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1. 发明授权

US08492308B2 Thermosensitive recording medium 有权
标题翻译：热敏记录介质
公开(公告)号：US08492308B2
公开(公告)日：2013-07-23
申请号：US12674296
申请日：2008-08-21
申请人： Tatsuyuki Kurihara , Tatsuo Nagai , Yoshimi Midorikawa , Akihito Ogino , Mamoru Suga , Yoshimune Aosaki
发明人： Tatsuyuki Kurihara , Tatsuo Nagai , Yoshimi Midorikawa , Akihito Ogino , Mamoru Suga , Yoshimune Aosaki
IPC分类号： B41M5/333
CPC分类号： B41M5/3336 , B41M5/3335 , B41M5/426 , B41M5/44 , B41M2205/04 , B41M2205/38 , B41M2205/40
摘要： The present invention provides a thermosensitive recording medium with excellent color developing sensitivity, moist heat resistance and plasticizer resistance, as well as excellent heat resistance, background coloring, light resistance and the like in the printed image.A diphenyl sulfone derivative containing a hydroxyl group on one end and an alkoxy group on the other end has a higher melting point than the one containing hydroxyl groups on both ends. As a result, the thermosensitive recording medium obtained using the diphenyl sulfone derivative as the color developing agent in the thermosensitive color developing layer has excellent heat resistance. However the color developing sensitivity of the thermosensitive recording medium generally declines simultaneously, when a color developing agent with a high melting point is ordinarily used. The thermosensitive recording medium of the present invention that uses a combination of the diphenyl sulfone derivative and a specific phenol derivative in the thermosensitive color developing layer has a good color developing sensitivity and an improved balance among the properties such as moist heat resistance, plasticizer resistance and the like.
摘要翻译：本发明提供了在印刷图像中具有优异的显色灵敏度，耐湿热性和耐增塑剂性以及优异的耐热性，背景着色，耐光性等的热敏记录介质。一端含有羟基，另一端含有烷氧基的二苯砜衍生物的熔点比两末端羟基的熔点高。结果，在热敏显色层中使用二苯砜衍生物作为彩色显影剂获得的热敏记录介质具有优异的耐热性。然而，当通常使用具有高熔点的彩色显影剂时，热敏记录介质的显色灵敏度通常会同时下降。在热敏显色层中使用二苯砜衍生物和特定苯酚衍生物的组合的本发明的热敏记录介质具有良好的显色灵敏度，并且在诸如耐湿热性，耐增塑剂性和类似。

2. 发明申请

US20110130281A1 THERMOSENSITIVE RECORDING MEDIUM 有权
标题翻译：耐热记录介质
公开(公告)号：US20110130281A1
公开(公告)日：2011-06-02
申请号：US12674296
申请日：2008-08-21
申请人： Tatsuyuki Kurihara , Tatsuo Nagai , Yoshimi Midorikawa , Akihito Ogino , Mamoru Suga , Yoshimune Aosaki
发明人： Tatsuyuki Kurihara , Tatsuo Nagai , Yoshimi Midorikawa , Akihito Ogino , Mamoru Suga , Yoshimune Aosaki
IPC分类号： B41M5/333 , B41M5/323 , B41M5/337
CPC分类号： B41M5/3336 , B41M5/3335 , B41M5/426 , B41M5/44 , B41M2205/04 , B41M2205/38 , B41M2205/40
摘要： The present invention provides a thermosensitive recording medium with excellent color developing sensitivity, moist heat resistance and plasticizer resistance, as well as excellent heat resistance, background coloring, light resistance and the like in the printed image.A diphenyl sulfone derivative containing a hydroxyl group on one end and an alkoxy group on the other end has a higher melting point than the one containing hydroxyl groups on both ends. As a result, the thermosensitive recording medium obtained using the diphenyl sulfone derivative as the color developing agent in the thermosensitive color developing layer has excellent heat resistance. However the color developing sensitivity of the thermosensitive recording medium generally declines simultaneously, when a color developing agent with a high melting point is ordinarily used. The thermosensitive recording medium of the present invention that uses a combination of the diphenyl sulfone derivative and a specific phenol derivative in the thermosensitive color developing layer has a good color developing sensitivity and an improved balance among the properties such as moist heat resistance, plasticizer resistance and the like.
摘要翻译：本发明提供了在印刷图像中具有优异的显色灵敏度，耐湿热性和耐增塑剂性以及优异的耐热性，背景着色，耐光性等的热敏记录介质。一端含有羟基，另一端含有烷氧基的二苯砜衍生物的熔点比两末端羟基的熔点高。结果，在热敏显色层中使用二苯砜衍生物作为彩色显影剂获得的热敏记录介质具有优异的耐热性。然而，当通常使用具有高熔点的彩色显影剂时，热敏记录介质的显色灵敏度通常会同时下降。在热敏显色层中使用二苯砜衍生物和特定苯酚衍生物的组合的本发明的热敏记录介质具有良好的显色灵敏度，并且在诸如耐湿热性，耐增塑剂性和类似。

3. 发明申请

US20130237414A1 NOVEL PHENOLSULFONIC ACID ARYL ESTER DERIVATIVE, AND HEAT-SENSITIVE RECORDING MATERIAL USING SAME 有权
标题翻译：新型酚醛酸酯衍生物和使用相同的热敏记录材料
公开(公告)号：US20130237414A1
公开(公告)日：2013-09-12
申请号：US13822991
申请日：2011-09-16
申请人： Mai Higuchi , Yoshimune Aosaki , Keiichiro Inada , Mamoru Suga , Katsuto Ohse , Yoshimi Midorikawa , Yukiko Sato
发明人： Mai Higuchi , Yoshimune Aosaki , Keiichiro Inada , Mamoru Suga , Katsuto Ohse , Yoshimi Midorikawa , Yukiko Sato
IPC分类号： B41M5/333 , B41M5/337 , B41M5/323
CPC分类号： B41M5/3336 , B41M5/323 , B41M5/3275 , B41M5/3335 , B41M5/3375 , C07C309/75
摘要： The invention provides a phenolsulfonic acid aryl ester represented by formula (1) wherein each symbol is as defined in the description. The phenolsulfonic acid aryl ester is useful as a developer to provide a thermal recording material with good color-developing sensitivity, image density when printed at a low application energy (i.e., high start-up sensitivity), and heat and plasticizer resistance. The invention also provides a thermal recording material using the developer.
摘要翻译：本发明提供由式（1）表示的苯酚磺酸芳基酯，其中每个符号如说明书中所定义。苯酚磺酸芳基酯可用作显影剂，以提供具有良好显色灵敏度的热敏记录材料，以低应用能量（即高启动灵敏度）印刷时的图像密度，耐热和耐增塑剂性。本发明还提供了使用显影剂的热敏记录材料。

4. 发明申请

US20110269622A1 THERMOSENSITIVE RECORDING MEDIUM 审中-公开
标题翻译：耐热记录介质
公开(公告)号：US20110269622A1
公开(公告)日：2011-11-03
申请号：US12934230
申请日：2009-03-27
申请人： Katsuto Ohse , Yoshimi Midorikawa , Akihito Ogino , Keiichirou Inada , Yoshimune Aosaki
发明人： Katsuto Ohse , Yoshimi Midorikawa , Akihito Ogino , Keiichirou Inada , Yoshimune Aosaki
IPC分类号： B41M5/333 , B41M5/323
CPC分类号： B41M5/44 , B41M5/3335 , B41M5/3336 , B41M2205/04 , B41M2205/40
摘要： The present invention provides a thermosensitive recording medium having an excellent image durability, even when used in a severe condition.A thermosensitive recording medium having a thermosensitive color developing layer comprising a colorless or pale colored dye and two kinds of color developing agents on a substrate, wherein the thermosensitive color developing layer contains bis (3-allyl-4-hydroxyphenyl) sulfone and a phenol novolac compound as the color developing agents.
摘要翻译：本发明提供即使在恶劣条件下使用也具有优异的图像耐久性的热敏记录介质。一种热敏记录介质，其具有在基材上包含无色或浅色染料和两种彩色显影剂的热敏显色层，其中热敏显色层含有双（3-烯丙基-4-羟基苯基）砜和苯酚酚醛清漆化合物作为显色剂。

5. 发明授权

US08975212B2 Phenolsulfonic acid aryl ester derivative, and heat-sensitive recording material using same 有权
标题翻译：苯酚磺酸芳酯衍生物和使用其的热敏记录材料
公开(公告)号：US08975212B2
公开(公告)日：2015-03-10
申请号：US13822991
申请日：2011-09-16
申请人： Mai Higuchi , Yoshimune Aosaki , Keiichiro Inada , Mamoru Suga , Katsuto Ohse , Yoshimi Midorikawa , Yukiko Sato
发明人： Mai Higuchi , Yoshimune Aosaki , Keiichiro Inada , Mamoru Suga , Katsuto Ohse , Yoshimi Midorikawa , Yukiko Sato
IPC分类号： B41M5/333 , B41M5/337 , C07C309/75 , B41M5/323 , B41M5/327
CPC分类号： B41M5/3336 , B41M5/323 , B41M5/3275 , B41M5/3335 , B41M5/3375 , C07C309/75
摘要： The invention provides a phenolsulfonic acid aryl ester represented by formula (1) wherein each symbol is as defined in the description. The phenolsulfonic acid aryl ester is useful as a developer to provide a thermal recording material with good color-developing sensitivity, image density when printed at a low application energy (i.e., high start-up sensitivity), and heat and plasticizer resistance. The invention also provides a thermal recording material using the developer.
摘要翻译：本发明提供由式（1）表示的苯酚磺酸芳基酯，其中每个符号如说明书中所定义。苯酚磺酸芳基酯可用作显影剂，以提供具有良好显色灵敏度的热敏记录材料，以低应用能量（即高启动灵敏度）印刷时的图像密度，耐热和耐增塑剂性。本发明还提供了使用显影剂的热敏记录材料。

6. 发明申请

US20090280980A1 Thermal recording material 有权
标题翻译：热敏记录材料
公开(公告)号：US20090280980A1
公开(公告)日：2009-11-12
申请号：US12311320
申请日：2007-09-26
申请人： Junpei Natsui , Hiroshi Kohama , Mamoru Suga , Yoshimune Aosaki
发明人： Junpei Natsui , Hiroshi Kohama , Mamoru Suga , Yoshimune Aosaki
IPC分类号： B41M5/333 , B41M5/323
CPC分类号： B41M5/3335
摘要： Provided is a thermal recording material superior in color development sensitivity, and having good preservation properties such as in heat resistance, moisture resistance, water resistance and the like.A thermal recording material comprising a support and a thermal recording layer comprising a colorless or pale basic leucodye and a developer to develop color of the basic leucodye, wherein the aforementioned developer comprises a first developer which is a condensate or condensed composition represented by the following formula (I) and a second developer other than the first developer, and the proportion of the first developer to the total amount of the developers is not less than 2 wt % and less than 50 wt %: wherein R is a hydrogen atom, a halogen atom, a hydroxyl group, a lower alkyl group, an alkoxyl group, a cyano group, a nitro group, an aryl group or an aralkyl group, R in the number of m may be the same or different, m is an integer of 0 to 3, n is an integer of 0 to 3, and X and Y are each a hydrogen atom, an alkyl group or an aryl group.
摘要翻译：提供了显色性良好且耐热性，耐湿性，耐水性等保存性优良的热敏记录材料。一种热敏记录材料，其包含支撑体和包含无色或浅色碱性亮氨酸的显影剂和显色剂，以显色出碱性白变色剂，其中上述显色剂包括第一显影剂，其为由下式表示的缩合物或缩合组合物（I）和第一显色剂之外的第二显影剂，第一显影剂与显影剂总量的比例不小于2重量％且小于50重量％：其中R是氢原子，卤素原子，羟基，低级烷基，烷氧基，氰基，硝基，芳基或芳烷基，m数可以相同或不同，m为整数0 至3，n为0〜3的整数，X和Y各自为氢原子，烷基或芳基。

7. 发明授权

US08202821B2 Thermal recording material 有权
标题翻译：热敏记录材料
公开(公告)号：US08202821B2
公开(公告)日：2012-06-19
申请号：US12311320
申请日：2007-09-26
申请人： Junpei Natsui , Hiroshi Kohama , Mamoru Suga , Yoshimune Aosaki
发明人： Junpei Natsui , Hiroshi Kohama , Mamoru Suga , Yoshimune Aosaki
IPC分类号： B41M5/333
CPC分类号： B41M5/3335
摘要： Provided is a thermal recording material superior in color development sensitivity, and having good preservation properties such as in heat resistance, moisture resistance, water resistance and the like.A thermal recording material comprising a support and a thermal recording layer comprising a colorless or pale basic leucodye and a developer to develop color of the basic leucodye, wherein the aforementioned developer comprises a first developer which is a condensate or condensed composition represented by the following formula (I) and a second developer other than the first developer, and the proportion of the first developer to the total amount of the developers is not less than 2 wt % and less than 50 wt %: wherein R is a hydrogen atom, a halogen atom, a hydroxyl group, a lower alkyl group, an alkoxyl group, a cyano group, a nitro group, an aryl group or an aralkyl group, R in the number of m may be the same or different, m is an integer of 0 to 3, n is an integer of 0 to 3, and X and Y are each a hydrogen atom, an alkyl group or an aryl group.
摘要翻译：提供了显色性良好且耐热性，耐湿性，耐水性等保存性优良的热敏记录材料。一种热敏记录材料，其包含支撑体和包含无色或浅色碱性亮氨酸的显影剂和显色剂，以显色所述碱性白变体的颜色，其中所述显影剂包含第一显影剂，所述第一显影剂是由下式表示的缩合物或缩合组合物（I）和第一显色剂之外的第二显影剂，第一显影剂与显影剂总量的比例不小于2重量％且小于50重量％：其中R是氢原子，卤素原子，羟基，低级烷基，烷氧基，氰基，硝基，芳基或芳烷基，m数可以相同或不同，m为整数0 至3，n为0〜3的整数，X和Y各自为氢原子，烷基或芳基。

8. 发明授权

US08470735B2 Coating solution for heat-sensitive color-developing layer, and heat-sensitive recording material 有权
标题翻译：用于热敏彩色显影层的涂布溶液和热敏记录材料
公开(公告)号：US08470735B2
公开(公告)日：2013-06-25
申请号：US13262701
申请日：2010-04-02
申请人： Yoshimune Aosaki , Mai Kaneko , Katsuto Ohse , Yukiko Sato
发明人： Yoshimune Aosaki , Mai Kaneko , Katsuto Ohse , Yukiko Sato
IPC分类号： B41M5/333 , B41M5/337 , C09D11/00
CPC分类号： B41M5/3336 , B41M5/323 , B41M5/3335 , B41M5/42 , B41M5/44 , B41M2205/04 , B41M2205/40
摘要： Provided are a coating solution for a thermosensitive color developing layer of excellent storability wherein color development during its storage or during producing a thermal recording material is suppressed, and a thermal recording material with excellent print portion (image portion) storability and suppressed staining in the background color (white background).A coating solution for a thermosensitive color developing layer, which comprises a colorless or pale-colored electron-donating leuco dye, a hindered phenol compound and, as an electron-accepting developer, a diphenylsulfone derivative represented by the following formula (1): wherein the aforementioned hindered phenol compound has an average particle size (D50) of not more than 0.5 μm, and the coating solution has a color tone a* of not less than −4.0 as measured according to JIS Z 8729 and a whiteness W of not less than 62 as measured according to JIS Z 8715.
摘要翻译：提供一种用于热存储性优良的热敏彩色显影层的涂布溶液，其中抑制了在其储存期间或在制备热敏记录材料期间的显色性，以及具有优异的印刷部分（图像部分）保存性和背景抑制染色的热敏记录材料颜色（白色背景）。一种用于热敏显色层的涂布溶液，其包含无色或浅色给电子的无色染料，受阻酚化合物和作为电子接受显影剂的由下式（1）表示的二苯砜衍生物：其中上述受阻酚化合物的平均粒径（D50）为0.5μm以下，根据JIS Z 8729测定，涂布液的色调a *不小于-4.0，白度W不低于大于62，按照JIS Z 8715测量。

9. 发明申请

US20120157303A1 COATING SOLUTION FOR HEAT-SENSITIVE COLOR-DEVELOPING LAYER, AND HEAT-SENSITIVE RECORDING MATERIAL 有权
标题翻译：用于感应色层的涂层溶液和感热记录材料
公开(公告)号：US20120157303A1
公开(公告)日：2012-06-21
申请号：US13262701
申请日：2010-04-02
申请人： Yoshimune Aosaki , Mai Kaneko , Katsuto Ohse , Yukiko Sato
发明人： Yoshimune Aosaki , Mai Kaneko , Katsuto Ohse , Yukiko Sato
IPC分类号： B41M5/333 , B41M5/337 , C09D5/00 , B41M5/323
CPC分类号： B41M5/3336 , B41M5/323 , B41M5/3335 , B41M5/42 , B41M5/44 , B41M2205/04 , B41M2205/40
摘要： Provided are a coating solution for a thermosensitive color developing layer of excellent storability wherein color development during its storage or during producing a thermal recording material is suppressed, and a thermal recording material with excellent print portion (image portion) storability and suppressed staining in the background color (white background).A coating solution for a thermosensitive color developing layer, which comprises a colorless or pale-colored electron-donating leuco dye, a hindered phenol compound and, as an electron-accepting developer, a diphenylsulfone derivative represented by the following formula (1): wherein the aforementioned hindered phenol compound has an average particle size (D50) of not more than 0.5 μm, and the coating solution has a color tone a* of not less than −4.0 as measured according to JIS Z 8729 and a whiteness W of not less than 62 as measured according to JIS Z 8715.
摘要翻译：提供一种用于热存储性优良的热敏彩色显影层的涂布溶液，其中抑制了在其储存期间或在制备热敏记录材料期间的显色性，以及具有优异的印刷部分（图像部分）保存性和背景抑制染色的热敏记录材料颜色（白色背景）。一种用于热敏显色层的涂布溶液，其包含无色或浅色给电子的无色染料，受阻酚化合物和作为电子接受显影剂的由下式（1）表示的二苯砜衍生物：其中上述受阻酚化合物的平均粒径（D50）不大于0.5μm，涂布液的色调a *不小于-4.0，根据JIS Z 8729测定，白度W不低于大于62，按照JIS Z 8715测量。

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