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1. 发明授权

US06962726B2 Method for preparing substrate for flexible print wiring board, and substrate for flexible print wiring board 失效
标题翻译：柔性印刷线路板用基板的制造方法以及柔性印刷电路板用基板
公开(公告)号：US06962726B2
公开(公告)日：2005-11-08
申请号：US10258057
申请日：2001-06-11
申请人： Akira Shigeta , Takeshi Yoshida , Jun-ichi Mori , Yoshiaki Echigo , Ryoichi Hasegawa , Minoru Noji , Seiichi Hayashi , Makoto Uchida
发明人： Akira Shigeta , Takeshi Yoshida , Jun-ichi Mori , Yoshiaki Echigo , Ryoichi Hasegawa , Minoru Noji , Seiichi Hayashi , Makoto Uchida
IPC分类号： C08J5/24 , H05K1/03 , B05D5/12
CPC分类号： H05K1/0346 , C08G73/1007 , C08L79/08 , H05K1/036 , Y10T428/31551 , Y10T428/31605
摘要： A method for preparing a substrate for a flexible print wiring board having a polyimide based resin layer wherein a solution of a polyimide based resin precursor is directly applied on an electrically conducting material to form a polyimide based resin precursor layer and then the precursor layer is cured by heating to prepare a polyimide based resin layer, characterized in that a solution of a polyimide based resin precursor B, which is one of solutions of two types of polyimide based resin precursors, is directly applied on an electrically conducting material and then, on the resultant layer is applied a solution of a polyimide based resin precursor A which allows resolving the residual strain generated in the polyimide based resin formed by the curing of the above polyimide based resin precursor B.
摘要翻译：一种用于制备具有聚酰亚胺基树脂层的柔性印刷布线板的基板的方法，其中将聚酰亚胺基树脂前体的溶液直接涂覆在导电材料上以形成聚酰亚胺基树脂前体层，然后将前体层固化通过加热制备聚酰亚胺基树脂层，其特征在于将作为两种类型的聚酰亚胺基树脂前体的溶液之一的聚酰亚胺树脂前体B的溶液直接施加到导电材料上，然后在施加聚酰亚胺基树脂前体A的溶液，其可以分解通过上述聚酰亚胺基树脂前体B的固化形成的聚酰亚胺基树脂中产生的残余应变。

2. 发明授权

US5840824A Epoxy resin, epoxy resin composition and hardened product thereof 失效
标题翻译：环氧树脂，环氧树脂组合物及其硬化产物
公开(公告)号：US5840824A
公开(公告)日：1998-11-24
申请号：US773967
申请日：1996-12-26
申请人： Yasumasa Akatsuka , Kenichi Kuboki , Yoshio Shimamura , Ryoichi Hasegawa
发明人： Yasumasa Akatsuka , Kenichi Kuboki , Yoshio Shimamura , Ryoichi Hasegawa
IPC分类号： C08G59/06 , C08G59/04 , C08G59/08 , C08G59/32 , C08G59/00 , C08G65/08 , C08G65/14
CPC分类号： C08G59/08 , C08G59/3218
摘要： An object is to provide hardened products having excellent water resistance and mechanical strength, and an epoxy resin and an epoxy resin composition for use in the production thereof. An epoxy resin obtained by the glycidylation of a novolak type resin which is prepared by the condensation of biphenyls with phenols and naphthols, and a resin composition containing said epoxy resin and hardened products thereof.
摘要翻译：本发明的目的是提供具有优异的耐水性和机械强度的硬化产品，以及用于其生产的环氧树脂和环氧树脂组合物。通过联苯与苯酚和萘酚的缩合制备的酚醛清漆型树脂的缩水甘油化获得的环氧树脂和含有所述环氧树脂的树脂组合物及其硬化物。

3. 发明授权

US5202449A Process for purifying 7-dimethylamino-6-demethyl-6-deoxytetracycline 失效
标题翻译：纯化7-二甲氨基-6-去甲基-6-脱氧木糖苷的方法
公开(公告)号：US5202449A
公开(公告)日：1993-04-13
申请号：US758274
申请日：1991-08-27
申请人： Ryoichi Hasegawa , Hiroaki Ohno , Kazuaki Sano , Yoshinori Saito , Hiroaki Nishiyama , Shin'ichi Umeda
发明人： Ryoichi Hasegawa , Hiroaki Ohno , Kazuaki Sano , Yoshinori Saito , Hiroaki Nishiyama , Shin'ichi Umeda
IPC分类号： C07C231/24
CPC分类号： C07C231/24
摘要： A process for purifying 7-dimenthylamino-6-demethyl-6-deoxytetracycline represented by the following formula, ##STR1## which comprises dissolving 7-dimethylamino-6-demethyl-6-deoxytetracycline or its hydrochloride having a lower purity in a mixed solvent of an alcohol and water by using hydrochloric acid and then adjusting the pH of the solution to 3.5 to 4.5 to recrystallize the hydrochloride having a higher purity.
摘要翻译：用于纯化由下式表示的7-二甲基氨基-6-脱甲基-6-脱氧四环素的方法，其包括将具有较低纯度的7-二甲基氨基-6-脱甲基-6-脱氧四环素或其盐酸盐溶于通过使用盐酸，然后将溶液的pH调节至3.5至4.5的醇和水的混合溶剂，使具有较高纯度的盐酸盐重结晶。

4. 发明授权

US6124420A Epoxy resin, epoxy resin composition and hardened product thereof 失效
标题翻译：环氧树脂，环氧树脂组合物及其硬化产物
公开(公告)号：US6124420A
公开(公告)日：2000-09-26
申请号：US930892
申请日：1997-12-05
申请人： Kenichi Kuboki , Yoshio Shimamura , Ryoichi Hasegawa , Yoshiaki Kurimoto , Akiyuki Kojima , Yukio Abe
发明人： Kenichi Kuboki , Yoshio Shimamura , Ryoichi Hasegawa , Yoshiaki Kurimoto , Akiyuki Kojima , Yukio Abe
IPC分类号： C08G59/08 , C08G59/18 , C08G59/32 , C08G59/68 , C08L63/04
CPC分类号： C08G59/688 , C08G59/08 , C08G59/18 , C08G59/3218 , C08L63/04
摘要： This invention provides a novolak type epoxy resin which has low melt viscosity but shows high heat resistance when hardened. Particularly, it relates to a novolak type epoxy resin in which the relationship between the total % by weight of 3 to 6 nucleus bodies and the melt viscosity measured by a cone plate method at 150.degree. C. satisfies specified conditions, an epoxy resin composition containing the same and hardened products thereof.
摘要翻译： PCT No.PCT / JP97 / 00331 Sec。 371 1997年12月5日第 102（e）日期1997年12月5日PCT提交1997年2月7日PCT公布。出版物WO97 / 29144 日期：1997年8月14日本发明提供了一种酚醛清漆型环氧树脂，其具有低熔体粘度，但在硬化时显示出高耐热性。特别涉及一种酚醛清漆型环氧树脂，其中3〜6个核体的总重量％与锥板法在150℃下测定的熔融粘度之间的关系满足规定的条件，含有其相同和硬化的产品。

5. 发明授权

US5403716A Method for measurement of tissue factor in high sensitivity and measurement kit therefor 失效
标题翻译：高灵敏度组织因子测量方法及其测量套件
公开(公告)号：US5403716A
公开(公告)日：1995-04-04
申请号：US924030
申请日：1992-09-03
申请人： Kimihiko Matsuzawa , Ryoichi Hasegawa
发明人： Kimihiko Matsuzawa , Ryoichi Hasegawa
IPC分类号： C07K16/36 , G01N33/86 , G01N33/544 , G01N33/535 , G01N33/551 , G01N33/577
CPC分类号： C07K16/36 , G01N33/86 , G01N2333/7454 , Y10S435/81 , Y10S436/826
摘要： The present invention provides an improved buffer solution for conducting an immunological method for measuring apoprotein of human tissue factor, and a kit therefor. More specifically, in a method for immunologically measuring the presence or concentration of apoprotein of human tissue factor contained in a sample, which method includes the steps of (1) forming in a buffer solution a ternary complex of (a) a first monoclonal antibody which is capable of specifically binding to the apoprotein and is immobilized on a solid carrier insoluble in the buffer solution, (b) the apoprotein and (c) a labeled second monoclonal antibody which is capable of specifically binding to the apoprotein at a different site from the binding site of the first monoclonal antibody, and (2) measuring the amount of labeled second monoclonal antibody in the ternary complex to determine the presence or concentration of apoprotein in the sample, the improvement of this invention comprising employing a buffer solution(i) containing in a concentration of 2 to 15 weight % at least one nonionic surfactant having an HLB value within a range of 12 to 30, and(ii) containing a protein having a molecular weight of about 16,000 to about 50,000 and an isoelectric point of 1.0 to 5.0.
摘要翻译： PCT No.PCT / JP92 / 00005 Sec。 371日期：1992年9月3日 102（e）1992年9月3日PCT PCT 1992年1月8日PCT公布。出版物WO92 / 日本1992年7月23日。本发明提供了一种改进的缓冲溶液，用于进行用于测量人组织因子的脱蛋白的免疫学方法及其试剂盒。更具体地，在用于免疫测定样品中包含的人组织因子的脱辅基蛋白的存在或浓度的方法中，所述方法包括以下步骤：（1）在缓冲溶液中形成（a）第一单克隆抗体的三元配合物，所述第一单克隆抗体能够特异性结合载脂蛋白并固定在不溶于缓冲溶液的固体载体上，（b）载脂蛋白和（c）标记的第二单克隆抗体，其能够与不同部位的脱辅基蛋白特异性结合第一单克隆抗体的结合位点，和（2）测量三元复合物中标记的第二单克隆抗体的量以确定样品中脱辅基蛋白的存在或浓度，本发明的改进包括使用缓冲溶液（i）浓度为2至15重量％的至少一种HLB值在12至30范围内的非离子表面活性剂，和（ii）含有蛋白质 n的分子量为约16,000至约50,000，等电点为1.0至5.0。

6. 发明授权

US4918208A Process for producing 7-dimethylamino-6-demethyl-6-deoxytetracycline 失效
标题翻译： 7-二甲基氨基-6-脱甲基-6-脱氧四环素的制备方法
公开(公告)号：US4918208A
公开(公告)日：1990-04-17
申请号：US222886
申请日：1988-07-22
申请人： Ryoichi Hasegawa , Hiroaki Ohno , Kazuaki Sano , Yoshinori Saito
发明人： Ryoichi Hasegawa , Hiroaki Ohno , Kazuaki Sano , Yoshinori Saito
IPC分类号： C07C231/22 , C07C237/26
CPC分类号： C07C231/22 , C07C237/26 , C07C2103/46
摘要： A process for producing 7-dimethylamino-6-demethyl-6-deoxytetracycline (minocycline) which comprises treating the reaction liquid containing minocycline and formaldehyde with hydroxylamine or urea, the reaction liquid being obtained after reductive methylation of 7-amino-6-demethyl-6-deoxytetracycline by using aldehyde, then subjecting the reaction liquid to an adsorption treatment with a nonionic adsorption resin (adsorbent), and subsequently eluting the intended product adsorbed to the adsorbent.
摘要翻译：一种7-二甲基氨基-6-脱氧四环素（二甲胺四环素）的制备方法，其包括用羟胺或尿素处理含有二甲胺四环素和甲醛的反应液体，所述反应液是在还原甲基化7-氨基-6-去甲基 - 通过使用醛，然后用非离子吸附树脂（吸附剂）对反应液进行吸附处理，随后洗脱吸附在吸附剂上的预期产物。

7. 发明授权

US4582928A Process for producing optically active phenylalanine 失效
标题翻译：光学活性苯丙氨酸的制备方法
公开(公告)号：US4582928A
公开(公告)日：1986-04-15
申请号：US716400
申请日：1985-03-27
申请人： Shigeru Aoki , Mamoru Katagiri , Ryoichi Hasegawa , Akikazu Mitsunobu , Yasuhisa Tashiro
发明人： Shigeru Aoki , Mamoru Katagiri , Ryoichi Hasegawa , Akikazu Mitsunobu , Yasuhisa Tashiro
IPC分类号： C07B57/00 , C07B31/00 , C07C67/00 , C07C227/34 , C07C229/36 , C07C101/08
CPC分类号： C07C227/34
摘要： This invention relates to a process for producing optically active phenylalanine, characterized by optically resolving DL-phenylalanine.optically active mandelic acid complexes in an aqueous solvent in the presence of an acidic compound having a pKa value of 0.90 to 2.10 and isolating optically active phenylalanine from the obtained optically active phenylalanine.optically active mandelic acid complex.According to the process of the present invention, it is possible to decrease the amount of a mother liquor of resolution to 1/5 to 1/10 of that when no acidic compound is used and to obtain optically active phenylalanine having an optical purity of as high as 96.5% or above without a step of optical purification when optically active phenylalanine is isolated from the obtained optically active phenylalanine.optically active mandelic acid complex.
摘要翻译：本发明涉及一种光学活性苯丙氨酸的制备方法，其特征在于在pKa值为0.90至2.10的酸性化合物存在下，在水性溶剂中光学拆分DL-苯丙氨酸光学活性扁桃酸配合物，并将光学活性苯丙氨酸从所得光学活性苯丙氨酸光学活性扁桃酸复合物。根据本发明的方法，可以将分辨率降低至不使用酸性化合物时的1/5至1/10的量，并获得具有光学纯度的光学活性苯丙氨酸光学活性苯丙氨酸光学活性苯丙氨酸复合物中分离出光学活性苯丙氨酸时，不需要光学纯化步骤，高达96.5％以上。

8. 发明授权

US5352583A Human tissue plasminogen activator-human plasminogen activator inhibitor complex immunoassay and kit therefor 失效
标题翻译：人体组织纤溶酶原激活物 - 人纤溶酶原激活物抑制剂复合物免疫测定及其试剂盒
公开(公告)号：US5352583A
公开(公告)日：1994-10-04
申请号：US687867
申请日：1991-06-03
申请人： Yoichi Sakata , Kazuhiko Itoh , Shuichiro Hino , Ryoichi Hasegawa , Naomi Okamoto , Atsushi Noro , Toshinobu Murakami
发明人： Yoichi Sakata , Kazuhiko Itoh , Shuichiro Hino , Ryoichi Hasegawa , Naomi Okamoto , Atsushi Noro , Toshinobu Murakami
IPC分类号： G01N33/543 , G01N33/86 , G01N33/53
CPC分类号： G01N33/54393 , G01N33/54306 , G01N33/86 , G01N2333/8132 , G01N2333/9726 , Y10S435/962
摘要： A kit for the immunological assay of the human tissue plasminogen activator-human plasminogen activator inhibitor complex in a human specimen, which kit comprises(i) a monoclonal antibody (first antibody) against a human plasminogen activator inhibitor linked onto an insoluble solid carrier having a specular surface,(ii) a polyclonal antibody (second antibody) against a human tissue plasminogen activator labelled by an enzyme,(iii) a substrate and a reaction-discontinuing agent for the assay of the enzyme activity,(iv) a diluent, and(v) a detergent containing a nonionic surfactant having an HLB (Hydrophile Lipophile Balance) value of at least 16,and a method for the immunological assay of the above complex and a method for the immunological assay of the active human plasminogen activator inhibitor, respectively in a human specimen using this kit.
摘要翻译： PCT No.PCT / JP90 / 01269 Sec。 371日期1991年6月3日 102（e）日期1991年6月3日PCT 1990年10月2日PCT PCT。公开号WO91 / 05257 日期：1991年4月18日。用于人体标本中人组织纤溶酶原激活物 - 人纤溶酶原激活物抑制剂复合物的免疫测定试剂盒，该试剂盒包含（i）针对人类纤溶酶原激活物抑制剂的单克隆抗体（第一抗体）到具有镜面的不溶性固体载体上，（ii）针对由酶标记的人组织纤溶酶原激活物的多克隆抗体（第二抗体），（iii）用于测定酶活性的底物和反应中断剂，（iv）稀释剂，和（v）含有HLB（亲水亲油平衡）值至少为16的非离子表面活性剂的洗涤剂，以及上述复合物的免疫学测定方法和活性人纤溶酶原激活物抑制剂，分别在使用该试剂盒的人体标本中。

9. 发明授权

US4212813A Process for producing substituted or unsubstituted naphthalic acids and acid anhydrides thereof 失效
标题翻译：制备取代或未取代的萘二甲酸及其酸酐的方法
公开(公告)号：US4212813A
公开(公告)日：1980-07-15
申请号：US950407
申请日：1978-10-11
申请人： Ryoichi Hasegawa
发明人： Ryoichi Hasegawa
IPC分类号： C07C51/31 , C07C205/57 , C07B3/00
CPC分类号： C07C205/57 , C07C201/12 , C07C51/313 , C07C51/56 , C07D307/92
摘要： Process for producing substituted or unsubstituted naphthalic acids and acid anhydrides thereof by oxidation of corresponding acenaphthenes whose naphthalene nucleus may have one or two substituents from the group consisting of halogens, sulfonic acid groups, sulfonate groups, and nitro. The oxidation is performed at 30.degree.-150.degree. C. using molecular oxygen in the presence of (1) at least one heavy metal compound, such as cobalt acetate or manganese acetate, in an amount of 0.005-0.3 mole per mole of said acenaphthenes or a mixture of heavy metal compounds in that amount and a bromine compound in the range of 5.times.10.sup.-5 to 2.times.10.sup.-1 mole/liter of reaction solution as a catalyst and (2) at least one accelerator selected from the group consisting of lower fatty acid anhydrides, ketones and aldehydes, whereby side reactions such as condensation can be suppressed to a satisfactory extent, thereby leading to an improvement in yield of final product. A subsequent treatment of the oxidation product obtained by this process with peroxides, hypohalogenates, or molecular oxygen results in a higher yield.
摘要翻译：通过氧化相应的苊的方法制备取代或未取代的萘二甲酸及其酸酐，其萘核可以具有一个或两个来自卤素，磺酸基，磺酸酯基和硝基的取代基。在（1）至少一种重金属化合物如乙酸钴或乙酸锰存在下，使用分子氧在30-150℃进行氧化，其量为每摩尔所述苊的0.005-0.3摩尔或这种量的重金属化合物的混合物和作为催化剂的反应溶液的5×10 -5至2×10 -1摩尔/升范围内的溴化合物和（2）至少一种选自低脂肪酸酐，酮和醛，由此可以将缩合的副反应抑制到令人满意的程度，从而导致最终产物的收率提高。用过氧化物，次卤酸盐或分子氧随后处理通过该方法获得的氧化产物导致更高的产率。

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