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1. 发明授权

US09675939B2 Composites and composite membranes 有权
公开(公告)号：US09675939B2
公开(公告)日：2017-06-13
申请号：US13367038
申请日：2012-02-06
申请人： Jochen Kerres , Thomas Häring , Rima Häring
发明人： Jochen Kerres , Thomas Häring , Rima Häring
IPC分类号： B01D61/00 , B01D67/00 , B01D69/14 , B01D71/00 , B01D71/02 , B01D71/62 , B01D71/68 , B01J21/16 , B01J31/10 , B01J31/16 , B01J35/06 , C08J5/22 , H01M8/1023 , H01M8/103 , H01M8/1032 , H01M8/1051 , H01M8/1081 , H01M8/0289
CPC分类号： B01D67/0041 , B01D69/141 , B01D71/00 , B01D71/024 , B01D71/62 , B01D71/68 , B01D2325/18 , B01D2325/26 , B01J21/16 , B01J31/10 , B01J31/1633 , B01J35/065 , C08J5/2275 , C08J2383/02 , H01M8/0289 , H01M8/1023 , H01M8/103 , H01M8/1032 , H01M8/1051 , H01M8/1081 , Y02E60/523 , Y02P70/56 , Y10T428/249953 , Y10T428/249969
摘要： The invention relates to a composite or a composite membrane consisting of an ionomer and of an inorganic optionally functionalized phyllosilicate. The isomer can be: (a) a cation exchange polymer; (b) an anion exchange polymer; (c) a polymer containing both anion exchanger groupings as well as cation exchanger groupings on the polymer chain; or (d) a blend consisting of (a) and (b), whereby the mixture ratio can range from 100% (a) to 100% (b). The blend can be ionically and even covalently cross-linked. The inorganic constituents can be selected from the group consisting of phyllosilicates or tectosilicates.

2. 发明授权

US09023557B2 Method for preparing a solution of a sulfonated polymer and an amino-phosphonic acid in an aprotic solvent 有权
标题翻译：在非质子传递溶剂中制备磺化聚合物和氨基膦酸溶液的方法
公开(公告)号：US09023557B2
公开(公告)日：2015-05-05
申请号：US12161932
申请日：2007-01-23
申请人： Thomas Häring
发明人： Thomas Häring
IPC分类号： H01M8/00 , C08J5/20 , H01M8/02 , B01D71/82 , C08J3/09 , C08J5/22 , H01M8/10
CPC分类号： H01M8/0291 , B01D71/82 , C08J3/091 , C08J5/2256 , C08J2371/10 , H01M8/0289 , H01M8/1039 , H01M8/1048 , H01M8/1072 , H01M8/1081 , Y02E60/523 , Y02P70/56
摘要： A method is disclosed for production of solutions of aminophosphonic acids and polymeric sulphonic acids in aprotic solvents. Membranes for membrane methodologies are produced from said solutions. Said membranes can also be doped with phosphoric acid.
摘要翻译：公开了用于在非质子溶剂中制备氨基膦酸和聚合磺酸的溶液的方法。用于膜方法的膜由所述溶液制备。所述膜也可掺杂磷酸。

3. 发明申请

US20140213672A1 PHOSPHONIC ACID-CONTAINING BLENDS AND PHOSPHONIC ACID-CONTAINING POLYMERS 审中-公开
公开(公告)号：US20140213672A1
公开(公告)日：2014-07-31
申请号：US14165456
申请日：2014-01-27
申请人： Thomas Häring
发明人： Thomas Häring , Jochen Kerres , Frank Schönberger , Martin Hein
IPC分类号： H01M8/10
CPC分类号： H01M8/1034 , B01J39/20 , C08G61/02 , C08G61/122 , C08J5/2287 , C08J2341/00 , H01M8/1011 , H01M8/1023 , H01M8/1025 , H01M8/1027 , H01M8/103 , H01M8/1032 , H01M8/1039 , H01M8/1044 , H01M8/1048 , H01M8/1072 , H01M2008/1095 , H01M2300/0082 , Y02E60/522 , Y02E60/523 , Y02P70/56
摘要： The invention relates to blends and blend membranes from low-molecular hydroxymethylene-oligo-phosphonic acids R—C(PO3H2)x(OH)y and polymers, the group R representing any organic group and the polymers containing the following functional groups: cation exchanger groups or their nonionic precursors of the type SO2X, X═HaI, OH, OMe, NR1R2, OR1 with Me=any metal cation or ammonium cation, R1, R2=H or any aryl- or alkyl group, POX2, COX and/or basic groups such as primary, secondary or tertiary amino groups, imidazole groups, pyridine groups, pyrazole groups etc. and/or OH groups. Low molecular hydroxymethylene-oligo-phosphonic acids R—C(PO3H2)x(OH)y are preferred in which x=2 and y=1. The invention also relates to low-molecular hydroxymethylene-oligo-phosphonic acids R—C(PO3H2)2(OH)1 and polymers, wherein the group R of the hydroxymethylene-oligophosphonic acid contains an aliphatic or aromatic basic group which ionically interacts with the acidic groups of the polymer or of the polymer mixture. The invention further relates to blends and blend membranes from low-molecular hydroxymethylene-oligo-phosphonic acids R—C(PO3H2)2(OH)1 and polymers, wherein the OH groups of the low-molecular hydroxymethylene-1,1-bisphosphonic acid are covalently cross-linked with each other or optionally with OH groups of the polymer. The invention also relates to polymers that are modified with the 1-hydroxymethylene-1,1-bisphosphonic acid group. The polymers are produced by reacting polymers which contain carboxylic acid groups or carboxylic halide groups —COHaI (Hal═F, Cl, Br, I) with phosphite compounds or by reacting polymeric aldehydes or polymeric keto compounds with phosphite esters while carrying out an amine catalysis, an oxidation of the intermediary hydroxyphosphonic acid with MnO2 or any other oxidant. The invention finally relates to methods for producing the aforementioned materials and to the use of membranes of the aforementioned materials in membrane processes and especially in fuel cells, even at temperatures of >100° C.

4. 发明授权

US08637174B2 Phosphonic acid-containing blends and phosphonic acid-containing polymers 有权
标题翻译：含膦酸的共混物和含膦酸的聚合物
公开(公告)号：US08637174B2
公开(公告)日：2014-01-28
申请号：US12278245
申请日：2007-02-05
申请人： Thomas Häring , Jochen Kerres , Frank Schönberger , Martin Hein
发明人： Thomas Häring , Jochen Kerres , Frank Schönberger , Martin Hein
IPC分类号： H01M8/10
CPC分类号： H01M8/1034 , B01J39/20 , C08G61/02 , C08G61/122 , C08J5/2287 , C08J2341/00 , H01M8/1011 , H01M8/1023 , H01M8/1025 , H01M8/1027 , H01M8/103 , H01M8/1032 , H01M8/1039 , H01M8/1044 , H01M8/1048 , H01M8/1072 , H01M2008/1095 , H01M2300/0082 , Y02E60/522 , Y02E60/523 , Y02P70/56
摘要： Various blends and blend membranes from low-molecular hydroxymethylene-oligo-phosphonic acids R—C(PO3H2)x(OH)y and polymers, the group R representing any organic group, the polymers containing cation exchanger groups or their nonionic precursors of the type SO2X, X being a halogen, OH, OMe, NR1R2, OR1 with Me being any metal cation or ammonium cation, R1, R2 being H or any aryl- or alkyl group, PDX2, COX and/or basic groups such as primary, secondary or tertiary amino groups, imidazole groups, pyridine groups, pyrazole groups etc. and/or OH groups. Such membranes may also include polymers that are modified with the 1-hydroxymethylene-1,1-bisphosphonic acid group. The polymers may be formed by reacting polymers which contain carboxylic acid groups or carboxylic halide groups —COHal (Hal=F, Cl, Br, I) with phosphite compounds or by reacting polymeric aldehydes or polymeric keto compounds with phosphite esters while carrying out an amine catalysis, an oxidation of the intermediary hydroxyphosphonic acid with MnO2 or another oxidant.
摘要翻译：来自低分子羟基亚甲基 - 寡聚膦酸RC（PO 3 H 2）x（OH）y和聚合物的各种共混物和共混膜，R代表任何有机基团，含有阳离子交换剂基团的聚合物或其SO 2 X型非离子前体， X是卤素，OH，OMe，NR1R2，OR1，其中Me是任何金属阳离子或铵阳离子，R1，R2是H或任何芳基或烷基，POX2，COX和/或碱性基团如伯，仲或叔氨基，咪唑基，吡啶基，吡唑基等和/或OH基。这样的膜还可以包括用1-羟基亚甲基-1,1-二膦酸基团改性的聚合物。聚合物可以通过使含有羧酸基团或羧酸卤化物-COHal（Hal = F，Cl，Br，I）的聚合物与亚磷酸酯化合物或通过使聚合醛或聚合酮化合物与亚磷酸酯反应同时进行胺催化，中间体羟基膦酸与MnO2或另一种氧化剂的氧化。

5. 发明授权

US08110517B2 Composites and composite membranes 有权
标题翻译：复合材料和复合膜
公开(公告)号：US08110517B2
公开(公告)日：2012-02-07
申请号：US12603017
申请日：2009-10-21
申请人： Jochen Kerres , Thomas Häring , Rima Häring
发明人： Jochen Kerres , Thomas Häring , Rima Häring
IPC分类号： B01J20/28 , B01D61/00 , H01M8/00
CPC分类号： B01D67/0041 , B01D69/141 , B01D71/00 , B01D71/024 , B01D71/62 , B01D71/68 , B01D2325/18 , B01D2325/26 , B01J21/16 , B01J31/10 , B01J31/1633 , B01J35/065 , C08J5/2275 , C08J2383/02 , H01M8/0289 , H01M8/1023 , H01M8/103 , H01M8/1032 , H01M8/1051 , H01M8/1081 , Y02E60/523 , Y02P70/56 , Y10T428/249953 , Y10T428/249969
摘要： The invention relates to a composite or a composite membrane consisting of an ionomer and of an inorganic optionally functionalized phyllosilicate. The isomer can be: (a) a cation exchange polymer; (b) an anion exchange polymer; (c) a polymer containing both anion exchanger groupings as well as cation exchanger groupings on the polymer chain; or (d) a blend consisting of (a) and (b), whereby the mixture ratio can range from 100% (a) to 100% (b). The blend can be ionically and even covalently cross-linked. The inorganic constituents can be selected from the group consisting of phyllosilicates or tectosilicates.
摘要翻译：本发明涉及由离聚物和无机任选官能化的页硅酸盐组成的复合膜或复合膜。异构体可以是：（a）阳离子交换聚合物; （b）阴离子交换聚合物; （c）聚合物链上含有阴离子交换剂组和聚合物链上的阳离子交换剂组的聚合物; 或（d）由（a）和（b）组成的共混物，其混合比可以在100％（a）至100％（b）的范围内。共混物可以是离子的，甚至共价交联的。无机成分可以选自页硅酸盐或三硅酸盐。

6. 发明申请

US20150064609A1 IONOMERS WITH IONIC GROUPS IN THE SIDE CHAIN 审中-公开
标题翻译：离子在侧链上的离子组
公开(公告)号：US20150064609A1
公开(公告)日：2015-03-05
申请号：US14293904
申请日：2014-11-12
申请人： Thomas Häring , Rima Häring
发明人： Thomas Häring , Jochen Kerres , Martin Hein
IPC分类号： B01J39/18 , H01M8/02 , C08J5/22
CPC分类号： B01J39/185 , B01D67/0006 , B01D67/0093 , B01D71/68 , B01D71/82 , B01D2325/16 , B01J39/19 , C08G65/48 , C08G75/0286 , C08J5/2231 , C08J5/2256 , C08J2365/02 , C08J2381/06 , H01M8/0289 , H01M8/1023 , H01M8/1025 , H01M8/1027 , H01M8/103 , H01M8/1032 , H01M8/1039 , H01M8/1072 , H01M2300/0082 , Y02E60/523 , Y02P70/56
摘要： Ionomers and ionomer membranes, consisting of a non-fluorinated or partly fluorinated non-, partly or fully-aromatic main chain and a non- or partly-fluorinated side chain with ionic groups or their non-ionic precursors, have a positive impact on the proton conductivity of the ionomers. Various processes produce these polymeric proton conductors.
摘要翻译：由非氟化或部分氟化的非部分或完全芳族主链和具有离子基团或其非离子前体的非或部分氟化的侧链组成的离聚物和离子交联聚合物膜对离聚物的质子电导率。各种方法产生这些聚合物质子导体。

7. 发明申请

US20140155502A1 FUNCTIONALIZED MAIN CHAIN POLYMERS 审中-公开
标题翻译：功能主链聚合物
公开(公告)号：US20140155502A1
公开(公告)日：2014-06-05
申请号：US14176815
申请日：2014-02-10
申请人： Thomas Häring
发明人： Thomas Häring
IPC分类号： B01J39/18
CPC分类号： B01J39/19 , B01D67/0093 , B01D71/52 , B01D71/68 , B01D71/80 , B01D71/82 , B01D2323/30 , B01J41/12 , B01J47/12 , C08G65/48 , C08G75/23 , C08G2650/02 , C08G2650/20 , C08J5/2256 , C08J5/2275 , C08J2371/00 , C08J2381/06 , C08L71/00 , C08L81/06 , C08L2312/00 , H01M8/0289 , H01M8/1027 , H01M8/1032 , H01M8/1034 , H01M8/1039 , H01M2008/1095 , H01M2300/0082 , H01M2300/0091 , Y02E60/523
摘要： A non crosslinked, covalently crosslinked and/or conically crosslinked polymer, having repeating units of the general formula (1) —K—R— (1) In which K is a bond, oxygen, sulfur, the radical R is a divalent radical of an aromatic or heteroaromatic compound.
摘要翻译：具有通式（1）-K-R-（1）的重复单元的非交联，共价交联和/或锥形交联的聚合物，其中K是键，氧，硫，基团R是芳族或杂芳族化合物。

8. 发明申请

US20120245237A1 IONOMERS WITH IONIC GROUPS IN THE SIDE CHAIN 失效
标题翻译：离子在侧链上的离子组
公开(公告)号：US20120245237A1
公开(公告)日：2012-09-27
申请号：US13330614
申请日：2011-12-19
申请人： Thomas Häring , Jochen Kerres , Martin Hein
发明人： Thomas Häring , Jochen Kerres , Martin Hein
IPC分类号： B01J39/18
CPC分类号： B01J39/185 , B01D67/0006 , B01D67/0093 , B01D71/68 , B01D71/82 , B01D2325/16 , B01J39/19 , C08G65/48 , C08G75/0286 , C08J5/2231 , C08J5/2256 , C08J2365/02 , C08J2381/06 , H01M8/0289 , H01M8/1023 , H01M8/1025 , H01M8/1027 , H01M8/103 , H01M8/1032 , H01M8/1039 , H01M8/1072 , H01M2300/0082 , Y02E60/523 , Y02P70/56
摘要： Ionomers and ionomer membranes with the ionic group on a flexible side chain have a positive impact on the proton conductivity of the ionomers. Various processes produce these polymeric proton conductors.
摘要翻译：在柔性侧链上具有离子基团的离子聚合物和离聚物膜对离聚物的质子传导性具有积极的影响。各种方法产生这些聚合物质子导体。

9. 发明申请

US20100092833A1 COMPOSITES AND COMPOSITE MEMBRANES 有权
标题翻译：复合材料和复合膜
公开(公告)号：US20100092833A1
公开(公告)日：2010-04-15
申请号：US12603017
申请日：2009-10-21
申请人： Jochen KERRES , Thomas HÄRING , Rima HÄRING
发明人： Jochen KERRES , Thomas HÄRING , Rima HÄRING
IPC分类号： H01M8/00 , B01J35/00 , B01D71/06
CPC分类号： B01D67/0041 , B01D69/141 , B01D71/00 , B01D71/024 , B01D71/62 , B01D71/68 , B01D2325/18 , B01D2325/26 , B01J21/16 , B01J31/10 , B01J31/1633 , B01J35/065 , C08J5/2275 , C08J2383/02 , H01M8/0289 , H01M8/1023 , H01M8/103 , H01M8/1032 , H01M8/1051 , H01M8/1081 , Y02E60/523 , Y02P70/56 , Y10T428/249953 , Y10T428/249969
摘要： The invention relates to a composite or a composite membrane consisting of an ionomer and of an inorganic optionally functionalized phyllosilicate. The isomer can be: (a) a cation exchange polymer; (b) an anion exchange polymer; (c) a polymer containing both anion exchanger groupings as well as cation exchanger groupings on the polymer chain; or (d) a blend consisting of (a) and (b), whereby the mixture ratio can range from 100% (a) to 100% (b). The blend can be ionically and even covalently cross-linked. The inorganic constituents can be selected from the group consisting of phyllosilicates or tectosilicates.
摘要翻译：本发明涉及由离聚物和无机任选官能化的页硅酸盐组成的复合膜或复合膜。异构体可以是：（a）阳离子交换聚合物; （b）阴离子交换聚合物; （c）聚合物链上含有阴离子交换剂组和聚合物链上的阳离子交换剂组的聚合物; 或（d）由（a）和（b）组成的共混物，其混合比可以在100％（a）至100％（b）的范围内。共混物可以是离子的，甚至共价交联的。无机成分可以选自页硅酸盐或三硅酸盐。

10. 发明授权

US07196151B2 Functionalized main chain polymers 失效
标题翻译：官能化主链聚合物
公开(公告)号：US07196151B2
公开(公告)日：2007-03-27
申请号：US10852594
申请日：2004-05-24
申请人： Thomas Häring
发明人： Thomas Häring
IPC分类号： C08F130/04 , C08G75/20
CPC分类号： B01D67/0093 , B01D69/141 , B01D71/52 , B01D71/68 , B01D71/80 , B01D71/82 , B01D2323/30 , B01J47/12 , C08G65/48 , C08J5/18 , C08J5/2218 , C08L71/10 , C08L79/04 , C08L81/06 , H01M8/1011 , H01M8/1023 , H01M8/1025 , H01M8/1027 , H01M8/103 , H01M8/1032 , H01M8/1048 , H01M8/1081 , H01M10/052 , H01M10/0565 , Y02E60/523 , Y02P70/56
摘要： A non crosslinked, covalently crosslinked and/or ionically crosslinked polymer, having repeating units of the general formula (1) —K—R— (1) In which K is a bond, oxygen, sulphur, the radical R is a divalent radical of an aromatic or heteroaromatic compound.
摘要翻译：非交联，共价交联和/或离子交联的聚合物，具有通式的重复单元

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