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1. 发明授权

US4616095A Isomer-directed process for producing asymmetric ketones using catalytic claisen rearrangement of allylic ethers, intermediates, and uses of products and intermediates of process in perfumery 失效
标题翻译：使用烯丙基醚的催化裂化重排，中间体以及香料中的产品和中间体的产物和中间体来生产不对称酮的异构体定向方法
公开(公告)号：US4616095A
公开(公告)日：1986-10-07
申请号：US765342
申请日：1985-08-13
申请人： Mark A. Sprecker , Robert P. Belko , William L. Schreiber , Michael Licciardello
发明人： Mark A. Sprecker , Robert P. Belko , William L. Schreiber , Michael Licciardello
IPC分类号： C07C43/305 , C07C45/51 , C07C49/21 , C07C49/217 , C11B9/00
CPC分类号： C07C403/16 , C07C43/305 , C07C45/515 , C11B9/0015 , C11B9/0034 , C11B9/0061 , C07C2101/14 , C07C2101/16
摘要： Described is an isomer-directed process for producing asymmetric ketones defined according to the generic structure: ##STR1## wherein one of Z.sub.1 or Z.sub.2 is the moiety: ##STR2## and the other of Z.sub.1 or Z.sub.2 is hydrogen; wherein R.sub.11 and R.sub.21 represent hydrogen or the same or different alkyl or alkenyl with the proviso that R.sub.11 and R.sub.21 are not both hydrogen or wherein R.sub.11 and R.sub.21 taken together:(i) complete a cycloalkyl, cycloalkenyl, bicycloalkyl, mono or polyalkyl cycloakyl or mono or polyalkyl cycloalkenyl ring, or(ii) represent alkylidene, cycloalkenyl alkylidene, aralkylidene, mono or polyalkyl cycloalkenyl alkylidene or mono or polyalkyl aralkylidene;and wherein R.sub.6, R.sub.7 and R.sub.8 are the same or different and each represents hydrogen or methyl, using a catalytic Claisen rearrangement of allylic ethers previously formed by reacting substituted or unsubstituted allylic alcohols defined according to the structure: ##STR3## with dialkyl ketals defined according to the structure: ##STR4## wherein R.sub.4 and R.sub.5 represent the same or different C.sub.1 -C.sub.4 alkyl.Also described are compounds and processes for using same in perfumery defined according the structures: ##STR5## Also described are certain diallylic ethers defined according to the generic structure: ##STR6##
摘要翻译：描述了根据通用结构定义的不对称酮的异构体定向方法：其中Z1或Z2之一为部分：Z1和Z2中的另一个为氢; 其中R11和R21表示氢或相同或不同的烷基或烯基，条件是R11和R21不同时为氢或其中R11和R21一起组合：（i）完成环烷基，环烯基，双环烷基，单或多烷基环烷基或单或聚烷基环烯基环，或（ii）代表亚烷基，环烯基亚烷基，亚烷叉基，单或多烷基环烯基亚烷基或单或多烷基亚烷基; 并且其中R 6，R 7和R 8相同或不同，并且各自表示氢或甲基，使用以前通过使根据以下结构定义的取代或未取代的烯丙基醇反应形成的烯丙基醚的催化Claisen重排：＆lt; IMAGE＆gt; 结构：其中R 4和R 5表示相同或不同的C 1 -C 4烷基。还描述了在根据以下结构定义的香料中使用它们的化合物和方法：其中描述了根据以下结构定义的某些二烯丙基醚：到通用结构：

2. 发明授权

US4576741A Isomer-directed process for producing asymmetric ketones using catalytic Claisen rearrangement of allylic ethers, intermediates, and uses of products and intermediates of process in perfumery 失效
标题翻译：使用烯丙基醚的催化Claisen重排，中间体以及香料中产品和方法中间体的用途来生产不对称酮的异构体定向方法
公开(公告)号：US4576741A
公开(公告)日：1986-03-18
申请号：US671473
申请日：1984-11-14
申请人： Mark A. Sprecker , Robert P. Belko , William L. Schreiber , Michael Licciardello
发明人： Mark A. Sprecker , Robert P. Belko , William L. Schreiber , Michael Licciardello
IPC分类号： C07C43/305 , C07C45/51 , C11B9/00 , C11D3/50 , A61K7/46
CPC分类号： C07C403/16 , C07C43/305 , C07C45/515 , C11B9/0015 , C11B9/0034 , C11B9/0061 , C07C2101/14 , C07C2101/16
摘要： Described in an isomer-directed process for producing asymmetric ketones defined according to the generic structure: ##STR1## wherein one of Z.sub.1 or Z.sub.2 is the moiety: ##STR2## and the other of Z.sub.1 or Z.sub.2 is hydrogen; wherein R.sub.11 and R.sub.21 represent hydrogen or the same or different alkyl or alkenyl with the proviso that R.sub.11 and R.sub.21 are not both hydrogen or wherein R.sub.11 and R.sub.21 taken together:(i) complete a cycloalkyl, cycloalkenyl, bicycloalkyl, mono or polyalkyl cycloalkyl or mono or polyalkyl cycloalkenyl ring, or(ii) represent alkylidene, cycloalkenyl alkylidene, aralkylidene, mono or polyalkyl cycloalkenyl alkylidene or mono or polyalkyl aralkylidene;and wherein R.sub.6, R.sub.7 and R.sub.8 are the same or different and each represents hydrogen or methyl, using a catalytic Claisen rearrangement of allylic ethers previously formed by reacting substituted or unsubstituted allylic alcohols defined according to the structure: ##STR3## with dialkyl ketals defined according to the structure: ##STR4## wherein R.sub.4 and R.sub.5 represent the same or different C.sub.1 -C.sub.4 alkyl.Also described are compounds and processes for using same in perfumery defined according the structures: ##STR5## Also described are certain diallylic ethers defined according to the generic structure: ##STR6##
摘要翻译：描述于根据通用结构定义的用于制备不对称酮的异构体定向方法：其中Z1或Z2之一为部分：Z1或Z2中的另一个为氢; 其中R11和R21表示氢或相同或不同的烷基或烯基，条件是R11和R21不同时为氢或其中R11和R21一起组合：（i）完成环烷基，环烯基，双环烷基，单或多烷基环烷基或单或聚烷基环烯基环，或（ii）代表亚烷基，环烯基亚烷基，亚烷叉基，单或多烷基环烯基亚烷基或单或多烷基亚烷基; 并且其中R 6，R 7和R 8相同或不同，并且各自表示氢或甲基，使用以前通过使根据以下结构定义的取代或未取代的烯丙基醇反应形成的烯丙基醚的催化Claisen重排：＆lt; IMAGE＆gt; 结构：其中R 4和R 5表示相同或不同的C 1 -C 4烷基。还描述了在根据以下结构定义的香水中使用该化合物的化合物和方法：还描述了根据通用物质定义的某些二烯丙基醚结构：

3. 发明授权

US4488988A Methyl carbonate of .alpha.,3,3-trimethyl cyclohexane methanol, organoleptic uses thereof and process for preparing same 失效
标题翻译： α，3,3-三甲基环己烷甲醇的碳酸甲酯，其感官用途及其制备方法
公开(公告)号：US4488988A
公开(公告)日：1984-12-18
申请号：US532001
申请日：1983-09-14
申请人： Michael Licciardello , Richard M. Boden
发明人： Michael Licciardello , Richard M. Boden
IPC分类号： C11B9/00
CPC分类号： C11B9/0034
摘要： Described is the methyl carbonate of .alpha.,3,3-trimethyl cyclohexane methanol defined according to the structure: ##STR1## and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles such as solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softeners, fabric softener articles as well as hair sprays, shampoos and bath oils and perfumed polymers. Also described is a process for preparing the methyl carbonate of .alpha.,3,3-trimethyl cyclohexane methanol according to the reaction: ##STR2##
摘要翻译：描述了根据以下结构限定的α，3,3-三甲基环己烷甲醇的碳酸甲酯：其用于增强或增强香料组合物，古龙水和香料制品的香气，例如固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂，织物柔软剂制品以及喷发剂，洗发剂和浴油以及加香聚合物。还描述了根据以下反应制备α3,3-三甲基环己烷甲醇的碳酸甲酯的方法：

4. 发明授权

US4548743A Ketal and use in perfumery 失效
标题翻译：金属和用于香料
公开(公告)号：US4548743A
公开(公告)日：1985-10-22
申请号：US602646
申请日：1984-04-20
申请人： Mark A. Sprecker , Robert P. Belko , William L. Schreiber , Michael Licciardello
发明人： Mark A. Sprecker , Robert P. Belko , William L. Schreiber , Michael Licciardello
IPC分类号： A61K8/00 , A61K8/35 , A61Q13/00 , C07C43/30 , C07C43/305 , C07C45/00 , C07C45/51 , C07C49/20 , C07C49/203 , C07C49/217 , C07C49/557 , C07C67/00 , C07C401/00 , C07C403/00 , C07C403/14 , C07C403/16 , C11B9/00 , A61K7/46 , C07C43/32
CPC分类号： C07C403/16 , C07C43/305 , C07C45/515 , C07C49/203 , C07C49/217 , C07C49/557 , C11B9/0015 , C11B9/0034 , C11B9/0061 , C07C2101/14 , C07C2101/16
摘要： Described is the compound having the structure ##STR1## useful in perfumery.
摘要翻译：描述了具有用于香料的结构的化合物。

5. 发明授权

US4452730A Alkyl-4-cyclooctenyl carbonates and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles 失效
标题翻译：烷基-4-环辛烯基碳酸酯及其用于增强或增强香料组合物，古龙水和香料制品的香气的用途
公开(公告)号：US4452730A
公开(公告)日：1984-06-05
申请号：US496649
申请日：1983-05-20
申请人： Richard M. Boden , Michael Licciardello
发明人： Richard M. Boden , Michael Licciardello
IPC分类号： C11B9/00 , A61K7/46
CPC分类号： C11B9/0049
摘要： Described are the 4-cyclooctenyl alkyl carbonates defined according to the structure: ##STR1## wherein R.sub.4 is methyl or ethyl, reaction products including a major proportion of said 4-cyclooctenyl alkylcarbonates and a minor proportion of bicyclooctanyl carbonates having the structures: ##STR2## wherein R.sub.5 is methyl or ethyl, and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles such as solid or liquid anionic, cationic, nonionic or Zwitterionic detergents, fabric softeners, fabric softener articles, hair sprays, shampoos, bath oils and perfumed polymers.
摘要翻译：描述根据以下结构定义的4-环辛烯基烷基碳酸酯：其中R 4是甲基或乙基，反应产物包括主要比例的所述4-环辛烯基碳酸烷基酯和较小比例的具有以下结构的二环辛基碳酸酯：其中R5是甲基或乙基，以及其用于增强或增强香料组合物，古龙水和加香制品如固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂，织物柔软剂制品，喷发剂，洗发剂，沐浴油和加香聚合物。

6. 发明授权

US4368145A Perfume use for oxoalkyl esters 失效
标题翻译：香料用于氧代烷基酯
公开(公告)号：US4368145A
公开(公告)日：1983-01-11
申请号：US307366
申请日：1981-10-01
申请人： Michael Licciardello , Richard M. Boden , Hugh Watkins , Marie R. Hanna
发明人： Michael Licciardello , Richard M. Boden , Hugh Watkins , Marie R. Hanna
IPC分类号： C11B9/00 , A61K7/46
CPC分类号： C11B9/0015 , C11B9/0061
摘要： Described is a genus of compounds defined according to the structure: ##STR1## wherein Z represents carbinol having the structure: ##STR2## or carboxaldehyde having the structure: ##STR3## and wherein R represents 3-heptanyl or phenyl produced by (i) reacting a carboxylic acid with 2,2-dimethyl-1,3--propanediol to form the compound wherein Z represents carbinol; (ii) and then, if, desired, subsequently reacting the resulting alcohol to form an aldehyde; and organoleptic uses of such compounds in the field of perfumery, colognes and perfumed articles (e.g. perfumed polymers, or solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, drier-added fabric softener articles, hair preparations, hair sprays, bath preparations and the like).
摘要翻译：描述了根据以下结构定义的化合物属：其中Z表示具有以下结构的甲醇：具有以下结构的羧甲基，其中R表示3-庚基或苯基，其通过以下步骤制备：（i）与2,2-二甲基-1,3-丙二醇的羧酸形成其中Z代表甲醇的化合物; （ii）然后如果需要，随后使所得醇反应形成醛; 以及这些化合物在香料，古龙水和香料制品领域（如加香聚合物，固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，干燥剂添加织物柔软剂制品，头发制剂，喷发剂）中的感官用途，浴液等）。

7. 发明申请

US20060272199A1 Aqueous gel candle for use with a warming device 审中-公开
标题翻译：用于加温装置的水性凝胶蜡烛
公开(公告)号：US20060272199A1
公开(公告)日：2006-12-07
申请号：US11143104
申请日：2005-06-02
申请人： Michael Licciardello , Kathleen LaPierre
发明人： Michael Licciardello , Kathleen LaPierre
IPC分类号： C11C5/00
CPC分类号： A61L9/03 , C11C5/002
摘要： A candle that is formed from an aqueous gel containing an aqueous phase and an oil phase is provided. During use, the aqueous gel is heated to cause the evaporation of one or more volatile fragrances contained within the gel matrix into the surrounding environment. In one particular embodiment, for example, the candle is heated with a warming device other than a wick.
摘要翻译：提供由含有水相和油相的含水凝胶形成的蜡烛。在使用期间，将水性凝胶加热以使包含在凝胶基体内的一种或多种挥发性香料蒸发到周围环境中。在一个具体实施例中，例如，蜡烛用除了灯芯之外的加温装置加热。

8. 发明授权

US4933320A Isomer-directed process for producing asymmetric ketones using catalytic Claisen rearrangement of allylic ethers, intermediates, and uses of products and intermediates of process in perfumery 失效
标题翻译：使用烯丙基醚的催化Claisen重排，中间体以及香料中产品和方法中间体的用途来生产不对称酮的异构体定向方法
公开(公告)号：US4933320A
公开(公告)日：1990-06-12
申请号：US863983
申请日：1986-05-16
申请人： Mark A. Sprecker , Robert P. Belko , William L. Schreiber , Michael Licciardello
发明人： Mark A. Sprecker , Robert P. Belko , William L. Schreiber , Michael Licciardello
IPC分类号： C07C43/303 , C07C43/305 , C07C45/51 , C07C49/203 , C07C49/217 , C07C49/557 , C11B9/00
CPC分类号： C11B9/0034 , C07C403/10 , C07C403/16 , C07C43/303 , C07C43/305 , C07C45/515 , C07C49/203 , C07C49/217 , C07C49/557 , C07C2101/14 , C07C2101/16
摘要： Described is an isomer-directed process for producing asymmetric ketones defined according to the generic structure: ##STR1## wherein one of Z.sub.1 or Z.sub.2 is the moiety: ##STR2## and the other of Z.sub.1 or Z.sub.2 is hydrogen; wherein R.sub.11 and R.sub.21 represent hydrogen or the same or different alkyl or alkenyl with the proviso that R.sub.11 and R.sub.21 are not both hydrogen or wherein R.sub.11 and R.sub.21 taken together:(i) complete a cycloalkyl, cycloalkenyl, bicycloalkyl, mono or polyalkyl cycloalkyl or mono or polyalkyl cycloalkenyl ring, or(ii) represent alkylidene, cycloalkenyl alkylidene, aralkylidene, mono or polyalkyl cycloalkenyl alkylidene or mono or polyalkyl aralkylidene;and wherein R.sub.6, R.sub.7 and R.sub.8 are the same or different and each represents hydrogen or methyl, using a catalytic Claisen rearrangement of allylic ethers previously formed by reacting substituted or unsubstituted allylic alcohols defined according to the structure: ##STR3## with dialkyl ketals defined according to the structure: ##STR4## wherein R.sub.4 and R.sub.5 represent the same or different C.sub.1 -C.sub.4 alkyl.Also described are compounds and processes for using same in perfumery defined according the structures: ##STR5## Also described are certain diallylic ethers defined according to the generic structure: ##STR6##
摘要翻译：描述了根据通用结构定义的不对称酮的异构体定向方法：其中Z1或Z2之一为部分：Z1和Z2中的另一个为氢; 其中R11和R21表示氢或相同或不同的烷基或烯基，条件是R11和R21不同时为氢或其中R11和R21一起组合：（i）完成环烷基，环烯基，双环烷基，单或多烷基环烷基或单或聚烷基环烯基环，或（ii）代表亚烷基，环烯基亚烷基，亚烷叉基，单或多烷基环烯基亚烷基或单或多烷基亚烷基; 并且其中R 6，R 7和R 8相同或不同，并且各自表示氢或甲基，使用以前通过使根据以下结构定义的取代或未取代的烯丙基醇反应形成的烯丙基醚的催化Claisen重排：＆lt; IMAGE＆gt; 结构：其中R 4和R 5表示相同或不同的C 1 -C 4烷基。还描述了根据以下结构定义的香水中使用它们的化合物和方法： + TR 是根据通用结构定义的某些二烯丙基醚：

9. 发明授权

US4425265A Branched chain alkenyl methyl carbonates, uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles and formate intermediates useful in preparing same 失效
标题翻译：支链链烯基甲基碳酸酯，其用于增强或增强香料组合物，古龙水和香料制品的香气以及可用于制备它的甲酸酯中间体
公开(公告)号：US4425265A
公开(公告)日：1984-01-10
申请号：US422526
申请日：1982-09-23
申请人： Richard M. Boden , Theodore J. Tyszkiewicz , Michael Licciardello
发明人： Richard M. Boden , Theodore J. Tyszkiewicz , Michael Licciardello
IPC分类号： C07C45/46 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0015 , C07C45/46 , C07C67/08 , C07C68/06
摘要： Described are branched chain alkenyl methyl carbonates and branched chain alkenyl formates defined according to the structure: ##STR1## wherein R.sub.3 represents hydrogen or methoxy and wherein in each of the molecules described by the structure, one of the dashed lines is a carbon-carbon double bond and each of the other of the dashed lines is a carbon-carbon single bond; and uses of the compounds wherein R.sub.3 is methoxy in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles such as solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, hair sprays, shampoos, bath oils and plastic fragrances.
摘要翻译：描述了根据以下结构定义的支链链烯基甲基碳酸酯和支链烯基甲酸酯：其中R 3表示氢或甲氧基，并且其中在由结构描述的每个分子中，虚线之一是碳 - 碳双并且虚线中的每一个都是碳 - 碳单键; 以及其中R3为甲氧基的化合物在增加或增强香料组合物，古龙水和香料制品如固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，发胶，洗发剂，沐浴油和塑料香水。

10. 发明授权

US4398038A Oxoalkyl esters 失效
标题翻译：氧代烷基酯
公开(公告)号：US4398038A
公开(公告)日：1983-08-09
申请号：US396290
申请日：1982-07-08
申请人： Michael Licciardello , Richard M. Boden , Hugh Watkins , Marie R. Hanna
发明人： Michael Licciardello , Richard M. Boden , Hugh Watkins , Marie R. Hanna
IPC分类号： C07D319/08 , C11B9/00 , C07C69/76
CPC分类号： C07D319/08 , C11B9/0015 , C11B9/0061 , Y02P20/582
摘要： Described is a genus of compounds defined according to the structure: ##STR1## wherein Z represents carbinol having the structure: ##STR2## or carboxaldehyde having the structure: ##STR3## and wherein R represents 3-heptanyl or phenyl produced by (i) reacting a carboxylic acid with 2,2-dimethyl-1,3-propanediol to form the compound wherein Z represents carbinol; (ii) and then, if desired, subsequently reacting the resulting alcohol to form an aldehyde; and organoleptic uses of such compounds in the field of perfumery, colognes and perfumed articles (e.g. perfumed polymers, or solid or liquid anionic, cationic, nonionic or switterionic detergents, fabric softener compositions, drier-added fabric softener articles, hair preparations, hair sprays, bath preparations and the like).
摘要翻译：描述了根据以下结构定义的化合物属：其中Z表示具有以下结构的甲醇：具有以下结构的羧甲基，其中R表示3-庚基或苯基，其通过以下步骤制备：（i）与2,2-二甲基-1,3-丙二醇的羧酸形成其中Z代表甲醇的化合物; （ii）然后，如果需要，随后使所得醇反应形成醛; 以及这些化合物在香料，古龙水和香料制品领域（例如加香聚合物，或固体或液体阴离子，阳离子，非离子或转换洗涤剂，织物柔软剂组合物，干燥剂加入的织物柔软剂制品，头发制剂，喷发剂）中的感官用途，浴液等）。

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