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1. 发明授权

US08790608B2 Siliceous materials having tunable porosity and surface morphology and methods of synthesizing same 有权
标题翻译：具有可调孔性和表面形态的硅质材料及其合成方法
公开(公告)号：US08790608B2
公开(公告)日：2014-07-29
申请号：US12209790
申请日：2008-09-12
申请人： Brian T. Holland , Sascha Welz
发明人： Brian T. Holland , Sascha Welz
IPC分类号： C01B33/00 , C01B33/12
CPC分类号： C01B33/126 , C01B33/193 , C01P2006/12 , C01P2006/14 , C01P2006/16 , Y10T428/2982 , Y10T428/2991
摘要： Non-spherical siliceous particles having a plurality of porous branches are disclosed and claimed. The porous branches are randomly oriented and elongated, ring-like, and/or aggregated. An additive introduced during synthesis of the particles modifies pore volume and morphology. The tunability of the pore volume includes an inner diameter ranging from about 2 Å to about 50,000 Å. Synthesizing the particles includes mixing under constant or intermittent stirring in a reaction vessel an aqueous silicic acid solution with an acidic heel solution to form a mixture. The stirring may optionally be performed at a variable speed. An additive is introduced into the mixture at a controlled rate, wherein the additive imposes a pH change from a lower pH to a higher pH to the mixture to induce siliceous particle precipitation. Optionally, a metal dopand may be introduced into the particles and/or at least a portion of an outer surface located outside of the pores and/or an inner surface located inside of the pores may be modified.
摘要翻译：公开并要求保护具有多个多孔分支的非球形硅质颗粒。多孔分支是随机取向的并且是细长的，环状的和/或聚集的。在合成颗粒期间引入的添加剂改变孔体积和形态。孔体积的可调性包括范围从约2到约50,000的内径。合成颗粒包括在反应容器中在恒定或间歇搅拌下混合含水硅酸溶液与酸性鞋底溶液以形成混合物。可以可选地以可变速度进行搅拌。将添加剂以受控的速率引入混合物中，其中添加剂将pH从较低的pH升高到较高的pH至混合物以诱导硅质颗粒沉淀。任选地，可以将金属掺杂物引入颗粒中，和/或位于孔外部的外表面的至少一部分和/或位于孔内部的内表面可以被修饰。

2. 发明申请

US20090220446A1 METHOD FOR TREATING HAIR 审中-公开
标题翻译：治疗头发的方法
公开(公告)号：US20090220446A1
公开(公告)日：2009-09-03
申请号：US12041081
申请日：2008-03-03
申请人： Yin Z. Hessefort , Brian T. Holland , Jeffery M. Atkins , Sascha Welz , Xiaojin Li
发明人： Yin Z. Hessefort , Brian T. Holland , Jeffery M. Atkins , Sascha Welz , Xiaojin Li
IPC分类号： A61K8/72 , A61Q5/00
CPC分类号： A61K8/817 , A61K8/8147 , A61Q5/12
摘要： A method of treating one or more hair shafts, each hair shaft including a cuticle layer and a cortex enclosed in the cuticle layer is disclosed. The method comprises: selecting one or more polymers that can penetrate the hair shafts with a pore size of about 5 angstroms to about 5000 angstroms; and treating the hair shafts by applying an effective amount of a composition containing said polymers to said hair shafts.
摘要翻译：公开了一种处理一个或多个毛发轴的方法，每个毛发轴包括角质层和包围在角质层中的皮质。该方法包括：选择一种或多种可以以大约5埃至大约5000埃的孔径穿透毛干的聚合物; 以及通过将有效量的含有所述聚合物的组合物施用到所述毛干来处理毛干。

3. 发明申请

US20070231249A1 Production and use of polysilicate particulate materials 审中-公开
标题翻译：生产和使用聚硅酸盐颗粒材料
公开(公告)号：US20070231249A1
公开(公告)日：2007-10-04
申请号：US11397134
申请日：2006-04-04
申请人： Francois Batllo , Brian Holland , John Krasniewski , Kim Long , Michael Romba , Sascha Welz , David Workman
发明人： Francois Batllo , Brian Holland , John Krasniewski , Kim Long , Michael Romba , Sascha Welz , David Workman
IPC分类号： C01B33/26
CPC分类号： C01B33/26 , A23L2/80 , B01J21/12 , B01J35/1019 , B01J35/1023 , B01J35/1042 , B01J35/1061 , B01J37/03 , B41M5/5218 , B82Y30/00 , C01B33/143 , C01B33/146 , C01B33/18 , C01P2004/64 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C09C1/3054 , D21H17/675 , D21H17/68 , D21H19/385 , D21H19/40 , D21H21/52
摘要： A method of preparing a particulate material comprising the steps of adding silicic acid solution, optionally doped with aluminum, optionally added to a slurry of pre-existing nanoparticles at a neutral to slightly acidic pH of no more than seven, and at a temperature of about 20° to 30° C. This yields a polysilicate particulate dispersion. Then, the pH of the dispersion is raised to greater than seven, to stabilize/reinforce particles of the particulate dispersion. Optionally, the particles may be dried, and have increased porosity and surface area.
摘要翻译：一种制备颗粒材料的方法，包括以下步骤：将任选地掺杂有铝的硅酸溶液任选加入到预先存在的纳米颗粒的浆液中，所述纳米颗粒在不大于7℃的中性至弱酸性pH和约7℃的温度下 20°至30℃。这产生聚硅酸盐颗粒分散体。然后，将分散体的pH提高到大于7，以稳定/增强颗粒分散体的颗粒。任选地，颗粒可以被干燥，并且具有增加的孔隙率和表面积。

4. 发明授权

US10227238B2 Production and use of polysilicate particulate materials 有权
公开(公告)号：US10227238B2
公开(公告)日：2019-03-12
申请号：US11397134
申请日：2006-04-04
申请人： Francois Batllo , Brian T. Holland , John M. Krasniewski , Kim M. Long , Michael A. Romba , Sascha Welz , David P. Workman
发明人： Francois Batllo , Brian T. Holland , John M. Krasniewski , Kim M. Long , Michael A. Romba , Sascha Welz , David P. Workman
IPC分类号： B01J21/12 , B01J35/10 , B01J37/03 , C09C1/30 , C01B33/18 , C01B33/26 , D21H17/67 , C01B33/143 , C01B33/146 , B82Y30/00 , B41M5/52 , A23L2/80 , D21H17/68 , D21H19/38 , D21H19/40 , D21H21/52
摘要： A method of preparing a particulate material comprising the steps of adding silicic acid solution, optionally doped with aluminum, optionally added to a slurry of pre-existing nanoparticles at a neutral to slightly acidic pH of no more than seven, and at a temperature of about 20° to 30° C. This yields a polysilicate particulate dispersion. Then, the pH of the dispersion is raised to greater than seven, to stabilize/reinforce particles of the particulate dispersion. Optionally, the particles may be dried, and have increased porosity and surface area.

5. 发明申请

US20100068519A1 SILICEOUS MATERIALS HAVING TUNABLE POROSITY AND SURFACE MORPHOLOGY AND METHODS OF SYNTHESIZING SAME 有权
标题翻译：具有可调节孔隙度和表面形态的硅质材料及其合成方法
公开(公告)号：US20100068519A1
公开(公告)日：2010-03-18
申请号：US12209790
申请日：2008-09-12
申请人： Brian T. Holland , Sascha Welz
发明人： Brian T. Holland , Sascha Welz
IPC分类号： C01B33/00 , B32B5/18 , B32B5/16
CPC分类号： C01B33/126 , C01B33/193 , C01P2006/12 , C01P2006/14 , C01P2006/16 , Y10T428/2982 , Y10T428/2991
摘要： Non-spherical siliceous particles having a plurality of porous branches are disclosed and claimed. The porous branches are randomly oriented and elongated, ring-like, and/or aggregated. An additive introduced during synthesis of the particles modifies pore volume and morphology. The tunability of the pore volume includes an inner diameter ranging from about 2 Å to about 50,000 Å. Synthesizing the particles includes mixing under constant or intermittent stirring in a reaction vessel an aqueous silicic acid solution with an acidic heel solution to form a mixture. The stirring may optionally be performed at a variable speed. An additive is introduced into the mixture at a controlled rate, wherein the additive imposes a pH change from a lower pH to a higher pH to the mixture to induce siliceous particle precipitation. Optionally, a metal dopand may be introduced into the particles and/or at least a portion of an outer surface located outside of the pores and/or an inner surface located inside of the pores may be modified.
摘要翻译：公开并要求保护具有多个多孔分支的非球形硅质颗粒。多孔分支是随机取向的并且是细长的，环状的和/或聚集的。在合成颗粒期间引入的添加剂改变孔体积和形态。孔体积的可调性包括范围从约2到约50,000的内径。合成颗粒包括在反应容器中在恒定或间歇搅拌下混合含水硅酸溶液与酸性鞋底溶液以形成混合物。可以可选地以可变速度进行搅拌。将添加剂以受控的速率引入混合物中，其中添加剂将pH从较低的pH升高到较高的pH至混合物以诱导硅质颗粒沉淀。任选地，可以将金属掺杂物引入颗粒中，和/或位于孔外部的外表面的至少一部分和/或位于孔内部的内表面可以被修饰。

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