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1. 发明授权

US10995400B2 Method of making coated article having antibacterial and/or antifungal coating and resulting product 有权
公开(公告)号：US10995400B2
公开(公告)日：2021-05-04
申请号：US13271828
申请日：2011-10-12
申请人： Rudolph Hugo Petrmichl , Jiangping Wang , Jason Barber
发明人： Rudolph Hugo Petrmichl , Jiangping Wang , Jason Barber
IPC分类号： C23C14/00 , C23C14/35 , C23C14/34 , C23C14/06 , C23C14/08 , C03C17/34 , C03C17/245 , C03C17/27 , C23C14/58 , A01N59/16
摘要： Techniques are provided for making a coated article including an antibacterial and/or antifungal coating. In certain example embodiments, the method includes providing a first sputtering target including Zr; providing a second sputtering target including Zn; and co-sputtering from at least the first and second sputtering targets in the presence of nitrogen to form a layer including ZnxZryNz on a glass substrate. These layers may be heat-treated or thermally tempered to form a single layer including ZnxZryOz. In other examples, two discrete layers of Zn and Zr may be formed. The coating may be heated or tempered to form a single layer including ZnxZryOz. Coated articles made using these methods may have antibacterial and/or antifungal properties.

2. 发明授权

US08435637B2 Scratch resistant coated glass article including carbide layer(s) resistant to fluoride-based etchant(s) 有权
标题翻译：包括耐氟化物腐蚀剂的耐磨涂层玻璃制品，
公开(公告)号：US08435637B2
公开(公告)日：2013-05-07
申请号：US12926979
申请日：2010-12-21
申请人： Nestor P. Murphy , Rudolph Hugo Petrmichl , Vijayan S. Veerasamy
发明人： Nestor P. Murphy , Rudolph Hugo Petrmichl , Vijayan S. Veerasamy
IPC分类号： B32B9/00
CPC分类号： C03C17/23 , C03C17/22 , C03C17/225 , C03C17/3417 , C03C17/3435 , C03C17/3441 , C03C17/3452 , C03C2217/215 , C03C2217/218 , C03C2217/228 , C03C2217/23 , C03C2217/281 , C03C2217/285 , C23C14/024 , C23C14/08 , C23C14/086 , C23C14/58 , Y10T428/26 , Y10T428/265 , Y10T428/30 , Y10T428/31627
摘要： A scratch resistant coated article is provided which is also resistant to attacks by at least some fluoride-based etchant(s) for at least a period of time. In certain example embodiments, an anti-etch layer(s) is provided on a glass substrate in order to protect the glass substrate from attacks by fluoride-based etchant(s). In certain example embodiments, the anti-etch layer(s) is substantially transparent to visible light. In certain embodiments, a DLC layer(s) may be provided over the anti-etch layer. An underlayer may be provided under the anti-etch layer(s) in certain example embodiments. In certain example embodiments, the anti-etch layer(s) may be of or include a carbide and/or oxycarbide of Zr, Sn or the like.
摘要翻译：提供了耐刮擦涂层制品，其还耐受至少一些基于氟化物的蚀刻剂至少一段时间的攻击。在某些示例性实施例中，在玻璃基板上提供抗蚀刻层，以便保护玻璃基板免受基于氟化物的蚀刻剂的攻击。在某些示例性实施例中，抗蚀刻层对可见光基本上是透明的。在某些实施例中，可以在抗蚀刻层上提供DLC层。在某些示例性实施例中，可以在抗蚀刻层下面设置底层。在某些示例性实施例中，抗蚀刻层可以是或包括Zr，Sn等的碳化物和/或碳氧化物。

3. 发明授权

US08354178B2 Coated article having diamond-like carbon (DLC) and protective film thereon 失效
标题翻译：具有类金刚石碳（DLC）和其上的保护膜的涂布制品
公开(公告)号：US08354178B2
公开(公告)日：2013-01-15
申请号：US12923775
申请日：2010-10-07
申请人： Nestor P. Murphy , Maximo Frati , Rudolph Hugo Petrmichl , Jiangping Wang , Jens-Peter Muller , Herbert Lage
发明人： Nestor P. Murphy , Maximo Frati , Rudolph Hugo Petrmichl , Jiangping Wang , Jens-Peter Muller , Herbert Lage
IPC分类号： B32B15/04
CPC分类号： C03C17/3441 , C03B27/012 , C03C17/3423 , C03C23/007 , C03C2217/78 , C03C2217/91 , C03C2218/322 , C03C2218/328 , C03C2218/355
摘要： There is provided a method of making a heat treated (HT) coated article to be used in shower door applications, window applications, or any other suitable applications where transparent coated articles are desired. For example, certain embodiments of this invention relate to a method of making a coated article including a step of heat treating a glass substrate coated with at least a layer of or including diamond-like carbon (DLC) and an overlying protective film thereon. In certain example embodiments, the protective film may be of or include an oxide of zinc. Following and/or during heat treatment (e.g., thermal tempering, or the like) the protective film may be removed. Other embodiments of this invention relate to the pre-HT coated article, or the post-HT coated article.
摘要翻译：提供了一种制造用于淋浴门应用，窗户应用或需要透明涂层制品的任何其它合适应用的热处理（HT）涂覆制品的方法。例如，本发明的某些实施方案涉及一种制备涂覆制品的方法，包括对涂覆有至少一层或类金刚石碳（DLC）的玻璃基板和其上覆盖的保护膜进行热处理的步骤。在某些示例性实施方案中，保护膜可以是或包括锌的氧化物。继续和/或在热处理（例如热回火等）期间，可以去除保护膜。本发明的其它实施方案涉及预HT涂覆制品或后HT涂覆制品。

4. 发明授权

US07879202B2 Scratch resistant coated glass article including carbide layer(s) resistant to fluoride-based etchant(s) 失效
公开(公告)号：US07879202B2
公开(公告)日：2011-02-01
申请号：US10989721
申请日：2004-11-17
申请人： Nestor P. Murphy , Rudolph Hugo Petrmichl , Vijayen S. Veerasamy
发明人： Nestor P. Murphy , Rudolph Hugo Petrmichl , Vijayen S. Veerasamy
IPC分类号： C23C14/34
CPC分类号： C23C14/58 , C03C17/22 , C03C17/23 , C03C17/3441 , C03C2217/282 , C03C2217/78 , C03C2218/155 , C03C2218/156 , C23C14/0057 , C23C14/024 , C23C14/06 , C23C14/0635 , C23C14/08 , C23C14/086
摘要： A scratch resistant coated article is provided which is also resistant to attacks by at least some fluoride-based etchant(s) for at least a period of time. In certain example embodiments, an anti-etch layer(s) is provided on a glass substrate in order to protect the glass substrate from attacks by fluoride-based etchant(s). In certain example embodiments, the anti-etch layer(s) is substantially transparent to visible light. In certain embodiments, a DLC layer(s) may be provided over the anti-etch layer. An underlayer may be provided under the anti-etch layer(s) in certain example embodiments. In certain example embodiments, the anti-etch layer(s) may be of or include a carbide and/or oxycarbide of Zr, Sn or the like.

5. 发明授权

US07833574B2 Method of making heat treated coated article using diamond-like carbon (DLC) coating and protective film 有权
标题翻译：使用类金刚石碳（DLC）涂层和保护膜制造热处理涂层制品的方法
公开(公告)号：US07833574B2
公开(公告)日：2010-11-16
申请号：US11699080
申请日：2007-01-29
申请人： Nestor P. Murphy , Maximo Frati , Rudolph Hugo Petrmichl , Jiangping Wang , Jens-Peter Muller , Herbert Lage
发明人： Nestor P. Murphy , Maximo Frati , Rudolph Hugo Petrmichl , Jiangping Wang , Jens-Peter Muller , Herbert Lage
IPC分类号： C23C16/26 , C23C16/40
CPC分类号： C03C17/3441 , C03B27/012 , C03C17/3423 , C03C23/007 , C03C2217/78 , C03C2217/91 , C03C2218/322 , C03C2218/328 , C03C2218/355
摘要： A method of making a heat treated (HT) coated article to be used in shower door applications, window applications, or any other suitable applications where transparent coated articles are desired. For example, certain embodiments of this invention relate to a method of making a coated article including a step of heat treating a glass substrate coated with at least a layer of or including diamond-like carbon (DLC) and an overlying protective film thereon. In certain example embodiments, the protective film may be of or include an oxide of zinc. Following and/or during heat treatment (e.g., thermal tempering, or the like) the protective film may be removed. Other embodiments of this invention relate to the pre-HT coated article, or the post-HT coated article.
摘要翻译：制造用于淋浴门应用，窗户应用或需要透明涂层制品的任何其它合适应用的热处理（HT）涂覆制品的方法。例如，本发明的某些实施方案涉及一种制备涂覆制品的方法，包括对涂覆有至少一层或类金刚石碳（DLC）的玻璃基板和其上覆盖的保护膜进行热处理的步骤。在某些示例性实施方案中，保护膜可以是或包括锌的氧化物。继续和/或在热处理（例如热回火等）期间，可以去除保护膜。本发明的其它实施方案涉及预HT涂覆制品或后HT涂覆制品。

6. 发明授权

US07510786B2 Coated article including titanium oxycarbide and method of making same 失效
标题翻译：包括碳氧化钛的涂层制品及其制造方法
公开(公告)号：US07510786B2
公开(公告)日：2009-03-31
申请号：US11389162
申请日：2006-03-27
申请人： Vijayen S. Veerasamy , Scott V. Thomsen , Rudolph Hugo Petrmichl
发明人： Vijayen S. Veerasamy , Scott V. Thomsen , Rudolph Hugo Petrmichl
IPC分类号： B32B9/04
CPC分类号： C23C14/5833 , C03C17/22 , C03C17/2456 , C03C2217/212 , C03C2217/282 , C03C2218/154 , C03C2218/32 , C23C14/06 , C23C14/083 , C23C14/48 , Y10T428/30 , Y10T428/31
摘要： A coated article is provided which includes a layer including titanium oxycarbide. In order to form the coated article, a layer of titanium oxide is deposited on a substrate by sputtering or the like. After sputtering of the layer including titanium oxide, an ion beam source(s) is used to implant at least carbon ions into the titanium oxide. When implanting, the carbon ions have sufficient ion energy so as to knock off oxygen (0) from TiOx molecules so as to enable a substantially continuous layer comprising titanium oxycarbide to form near a surface of the previously sputtered layer.
摘要翻译：提供了包括包含碳氧化钛的层的涂覆制品。为了形成被覆制品，通过溅射等将氧化钛层沉积在基板上。在溅射包括氧化钛的层之后，使用离子束源至少将碳离子注入到氧化钛中。当注入时，碳离子具有足够的离子能量，从而从TiOx分子中除去氧（0），以使得能够在先前溅射层的表面附近形成包含碳氧化钛的基本连续的层。

7. 发明授权

US07030390B2 Ion source with electrode kept at potential(s) other than ground by zener diode(s), thyristor(s) and/or the like 失效
标题翻译：具有通过齐纳二极管，晶闸管和/或类似物保持在除地电位之外的电极的离子源
公开(公告)号：US07030390B2
公开(公告)日：2006-04-18
申请号：US10919479
申请日：2004-08-17
申请人： Vijayen S. Veerasamy , Rudolph Hugo Petrmichl
发明人： Vijayen S. Veerasamy , Rudolph Hugo Petrmichl
IPC分类号： H01J27/00
CPC分类号： H01J37/08 , H01J27/143 , H01J2237/0206 , H01J2237/061
摘要： An ion source is provided, which generates or emits an ion beam which may be used to deposit a layer on a substrate, or the perform other functions. The ion source includes at least one anode and at least one cathode. In certain example embodiments, the cathode(s) is maintained or kept at a reference potential(s) other than ground for at least a period of time. This may be done, for example and without limitation, by electrically connecting a zener diode (single or double type, for example), thyristor (actively), or the like to the cathode. Thus, the ion source can be made so that it does not react adversely to its environment, and/or undesirable arcing between the anode and cathode can be reduced thereby improving ion source operation.
摘要翻译：提供离子源，其产生或发射可用于在衬底上沉积层的离子束或执行其它功能。离子源包括至少一个阳极和至少一个阴极。在某些示例性实施例中，阴极保持或保持在除地面以外的参考电位至少一段时间。这可以例如但不限于通过将齐纳二极管（例如单一或双类型），可控硅（主动）等电连接到阴极来完成。因此，可以使离子源不会对其环境产生不利影响，和/或可以减少阳极和阴极之间的不期望的电弧，从而改善离子源的操作。

8. 发明授权

US06740211B2 Method of manufacturing windshield using ion beam milling of glass substrate(s) 失效
标题翻译：使用玻璃基板的离子束铣削制造挡风玻璃的方法
公开(公告)号：US06740211B2
公开(公告)日：2004-05-25
申请号：US10074685
申请日：2002-02-14
申请人： Scott V. Thomsen , Rudolph Hugo Petrmichl , Anthony V. Longobardo , Vijayen S. Veerasamy , David R. Hall, Jr. , Henry Luten
发明人： Scott V. Thomsen , Rudolph Hugo Petrmichl , Anthony V. Longobardo , Vijayen S. Veerasamy , David R. Hall, Jr. , Henry Luten
IPC分类号： C23C1434
CPC分类号： C03C17/3618 , B32B17/10036 , B32B17/10174 , B32B17/10981 , C03C17/22 , C03C17/36 , C03C17/3626 , C03C17/3639 , C03C17/3644 , C03C17/3652 , C03C17/366 , C03C17/3681 , C03C23/006 , C03C2217/282 , C03C2218/31 , C03C2218/32 , C03C2218/36 , C03C2218/365 , Y10T156/1028 , Y10T428/24628 , Y10T428/315 , Y10T428/31623 , Y10T428/3163
摘要： This invention relates to a method of making a laminated window such as a vehicle windshield. At least one of the two glass substrates of the window is ion beam milled prior to heat treatment and lamination. As a result, defects in the resulting window and/or haze may be reduced.
摘要翻译：本发明涉及一种制造诸如车辆挡风玻璃的层压窗的方法。在热处理和层压之前，窗口的两个玻璃基板中的至少一个是离子束研磨的。结果，可能降低所得到的窗口和/或雾度中的缺陷。

9. 发明授权

US06504294B1 Method and apparatus for deposition of diamond-like carbon and silicon-doped diamond-like carbon coatings from a hall-current ion source 有权
标题翻译：用于从霍尔电流离子源沉积类金刚石碳和掺硅的类金刚石碳涂层的方法和装置
公开(公告)号：US06504294B1
公开(公告)日：2003-01-07
申请号：US09613684
申请日：2000-07-11
申请人： Leonard Joseph Mahoney , David Ward Brown , Rudolph Hugo Petrmichl
发明人： Leonard Joseph Mahoney , David Ward Brown , Rudolph Hugo Petrmichl
IPC分类号： H01J152
CPC分类号： C23C16/401 , C23C16/26 , C23C16/486 , G11B5/8408 , Y10S427/103 , Y10S427/104
摘要： A unique Hall-Current ion source apparatus is used for direct ion beam deposition of DLC coatings with hardness values greater than 10 GPa and at deposition rates greater than 10 Å per second. This ion source has a unique fluid-cooled anode with a shadowed gap through which ion sources feed gases are introduced while depositing gases are injected into the plasma beam. The shadowed gap provides a well maintained, electrically active area at the anode surface which stays relatively free of non-conductive deposits. The anode discharge region is insulatively sealed to prevent discharges from migrating into the interior of the ion source. A method is described in which a substrate is disposed within a vacuum chamber, coated with a coating of DLC or Si-DLC at a high deposition rate using a Hall-Current ion source operating on carbon-containing or carbon-containing and silicon-containing precursor gases, respectively. The method is particularly advantageous for producing thin, hard, wear resistant DLC and Si-DLC coatings for magnetic transducers and media used for magnetic data storage applications.
摘要翻译：独特的霍尔电流离子源设备用于DLC涂层的直接离子束沉积，硬度值大于10 GPa，沉积速率大于每秒10埃。该离子源具有独特的流体冷却阳极，其具有阴影间隙，通过该阴极间隙引入离子源进料气体，同时将等离子体束注入沉积气体。阴影间隙在阳极表面处提供良好维护的电活性区域，其保持相对不含非导电沉积物。阳极放电区被绝对密封，以防止放电进入离子源的内部。描述了一种方法，其中使用在含碳或含碳和含硅的操作的霍尔电流离子源，将衬底设置在真空室内，以高沉积速率涂覆DLC或Si-DLC的涂层前体气体。该方法特别有利于生产用于磁性数据存储应用的磁性换能器和介质的薄的，硬的耐磨DLC和Si-DLC涂层。

10. 发明授权

US06312808B1 Hydrophobic coating with DLC & FAS on substrate 有权
标题翻译： DLC和FAS在底物上的疏水涂层
公开(公告)号：US06312808B1
公开(公告)日：2001-11-06
申请号：US09617815
申请日：2000-07-17
申请人： Vijayen S. Veerasamy , Rudolph Hugo Petrmichl
发明人： Vijayen S. Veerasamy , Rudolph Hugo Petrmichl
IPC分类号： B32B900
CPC分类号： B08B17/06 , B05D5/083 , B08B17/065 , B32B17/1033 , B60S1/54 , B60S1/58 , C03C3/076 , C03C17/22 , C03C17/3441 , C03C17/3482 , C03C17/36 , C03C17/3634 , C03C17/3644 , C03C17/3652 , C03C17/42 , C03C23/0075 , C03C2217/282 , C03C2217/76 , C03C2217/78 , C03C2218/151 , C03C2218/31 , C23C16/26 , G02B5/208 , Y10T428/24983 , Y10T428/30 , Y10T428/31663
摘要： A substrate is coated with a hydrophobic coating system including diamond-like carbon (DLC) and at least one fluoro-alkyl silane (FAS) compound. In certain embodiments, the coating system includes an FAS inclusive layer provided over at least one DLC inclusive layer in order to increase the initial contact angle of the coated article.
摘要翻译：用包括类金刚石碳（DLC）和至少一种氟烷基硅烷（FAS）化合物的疏水涂层体系涂覆基材。在某些实施方案中，涂层系统包括在至少一个含DLC层上提供的包含FAS的层，以便增加涂覆制品的初始接触角。

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