiYoshimi MidorikawaAkihito OginoMamoru SugaYoshimune Aosaki
    • Tatsuyuki KuriharaTatsuo NagaiYoshimi MidorikawaAkihito OginoMamoru SugaYoshimune Aosaki
    • B41M5/333B41M5/323B41M5/337
    • B41M5/3336B41M5/3335B41M5/426B41M5/44B41M2205/04B41M2205/38B41M2205/40
    • The present invention provides a thermosensitive recording medium with excellent color developing sensitivity, moist heat resistance and plasticizer resistance, as well as excellent heat resistance, background coloring, light resistance and the like in the printed image.A diphenyl sulfone derivative containing a hydroxyl group on one end and an alkoxy group on the other end has a higher melting point than the one containing hydroxyl groups on both ends. As a result, the thermosensitive recording medium obtained using the diphenyl sulfone derivative as the color developing agent in the thermosensitive color developing layer has excellent heat resistance. However the color developing sensitivity of the thermosensitive recording medium generally declines simultaneously, when a color developing agent with a high melting point is ordinarily used. The thermosensitive recording medium of the present invention that uses a combination of the diphenyl sulfone derivative and a specific phenol derivative in the thermosensitive color developing layer has a good color developing sensitivity and an improved balance among the properties such as moist heat resistance, plasticizer resistance and the like.
    • 本发明提供了在印刷图像中具有优异的显色灵敏度,耐湿热性和耐增塑剂性以及优异的耐热性,背景着色,耐光性等的热敏记录介质。 一端含有羟基,另一端含有烷氧基的二苯砜衍生物的熔点比两末端羟基的熔点高。 结果,在热敏显色层中使用二苯砜衍生物作为彩色显影剂获得的热敏记录介质具有优异的耐热性。 然而,当通常使用具有高熔点的彩色显影剂时,热敏记录介质的显色灵敏度通常会同时下降。 在热敏显色层中使用二苯砜衍生物和特定苯酚衍生物的组合的本发明的热敏记录介质具有良好的显色灵敏度,并且在诸如耐湿热性,耐增塑剂性和 类似。
    • 7. 发明授权
    • Electrolysis method
    • 电解法
    • US08313637B2
    • 2012-11-20
    • US12934194
    • 2008-12-26
    • Minoru UchidaTatsuo NagaiShunichi Kanamori
    • Minoru UchidaTatsuo NagaiShunichi Kanamori
    • B01D59/40C02F1/461C25F1/00
    • C25B1/285G03F7/423
    • A wear of an electrode is prevented as much as possible, thereby efficiently electrolyzing a sulfuric acid solution and the like. An electrolysis method includes: passing an electrolytic solution through an electrolysis cell including at least a pair of an anode and a cathode; and supplying the electrodes with an electric power, so as to electrolyze the electrolytic solution, wherein a viscosity of the electrolytic solution is set in a range in response to a current density upon the electric power supply to carry out the electrolysis. The viscosity of a sulfuric acid solution as the electrolytic solution is equal to or less than 10 cP when the current density is equal to or less than 50 A/dm2, the viscosity of the sulfuric acid solution is equal to or less than 8 cP when the current density is from more than 50 to 75 A/dm2, and the viscosity of the sulfuric acid solution is equal to or less than 6 cP when the current density is from more than 75 to 100 A/dm2. Particularly when a highly-concentrated sulfuric acid solution is electrolyzed at a high current density using diamond electrodes, the electrolysis process can be carried out highly efficiently while a wear of the electrode is reduced.
    • 尽可能地防止电极的磨损,从而有效地电解硫酸溶液等。 电解方法包括:使电解液通过包括至少一对阳极和阴极的电解槽; 以及向所述电极供电,以便电解所述电解液,其中所述电解液的粘度响应于所述电源上的电流密度而设定在一定范围内以进行所述电解。 当电流密度等于或小于50A / dm 2时,作为电解液的硫酸溶液的粘度等于或小于10cP,硫酸溶液的粘度等于或小于8cP,当 电流密度为50〜75A / dm 2,当电流密度为75〜100A / dm 2时,硫酸溶液的粘度为6cP以下。 特别是当使用金刚石电极以高电流密度电解高浓度硫酸溶液时,可以高效地进行电解处理,同时降低电极的磨损。
    • 9. 发明申请
    • ELECTROLYSIS METHOD
    • 电解法
    • US20110017606A1
    • 2011-01-27
    • US12934194
    • 2008-12-26
    • Minoru UchidaTatsuo NagaiShunichi Kanamori
    • Minoru UchidaTatsuo NagaiShunichi Kanamori
    • C25B15/02C25B1/00
    • C25B1/285G03F7/423
    • A wear of an electrode is prevented as much as possible, thereby efficiently electrolyzing a sulfuric acid solution and the like. An electrolysis method includes: passing an electrolytic solution through an electrolysis cell including at least a pair of an anode and a cathode; and supplying the electrodes with an electric power, so as to electrolyze the electrolytic solution, wherein a viscosity of the electrolytic solution is set in a range in response to a current density upon the electric power supply to carry out the electrolysis. The viscosity of a sulfuric acid solution as the electrolytic solution is equal to or less than 10 cP when the current density is equal to or less than 50 A/dm2, the viscosity of the sulfuric acid solution is equal to or less than 8 cP when the current density is from more than 50 to 75 A/dm2, and the viscosity of the sulfuric acid solution is equal to or less than 6 cP when the current density is from more than 75 to 100 A/dm2. Particularly when a highly-concentrated sulfuric acid solution is electrolyzed at a high current density using diamond electrodes, the electrolysis process can be carried out highly efficiently while a wear of the electrode is reduced.
    • 尽可能地防止电极的磨损,从而有效地电解硫酸溶液等。 电解方法包括:使电解液通过包括至少一对阳极和阴极的电解槽; 以及向所述电极供电,以便电解所述电解液,其中所述电解液的粘度响应于所述电源上的电流密度而设定在一定范围内以进行所述电解。 当电流密度等于或小于50A / dm 2时,作为电解液的硫酸溶液的粘度等于或小于10cP,硫酸溶液的粘度等于或小于8cP,当 电流密度为50〜75A / dm 2,当电流密度为75〜100A / dm 2时,硫酸溶液的粘度为6cP以下。 特别是当使用金刚石电极以高电流密度电解高浓度硫酸溶液时,可以高效地进行电解处理,同时降低电极的磨损。
    • 10. 发明申请
    • SUBSTRATE PROCESSING APPARATUS AND SUBSTRATE PROCESSING METHOD
    • 基板处理装置和基板处理方法
    • US20100175714A1
    • 2010-07-15
    • US12440400
    • 2007-09-05
    • Tatsuo NagaiHiroshi MoritaHiroaki TakahashiHiroaki UchidaToyohide Hayashi
    • Tatsuo NagaiHiroshi MoritaHiroaki TakahashiHiroaki UchidaToyohide Hayashi
    • B08B3/08
    • G03F7/423H01L21/6708
    • A substrate processing apparatus and a substrate processing method, with which a resist can be removed satisfactorily from the substrate and a processing solution used for removing the resist can be recycled, are provided. The substrate processing apparatus includes: a substrate holding means holding a substrate; a peroxosulfuric acid generating means generating a peroxosulfuric acid using sulfuric acid; a mixing means mixing the peroxosulfuric acid generated by the peroxosulfuric acid generating means and sulfuric acid of higher temperature and higher concentration than the sulfuric acid used in the peroxosulfuric acid generating means; and a discharging means discharging, toward the substrate held by the substrate holding means, the mixed solution of the peroxosulfuric acid and the sulfuric acid mixed by the mixing means as a processing solution for removing a resist from the substrate.
    • 提供了可以从衬底中令人满意地去除抗蚀剂的衬底处理设备和衬底处理方法,并且可以再循环用于除去抗蚀剂的处理溶液。 基板处理装置包括:保持基板的基板保持装置; 使用硫酸生成过氧硫酸的过氧硫酸生成装置; 将由过硫酸产生装置产生的过氧硫酸与比过硫酸产生装置中使用的硫酸更高和更高浓度的硫酸混合的混合装置; 以及排出装置将由所述基板保持装置保持的基板排出由所述混合装置混合的所述过硫酸和所述硫酸的混合溶液作为从所述基板除去抗蚀剂的处理溶液。