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    • 5. 发明授权
    • Method for manufacturing a low loss, low temperature cofired ceramic
    • 低损耗,低温烧结陶瓷的制造方法
    • US5683528A
    • 1997-11-04
    • US460953
    • 1995-06-05
    • Deborah P. PartlowStephen R. GurkovichKenneth C. RadfordAndrew J. Piloto
    • Deborah P. PartlowStephen R. GurkovichKenneth C. RadfordAndrew J. Piloto
    • B32B18/00C04B35/16C04B35/624C04B37/00
    • C04B35/16B32B18/00C04B35/624C04B2237/12C04B2237/341C04B2237/62C04B2237/68
    • A method for forming a low temperature cofired ceramic package which is made using a multi-layered densified spherical powder formed via a sol-gel process. This densified powder is formed from layers of SiO.sub.2 reacted with trimethyl borate. The spherical powder has a preselected particle size and boron content sufficient to render the low temperature cofired ceramic package fully dense, even in the presence of a second phase filler ceramic, at a sintering temperature below 1000.degree. C. Binder material is added to the spherical powder and ceramic filler to form a plurality of tapes. A ceramic assembly is then formed by layering the plurality of tapes upon one another and firing the ceramic assembly at a temperature below 1025.degree. C. to form a fully dense cofired ceramic package. In order to form the multi-layered densified spherical powder, a silica core, which is formed using a sol-gel process, is reacted with trimethyl borate. An additional layer of silica is provided upon the reacted product which, in turn, is reacted with trimethyl borate. This process is continued until a spherical powder of desired size is formed.
    • 一种用于形成低温共烧陶瓷封装的方法,其使用通过溶胶 - 凝胶法形成的多层致密球形粉末制成。 该致密化粉末由与硼酸三甲酯反应的SiO 2层形成。 即使在第二相填料陶瓷的存在下,在低于1000℃的烧结温度下,球形粉末具有足以使低温共烧陶瓷封装完全致密的预选粒度和硼含量。将粘合剂材料加入到球形 粉末和陶瓷填料以形成多个带。 然后通过将多个带彼此层叠并在低于1025℃的温度下烧制陶瓷组件以形成完全致密的共烧陶瓷封装形成陶瓷组件。 为了形成多层致密球形粉末,使用溶胶 - 凝胶法形成的二氧化硅芯与硼酸三甲酯反应。 在反应产物上提供另外的二氧化硅层,其又与硼酸三甲酯反应。 继续该过程,直到形成所需尺寸的球形粉末。