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1. 发明授权

US06869484B2 Continuous feed coater 有权
标题翻译：连续进料涂布机
公开(公告)号：US06869484B2
公开(公告)日：2005-03-22
申请号：US09952881
申请日：2001-09-15
申请人： Andrew T. Hunt , Wayne Neilson , Miodrag Oljaca , Edward J. Reardon , Tzyy-Jiuan Jan Hwang , William D. Danielson, Jr. , James D. Huggins , David E. Bane , Ian H. Campbell , Yibin Xue
发明人： Andrew T. Hunt , Wayne Neilson , Miodrag Oljaca , Edward J. Reardon , Tzyy-Jiuan Jan Hwang , William D. Danielson, Jr. , James D. Huggins , David E. Bane , Ian H. Campbell , Yibin Xue
IPC分类号： C23C16/00 , C23C16/44 , C23C16/453 , C23C16/455 , C23C16/54 , C23C14/00
CPC分类号： C23C16/45563 , C23C16/4412 , C23C16/453 , C23C16/45578 , C23C16/45585 , C23C16/45589 , C23C16/45591 , C23C16/545
摘要： A continuous feed coater for coating a length of substrate with vaporized or sprayed material, is disclosed. A specific example is a roll-to-roll coater which includes two lower supply rollers for supporting two webs of uncoated material, and two upper take-up rollers for supporting the webs after they are coated. A central web-support forms a plenum that acts as a deposition chimney or chamber by bringing the two webs into close proximity to each other to form two large walls of the plenum. The ends of the webs are sealed using side dams to form the chimney with a rectangular cross section such that the vapor cannot exit from the edges of the material. The vaporized coating constituents to be deposited on the rolled material are directed into the deposition plenum from a coating material supply source located at the bottom of the plenum, and are exhausted through the top of the plenum. By providing a plenum having two large surface area walls formed of the material to be coated, an extremely efficient coating system is provided. The top of the plenum includes an exhaust system with an orifice plate with a plurality of orifices spaced across the width of the deposition plenum. These orifices restrict gas exhaust to provide the gas and vapor residence time for the materials being used.
摘要翻译：公开了一种用蒸发或喷射材料涂覆一段衬底的连续进料涂布机。一个具体的例子是卷对卷涂布机，其包括用于支撑两个未涂覆材料的两个下供应辊和两个用于在涂布之后支撑网的上卷取辊。中央腹板支撑件形成通过使两个腹板彼此靠近以形成气室的两个大壁的作为沉积烟囱或腔的充气室。使用侧坝将腹板的端部密封以形成具有矩形横截面的烟囱，使得蒸气不能从材料的边缘排出。要沉积在轧制材料上的蒸发的涂层组分从位于集气室底部的涂料供应源引入沉积室，并通过气室的顶部排出。通过提供具有由待涂覆材料形成的两个大的表面积壁的增压室，提供了非常有效的涂层系统。增压室的顶部包括具有孔板的排气系统，孔板具有跨过沉积室的宽度间隔开的多个孔口。这些孔限制排气，为所用材料提供气体和蒸气停留时间。

2. 发明授权

US07351449B2 Chemical vapor deposition methods for making powders and coatings, and coatings made using these methods 有权
标题翻译：用于制造粉末和涂层的化学气相沉积方法以及使用这些方法制备的涂层
公开(公告)号：US07351449B2
公开(公告)日：2008-04-01
申请号：US09748714
申请日：2000-12-21
申请人： Andrew T. Hunt , Girish N. Deshpande , Tzyy-Jiuan Jan Hwang , Nii Sowa Laye , Miodrag Oljaca , Subramaniam Shanmugham , Shara S. Shoup , Trifon Tomov , William J. Dalzell, Jr. , Aimee Poda , Michelle Hendrick
发明人： Andrew T. Hunt , Girish N. Deshpande , Tzyy-Jiuan Jan Hwang , Nii Sowa Laye , Miodrag Oljaca , Subramaniam Shanmugham , Shara S. Shoup , Trifon Tomov , William J. Dalzell, Jr. , Aimee Poda , Michelle Hendrick
IPC分类号： C23C16/00 , C23C4/00
CPC分类号： C23C16/45587 , C23C16/453 , Y10T428/31507 , Y10T428/31598 , Y10T428/31786
摘要： Flame produced vapors for combustion chemical vapor deposition are redirected from the direction of the flame by differential atmospheric pressure, such as positive pressure provided by a blower or negative pressure provided by a vacuum. This allows, for example, lower surface temperatures of substrates being coated with flame-produced vapors and coating of interior surfaces.
摘要翻译：用于燃烧化学气相沉积的火焰产生的蒸气从不同的大气压力（例如由真空提供的正压力或由真空提供的负压）从火焰的方向转向。这允许例如涂覆有火焰产生的蒸汽的衬底的较低表面温度和内表面的涂层。

3. 发明授权

US07282238B2 Method of depositing materials 有权
标题翻译：材料沉积方法
公开(公告)号：US07282238B2
公开(公告)日：2007-10-16
申请号：US10111684
申请日：2001-06-27
申请人： Subramaniam Shanmugham , Andrew Tye Hunt , Girish Deshpande , Tzyy-Jiuan Jan Hwang , Erika Moore , Yongdong Jiang
发明人： Subramaniam Shanmugham , Andrew Tye Hunt , Girish Deshpande , Tzyy-Jiuan Jan Hwang , Erika Moore , Yongdong Jiang
IPC分类号： B05D3/08
CPC分类号： C03C17/001 , B05D1/08 , B05D1/34 , B05D3/0254 , B05D3/08 , B05D2518/10 , C03C17/007 , C03C17/009 , C03C17/32 , C03C17/42 , C03C2217/425 , C03C2217/445 , C03C2217/475 , C08K3/22 , C08K3/346 , C09D7/61 , C09D183/04 , C23C4/12 , C23C4/123 , C23C26/00 , Y10T428/12583 , Y10T428/31522
摘要： A coherent material is formed on a substrate (10) by providing a precursor suspension (14) in which particulates are suspended in a carrier fluid, and directing the precursor suspension (14) at the substrate (10) from a first source (12). Generally contemporaneously with application of the deposited precursor suspension (14) to the surface, hot gases, e.g. hot gases produced by a flame (16), are directed at the substrate (10) from a remote second source (18) to fuse the particulates into the coherent material.
摘要翻译：通过提供一种前体悬浮液（14），其中颗粒悬浮在载体流体中，并且将前体悬浮液（14）从第一源（12）引导到基底（10）处，在基底（10）上形成相干材料，。通常同时将沉积的前体悬浮液（14）施加到表面，热气体，例如，由火焰（16）产生的热气体从远程第二源（18）引导到衬底（10），以将微粒熔合成粘结材料。

4. 发明授权

US07033637B1 Epitaxial thin films 有权
标题翻译：外延薄膜
公开(公告)号：US07033637B1
公开(公告)日：2006-04-25
申请号：US09889237
申请日：2000-01-12
申请人： Andrew Tye Hunt , Girish Deshpande , Wen-Yi Lin , Tzyy-Jiuan Jan
发明人： Andrew Tye Hunt , Girish Deshpande , Wen-Yi Lin , Tzyy-Jiuan Jan
IPC分类号： B05D5/12
CPC分类号： H01M8/124 , B01D53/228 , B01D67/0072 , B01D71/024 , B01D2256/12 , B01D2325/22 , B01D2325/26 , C23C16/453 , H01G4/1209 , H01G4/33 , H01M8/0687 , H01M8/1253 , Y02E60/525 , Y02P70/56 , Y10T29/49115 , Y10T29/5313 , Y10T29/53135 , Y10T29/532 , Y10T29/53204
摘要： Epitatial thin films for use as buffer layers for high temperature superconductors, electrolytes in solid oxide fuel cells (SOFC), gas separation membranes or dielectric material in electronic devices, are disclosed. By using CCVD, CACVD or any other suitable deposition process, epitaxial films having pore-free, ideal grain boundaries, and dense structure can be formed. Several different types of materials are disclosed for use as buffer layers in high temperature superconductors. In addition, the use of epitaxial thin films for electrolytes and electrode formation in SOFCs results in densification for pore-free and ideal gain boundary/interface microstructure. Gas separation membranes for the production of oxygen and hydrogen are also disclosed. These semipermeable membranes are formed by high-quality, dense, gas-tight, pinhole free sub-micro scale layers of mixed-conducting oxides on porous ceramic substrates. Epitaxial thin films as dielectric material in capacitors are also taught herein. Capacitors are utilized according to their capacitance values which are dependent on their physical structure and dielectric permittivity. The epitaxial thin films of the current invention form low-loss dielectric layers with extremely high permittivity. This high permittivity allows for the formation of capacitors that can have their capacitance adjusted by applying a DC bias between their electrodes.
摘要翻译：公开了用作高温超导体的缓冲层的外延薄膜，固体氧化物燃料电池（SOFC）中的电解质，电子装置中的气体分离膜或电介质材料。通过使用CCVD，CACVD或任何其它合适的沉积工艺，可以形成具有无孔，理想晶界和致密结构的外延膜。公开了几种不同类型的材料用作高温超导体中的缓冲层。此外，在SOFC中使用外延薄膜用于电解质和电极形成导致无孔和理想的增益边界/界面微结构的致密化。还公开了用于生产氧气和氢气的气体分离膜。这些半透膜由多孔陶瓷基板上的高质量，致密，气密，无针孔的微小尺度的混合导电氧化物层形成。本文还介绍了作为电容器中的介电材料的外延薄膜。根据电容值的物理结构和介电常数，使用电容器。本发明的外延薄膜形成具有极高介电常数的低损耗介电层。这种高介电常数允许形成可以通过在它们的电极之间施加直流偏压来调整其电容的电容器。

5. 发明授权

US06939576B2 Polymer coatings 有权
标题翻译：聚合物涂料
公开(公告)号：US06939576B2
公开(公告)日：2005-09-06
申请号：US10311785
申请日：2001-06-27
申请人： Girish Deshpande , Andrew Tye Hunt , Subramaniam Shanmugham , Eric J. Yurtkuran , Todd Polley , Miodrag Oljara , Tzyy-Jiuan Jan Hwang , Aimee Poda , George Neuman
发明人： Girish Deshpande , Andrew Tye Hunt , Subramaniam Shanmugham , Eric J. Yurtkuran , Todd Polley , Miodrag Oljara , Tzyy-Jiuan Jan Hwang , Aimee Poda , George Neuman
IPC分类号： B05D1/08 , B05D1/34 , B05D3/02 , B05D3/08 , C03C17/00 , C03C17/32 , C03C17/42 , C09D7/12 , C09D183/04 , C23C4/12 , C23C26/00 , B05D3/00
CPC分类号： C03C17/001 , B05D1/08 , B05D1/34 , B05D3/0254 , B05D3/08 , B05D2518/10 , C03C17/007 , C03C17/009 , C03C17/32 , C03C17/42 , C03C2217/425 , C03C2217/445 , C03C2217/475 , C08K3/22 , C08K3/346 , C09D7/61 , C09D183/04 , C23C4/12 , C23C4/123 , C23C26/00 , Y10T428/12583 , Y10T428/31522
摘要： Coatings, particularly thin films, of polymeric material are produced in accordance with the invention by applying a finely divided aerosol of polymer solution to a substrate and substantially simultaneously applying an energy source to the applied solution to apply the solution. In cases where the polymer is cross-linking, the energy source assists in cross-linking of the polymer. The preferred energy source is a flame that may optionally or desirably deposit material along with the polymer spray. One particular aspect of the invention is directed to production of polyimide films. In accordance with another aspect of the invention, the co-deposition process is used to provide thin polysiloxane coatings on glass and other substrates.
摘要翻译：根据本发明，通过将细分散的聚合物溶液气溶胶施加到基底上并基本上同时向所施加的溶液施加能量来施加溶液来制备聚合材料的涂层，特别是薄膜。在聚合物交联的情况下，能量源有助于聚合物的交联。优选的能源是可以任选地或期望地将材料与聚合物喷雾一起沉积的火焰。本发明的一个特定方面涉及聚酰亚胺膜的制备。根据本发明的另一方面，共沉积方法用于在玻璃和其它基底上提供薄的聚硅氧烷涂层。

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