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1. 发明授权

US5760156A Manufacturing method for polycarbonate 失效
标题翻译：聚碳酸酯的制造方法
公开(公告)号：US5760156A
公开(公告)日：1998-06-02
申请号：US764816
申请日：1996-12-12
申请人： Satoshi Inoki , Yoshio Motoyama , Hideto Matsuoka , Hajime Oyoshi , Michio Tanaka , Tomoaki Shimoda , Akio Kanezawa , Kazutoyo Uno
发明人： Satoshi Inoki , Yoshio Motoyama , Hideto Matsuoka , Hajime Oyoshi , Michio Tanaka , Tomoaki Shimoda , Akio Kanezawa , Kazutoyo Uno
IPC分类号： C08G64/20 , C08G64/30 , C08G18/70
CPC分类号： C08G64/307
摘要： A manufacturing method for polycarbonate comprising �I! a process for manufacturing diaryl carbonate from an aromatic hydroxy compound and an aromatic hydroxy compound, �II! a process for manufacturing polycarbonate by solution polymerization of the diaryl carbonate obtained in �II! and an aromatic dihydroxy compound in the presence of a catalyst comprising a nitrogen-containing basic compound, and �III! a process for separating and removing the nitrogen-containing compound from the aromatic hydroxy by-products in �II! and returning the resultant aromatic hydroxy compounds to process �I! effectively reuses aromatic hydroxy by-products (e.g., phenols) of polycarbonate manufacturing to manufacture diaryl carbonate, while suppressing the production of alkyl aromatic ethers and then uses this diaryl carbonate to manufacture polycarbonate with good productivity.
摘要翻译：一种聚碳酸酯的制造方法，其包含：[I]由芳香族羟基化合物和芳香族羟基化合物制造碳酸二芳基酯的方法，[II]通过在[II]中得到的碳酸二芳基酯的溶液聚合制造聚碳酸酯的方法和芳香族二羟基在含有含氮碱性化合物的催化剂存在下的化合物，和[III]从[II]中的芳族羟基副产物中分离除去含氮化合物并将所得芳族羟基化合物返回到方法 [I]有效地重复使用制造碳酸二甲酯的聚碳酸酯的芳族羟基副产物（例如酚），同时抑制烷基芳族醚的生产，然后使用该碳酸二芳基酯以高生产率制造聚碳酸酯。

2. 发明授权

US06437194B2 Process for preparing an alkylcyclohexanol alkylene oxide adduct 失效
标题翻译：制备烷基环己醇烯化氧加合物的方法
公开(公告)号：US06437194B2
公开(公告)日：2002-08-20
申请号：US09270017
申请日：1999-03-16
申请人： Yoshihisa Inoue , Hiroyoshi Watanabe , Yasuko Ono , Masumi Okita , Daisuke Fukuoka , Yoshio Motoyama , Kenji Shimamoto
发明人： Yoshihisa Inoue , Hiroyoshi Watanabe , Yasuko Ono , Masumi Okita , Daisuke Fukuoka , Yoshio Motoyama , Kenji Shimamoto
IPC分类号： C07C4109
CPC分类号： C07C41/20 , C07C41/42 , C07C43/196 , C07C2601/14 , C08G65/322
摘要： The invention is a preparation process of alkylcyclohexanol alkylene oxide adduct which contains almost no alkylphenol alkylene oxide adduct 1) in the absence of a solvent, 2) in the presence of a saturated hydrocarbon solvent, or 3) in the presence of water. The invention can prepare alkylcyclohexanol alkylene oxide having a 200 ppm or less content of alkylphenol and alkylphenol alkylene oxide adduct. The alkylcyclohexanol alkylene oxide adduct obtained in the process of the invention has less ultraviolet absorption and fluorescence due to alkylphenol alkylene oxide adduct and is thus useful for spectrometric analysis of protein and further has excellent properties in the field of detergent and other common uses of surface active agents.
摘要翻译：本发明是在不存在溶剂的情况下几乎不含烷基酚环氧烷加合物1）的烷基环己醇烯化氧加合物的制备方法，2）在饱和烃溶剂存在下，或3）在水存在下。可以制备具有200ppm或更少含量的烷基酚和烷基酚环氧烷加合物的烷基环己醇烯化氧。在本发明方法中获得的烷基环己醇烯化氧加合物由于烷基酚烯化氧加合物而具有较少的紫外线吸收和荧光，因此可用于蛋白质的光谱分析，并且在洗涤剂领域和表面活性剂的其它常用用途中具有优异的性能代理商

3. 发明授权

US5932759A Process for producing substituted amines and a method for purifying synthetic intermediates therefor 失效
标题翻译：制备取代胺的方法及其合成中间体的纯化方法
公开(公告)号：US5932759A
公开(公告)日：1999-08-03
申请号：US800149
申请日：1997-02-13
申请人： Yoshio Motoyama , Naoshi Nagai , Takeshi Ishitoku , Noriaki Kihara
发明人： Yoshio Motoyama , Naoshi Nagai , Takeshi Ishitoku , Noriaki Kihara
IPC分类号： C07C239/20 , C07C261/00
CPC分类号： C07C239/20
摘要： The present invention relates to a process for producing a substituted amine represented by the general formula (IV):R.sup.2 NHOR.sup.3 (IV)(wherein R.sup.2 represents a hydrogen atom, a hydrocarbon group or a heteroatom-containing hydrocarbon group, and R.sup.3 represents a hydrocarbon group or a heteroatom-containing hydrocarbon group), which comprises the steps of:(b) reacting a hydroxamic acid represented by the general formula (II):R.sup.1 CONHOH (II)(wherein R.sup.1 represents a hydrogen atom or a hydrocarbon group) in the presence of a base with a reaction reagent capable of introducing a hydrocarbon or a heteroatom-containing hydrocarbon group to an oxygen atom and/or a nitrogen atom to form a substituted hydroxamic acid represented by the general formula (III): ##STR1## (wherein R.sup.1, R.sup.2 and R.sup.3 possess the same meanings as defined above),(c) hydrolyzing said substituted hydroxamic acid (III) in the presence of a base or an acid to produce a substituted amine represented by the general formula (IV):R.sup.2 NHOR.sup.3 (IV)(wherein R.sup.2 and R.sup.3 possess the same meanings as defined above). The present further relates to a method for purifying a synthetic intermediate for said substituted amine.
摘要翻译：本发明涉及由通式（IV）表示的取代胺的制备方法：R2NHOR3（IV）（其中R2表示氢原子，烃基或含杂原子的烃基，R3表示烃基或含杂原子的烃基），其包括以下步骤：（b）使通式（II）表示的异羟肟酸：R 1 CONHOH（II）（其中R 1表示氢原子或烃基）的具有能够将烃或含杂原子的烃基引入氧原子和/或氮原子的反应试剂形成由通式（III）表示的取代的异羟肟酸的反应试剂：其中R1，R2和 R3具有与上述相同的含义），（c）在碱或酸的存在下水解所述取代的异羟肟酸（III）以产生由通式（IV）表示的取代胺：R2NHOR3（IV）（其中 R 2和R3具有与上述相同的含义）。本发明还涉及纯化所述取代胺的合成中间体的方法。

4. 发明授权

US06737548B2 Process for preparing 1,5-diaminonaphthalene derivative 失效
标题翻译：制备1,5-二氨基萘衍生物的方法
公开(公告)号：US06737548B2
公开(公告)日：2004-05-18
申请号：US10312852
申请日：2003-01-02
申请人： Satoshi Inoki , Yoshio Motoyama
发明人： Satoshi Inoki , Yoshio Motoyama
IPC分类号： C07C20936
CPC分类号： C07C209/52 , C07C201/12 , C07C209/36 , C07C209/40 , C07C209/68 , C07C211/58 , C07C249/02 , C07C249/08 , C07C2602/10 , C07C251/44 , C07C251/20 , C07C205/06 , C07C205/45 , C07C205/56
摘要： In a process where an ortho-alkylnitrobenzene derivative and a vinyl compound as starting materials are used to prepare a 1,5-diaminonaphthalene derivative via a 4-(2-nitrobenzene)propane derivative and a 5-nitro-1-tetralone derivative, the ortho-alkylnitrobenzene derivative and a vinyl compound having an electron withdrawing group such as an acrylonitrile derivative and an acrylate may be reacted in the presence of a base to provide an aromatic nitro compound. An aromatic nitro compound such as 4-(2-nitrobenzene)butanonitrile thus obtained may be cyclized to safely, cost-effectively and selectively provide a 5-nitro-1-tetralone derivative without forming any isomer. Furthermore, from the 5-nitro-1-tetralone derivative, a 1,5-diaminonaphthalene derivative may be prepared without forming any isomer.
摘要翻译：在使用原烷基硝基苯衍生物和乙烯基化合物作为原料的方法中，通过4-（2-硝基苯）丙烷衍生物和5-硝基-1-四氢萘酮衍生物制备1,5-二氨基萘衍生物，正烷基硝基苯衍生物和具有吸电子基团的乙烯基化合物如丙烯腈衍生物和丙烯酸酯可以在碱的存在下反应以提供芳族硝基化合物。如此获得的芳族硝基化合物如4-（2-硝基苯）丁腈可以环化以安全，成本有效地选择性地提供5-硝基-1-四氢萘酮衍生物而不形成任何异构体。此外，从5-硝基-1-四氢萘酮衍生物可以制备1,5-二氨基萘衍生物而不形成任何异构体。

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