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    • 9. 发明授权
    • Method of preparing metal powders, metal powders prepared in this way and compacts that include these powders
    • 制备金属粉末的方法,以这种方式制备的金属粉末和包括这些粉末的压块
    • US06464750B1
    • 2002-10-15
    • US09592440
    • 2000-06-12
    • Philippe TailhadesValérie CarlesAbel Rousset
    • Philippe TailhadesValérie CarlesAbel Rousset
    • C22C104
    • B82Y25/00B22F1/004B22F9/22C06B33/00C22B5/12C22B23/00C22B59/00H01F1/065H01F1/20H01M4/803H01M6/36
    • The invention relates to a method of preparing metal powder comprising: preparing a simple or mixed oxalate of one or more metals formed of particles with needle-like morphology having a mean acicularity ratio (length/diameter) of from 4 to 20, and a length of from 5 to 10 microns and converting said oxalate to metal or metal alloy powder by reducing treatment with gaseous hydrogen. The conversion of said oxalate can be carried out by decomposing said oxalate, in air, to an oxide and then reducing said oxide to metal or metal alloy. The metal is chosen from among the rare earth metals and the transition metals, preferably from among iron, cobalt, and nickel. The method is particularly suitable for making iron powder metal having a spongy and filament-like microstructure which makes it suitable for use in heating composition for thermo-piles. In addition, the invention relates to metal compacts unstoved or annealed which are obtained by applying compaction pressure to the powders according to the invention.
    • 本发明涉及一种制备金属粉末的方法,包括:制备一种或多种由具有4至20的平均针刺比(长/直径)的针状形态的颗粒形成的一种或多种金属的简单或混合草酸盐, 为5至10微米,并通过减少用气态氢处理将所述草酸盐转化为金属或金属合金粉末。 所述草酸盐的转化可以通过将所述草酸盐在空气中分解成氧化物,然后将所述氧化物还原成金属或金属合金来进行。 金属选自稀土金属和过渡金属,优选从铁,钴和镍中选出。 该方法特别适用于制造具有海绵状和丝状微细结构的铁粉金属,使其适用于热桩用加热组合物。 此外,本发明涉及通过对根据本发明的粉末施加压实压力而获得的未加工或退火的金属压块。