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1. 发明授权

US4398038A Oxoalkyl esters 失效
标题翻译：氧代烷基酯
公开(公告)号：US4398038A
公开(公告)日：1983-08-09
申请号：US396290
申请日：1982-07-08
申请人： Michael Licciardello , Richard M. Boden , Hugh Watkins , Marie R. Hanna
发明人： Michael Licciardello , Richard M. Boden , Hugh Watkins , Marie R. Hanna
IPC分类号： C07D319/08 , C11B9/00 , C07C69/76
CPC分类号： C07D319/08 , C11B9/0015 , C11B9/0061 , Y02P20/582
摘要： Described is a genus of compounds defined according to the structure: ##STR1## wherein Z represents carbinol having the structure: ##STR2## or carboxaldehyde having the structure: ##STR3## and wherein R represents 3-heptanyl or phenyl produced by (i) reacting a carboxylic acid with 2,2-dimethyl-1,3-propanediol to form the compound wherein Z represents carbinol; (ii) and then, if desired, subsequently reacting the resulting alcohol to form an aldehyde; and organoleptic uses of such compounds in the field of perfumery, colognes and perfumed articles (e.g. perfumed polymers, or solid or liquid anionic, cationic, nonionic or switterionic detergents, fabric softener compositions, drier-added fabric softener articles, hair preparations, hair sprays, bath preparations and the like).
摘要翻译：描述了根据以下结构定义的化合物属：其中Z表示具有以下结构的甲醇：具有以下结构的羧甲基，其中R表示3-庚基或苯基，其通过以下步骤制备：（i）与2,2-二甲基-1,3-丙二醇的羧酸形成其中Z代表甲醇的化合物; （ii）然后，如果需要，随后使所得醇反应形成醛; 以及这些化合物在香料，古龙水和香料制品领域（例如加香聚合物，或固体或液体阴离子，阳离子，非离子或转换洗涤剂，织物柔软剂组合物，干燥剂加入的织物柔软剂制品，头发制剂，喷发剂）中的感官用途，浴液等）。

2. 发明授权

US4390435A Oxoalkyl esters, organoleptic uses thereof and process for preparing same 失效
标题翻译：氧代烷基酯，感官用途及其制备方法
公开(公告)号：US4390435A
公开(公告)日：1983-06-28
申请号：US396252
申请日：1982-07-08
申请人： Michael Licciardello , Richard M. Boden , Hugh Watkins , Marie R. Hanna
发明人： Michael Licciardello , Richard M. Boden , Hugh Watkins , Marie R. Hanna
IPC分类号： C11B9/00 , D06M13/00 , D06M13/12
CPC分类号： D06M13/005 , C11B9/0015 , C11B9/0061
摘要： Described is a genus of compounds defined according to the structure: ##STR1## wherein Z represents carbinol having the structure: ##STR2## or carboxaldehyde having the structure: ##STR3## and wherein R represents 3-heptanyl or phenyl produced by (i) reacting a carboxylic acid with 2,2-dimethyl-1,3-propanediol to form the compound wherein Z represents carbinol; (ii) and then, if, desired, subsequently reacting the resulting alcohol to form an aldehyde; and organoleptic uses of such compounds in the field of perfumery, colognes and perfumed articles (e.g. perfumed polymers, or solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, drier-added fabric softener articles, hair preparations, hair sprays, bath preparations and the like).
摘要翻译：描述了根据以下结构定义的化合物属：其中Z表示具有以下结构的甲醇：具有以下结构的羧甲基，其中R表示3-庚基或苯基，其通过以下步骤制备：（i）与2,2-二甲基-1,3-丙二醇的羧酸形成其中Z代表甲醇的化合物; （ii）然后如果需要，随后使所得醇反应形成醛; 以及这些化合物在香料，古龙水和香料制品领域（如加香聚合物，固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，干燥剂添加织物柔软剂制品，头发制剂，喷发剂）中的感官用途，浴液等）。

3. 发明授权

US4368145A Perfume use for oxoalkyl esters 失效
标题翻译：香料用于氧代烷基酯
公开(公告)号：US4368145A
公开(公告)日：1983-01-11
申请号：US307366
申请日：1981-10-01
申请人： Michael Licciardello , Richard M. Boden , Hugh Watkins , Marie R. Hanna
发明人： Michael Licciardello , Richard M. Boden , Hugh Watkins , Marie R. Hanna
IPC分类号： C11B9/00 , A61K7/46
CPC分类号： C11B9/0015 , C11B9/0061
摘要： Described is a genus of compounds defined according to the structure: ##STR1## wherein Z represents carbinol having the structure: ##STR2## or carboxaldehyde having the structure: ##STR3## and wherein R represents 3-heptanyl or phenyl produced by (i) reacting a carboxylic acid with 2,2-dimethyl-1,3--propanediol to form the compound wherein Z represents carbinol; (ii) and then, if, desired, subsequently reacting the resulting alcohol to form an aldehyde; and organoleptic uses of such compounds in the field of perfumery, colognes and perfumed articles (e.g. perfumed polymers, or solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, drier-added fabric softener articles, hair preparations, hair sprays, bath preparations and the like).
摘要翻译：描述了根据以下结构定义的化合物属：其中Z表示具有以下结构的甲醇：具有以下结构的羧甲基，其中R表示3-庚基或苯基，其通过以下步骤制备：（i）与2,2-二甲基-1,3-丙二醇的羧酸形成其中Z代表甲醇的化合物; （ii）然后如果需要，随后使所得醇反应形成醛; 以及这些化合物在香料，古龙水和香料制品领域（如加香聚合物，固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，干燥剂添加织物柔软剂制品，头发制剂，喷发剂）中的感官用途，浴液等）。

4. 发明授权

US4404307A Oxoalkyl esters, organoleptic uses thereof and process for preparing same 失效
公开(公告)号：US4404307A
公开(公告)日：1983-09-13
申请号：US396257
申请日：1982-07-08
申请人： Michael Licciardello , Richard M. Boden , Hugh Watkins , Marie R. Hanna
发明人： Michael Licciardello , Richard M. Boden , Hugh Watkins , Marie R. Hanna
IPC分类号： C08K5/10 , C11B9/00 , C08K5/09 , C08K5/12 , C08K5/13
CPC分类号： A61Q1/12 , A61K8/8111 , A61Q5/06 , C08K5/10 , C11B9/0015 , C11B9/0061 , A61Q5/02 , A61Q5/12 , Y02P20/582
摘要： Described is a genus of compounds defined according to the structure: ##STR1## wherein Z represents carbinol having the structure: ##STR2## or carboxaldehyde having the structure: ##STR3## and wherein R represents 3-heptanyl or phenyl produced by (i) reacting a carboxylic acid with 2,2-dimethyl-1,3-propanediol to form the compound wherein Z represents carbinol; (ii) and then, if, desired, subsequently reacting the resulting alcohol to form an aldehyde; and organoleptic uses of such compounds in the field of perfumery, colognes and perfumed articles (e.g. perfumed polymers, or solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, drier-added fabric softener articles, hair preparations, hair sprays, bath preparations and the like).

5. 发明授权

US4400290A Process for augmenting or enchancing the aroma of detergent compositions using oxyalkyl esters 失效
标题翻译：使用氧烷基酯增强或增强洗涤剂组合物的香气的方法
公开(公告)号：US4400290A
公开(公告)日：1983-08-23
申请号：US396289
申请日：1982-07-08
申请人： Michael Licciardello , Richard M. Boden , Hugh Watkins , Marie R. Hanna
发明人： Michael Licciardello , Richard M. Boden , Hugh Watkins , Marie R. Hanna
IPC分类号： C11B9/00 , C11D3/50
CPC分类号： C11D3/50 , C11B9/0015 , C11B9/0061
摘要： Described is a genus of compounds defined according to the structure: ##STR1## wherein Z represents carbinol having the structure: ##STR2## or carboxaldehyde having the structure: ##STR3## and wherein R represents 3-heptanyl or phenyl produced by (i) reacting a carboxylic acid with 2,2-dimethyl-1,3-propanediol to form the compound wherein Z represents carbinol; (ii) and then, if, desired, subsequently reacting the resulting alcohol to form an aldehyde; and organoleptic uses of such compounds in the field of perfumery, colognes and perfumed articles (e.g. perfumed polymers, or solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, drier-added fabric softener articles, hair preparations, hair sprays, bath preparations and the like).
摘要翻译：描述了根据以下结构定义的化合物属：其中Z表示具有以下结构的甲醇：具有以下结构的羧甲基，其中R表示3-庚基或苯基，其通过以下步骤制备：（i）与2,2-二甲基-1,3-丙二醇的羧酸形成其中Z代表甲醇的化合物; （ii）然后如果需要，随后使所得醇反应形成醛; 以及这些化合物在香料，古龙水和香料制品领域（如加香聚合物，固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，干燥剂添加织物柔软剂制品，头发制剂，喷发剂）中的感官用途，浴液等）。

6. 发明授权

US4460795A Process for preparing mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives 失效
公开(公告)号：US4460795A
公开(公告)日：1984-07-17
申请号：US478355
申请日：1983-03-24
申请人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
发明人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
IPC分类号： A24B15/34 , C07C47/347 , C07C47/445 , C07C93/16
CPC分类号： A24B15/345 , C07C47/347 , C07C47/445
摘要： Described are mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives having the generic structure: ##STR1## wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond; wherein R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 "', R.sub.1 "", R.sub.3, R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 "', R.sub.5 "" and R.sub.6 represent hydrogen or methyl with the provisos:(i) at least four of R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 "' and R.sub.1 "" are hydrogen; and (ii) at least four of R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 "' and R.sub.5 "" represent hydrogen;and wherein Z represents one of the moieties:(i) carboxaldehyde having the structure: ##STR2## (ii) alkylene dioxy or dialkoxy methyl having the structure: ##STR3## (iii) hydroxy methyl having the structure: ##STR4## (iv) acetoxymethyl having the structure: ##STR5## and wherein R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl or R.sub.7 and R.sub.8 taken together represent C.sub.2 -C.sub.4 alkylene; wherein the line represented by:[++++]is either (i) a carbon-carbon single bond when R.sub.7 and R.sub.8 taken together are C.sub.2 -C.sub.4 alkylene or (ii) no bond at all when R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl. Also described are processes for preparing such mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives, and processes for using the above defined mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives for their organoleptic properties and compositions containing said mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives including perfumes, perfumed articles (such as solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfumed polymers, fabric softeners and cosmetic powders), foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, smoking tobaccos and smoking tobacco articles.

7. 发明授权

US4448984A Mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives 失效
公开(公告)号：US4448984A
公开(公告)日：1984-05-15
申请号：US458890
申请日：1983-01-18
申请人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
发明人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
IPC分类号： A24B15/34 , C07C47/347 , C07C47/445 , C07C43/162 , C07C35/28 , C07C67/035 , C07C67/04
CPC分类号： A24B15/345 , C07C47/347 , C07C47/445
摘要： Described are mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives having the generic structure: ##STR1## wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond; wherein R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '", R.sub.1 "", R.sub.3, R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '", R.sub.5 "" and R.sub.6 represent hydrogen or methyl with the provisos:(i) at least four of R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '" and R.sub.1 "" are hydrogen; and (ii) at least four of R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '" and R.sub.5 "" represent hydrogen;and wherein Z represents one of the moieties:(i) carboxaldehyde having the structure: ##STR2## (ii) alkylene dioxy or dialkoxy methyl having the structure: ##STR3## (iii) hydroxy methyl having the structure: ##STR4## (iv) acetoxymethyl having the structure: ##STR5## and wherein R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl or R.sub.7 and R.sub.8 taken together represent C.sub.2 -C.sub.4 alkylene; wherein the line represented by:[++++] is either (i) a carbon-carbon single bond when R.sub.7 and R.sub.8 taken together are C.sub.2 -C.sub.4 alkylene or (ii) no bond at all when R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl. Also described are processes for preparing such mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives, and processes for using the above defined mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives for their organoleptic properties and compositions containing said mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives including perfumes, perfumed articles (such as solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfumed polymers, fabric softeners and cosmetic powders), foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, smoking tobaccos and smoking tobacco articles.

8. 发明授权

US4391284A Use in modifying smoking tobacco aroma and flavor or mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives 失效
标题翻译：用于改变吸烟烟草香气和风味或单氧甲基取代的多羟基甲基萘衍生物
公开(公告)号：US4391284A
公开(公告)日：1983-07-05
申请号：US354387
申请日：1982-03-02
申请人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
发明人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
IPC分类号： A24B15/34 , C07C47/347 , C07C47/445 , A24B3/12 , A24B15/30
CPC分类号： A24B15/345 , C07C47/347 , C07C47/445
摘要： Described is the use in modifying, augmenting or enhancing the aroma or taste of smoking tobacco products of mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives having the generic structure: ##STR1## wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond; wherein R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '", R.sub.1 "", R.sub.3, R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '", R.sub.5 "" and R.sub.6 represent hydrogen or methyl with the provisos:(i) at least four of R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '" and R.sub.1 "" are hydrogen; and (ii) at least four of R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '" and R.sub.5 "" represent hydrogen;and wherein Z represents one of the moieties:(i) carboxaldehyde having the structure: ##STR2## (ii) alkylene dioxy or dialkoxy methyl having the structure: ##STR3## (iii) hydroxy methyl having the structure: ##STR4## (iv) acetoxymethyl having the structure: ##STR5## and wherein R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl or R.sub.7 and R.sub.8 taken together represent C.sub.2 -C.sub.4 alkylene; wherein the line represented by:[++++]is either (i) a carbon-carbon single bond when R.sub.7 and R.sub.8 taken together are C.sub.2 -C.sub.4 alkylene or (ii) no bond at all when R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl.
摘要翻译：描述了用于改变，增强或增强具有以下通用结构的单氧代甲基取代的多羟基甲基萘衍生物的烟草产品的香气或味道：其中虚线表示碳 - 碳单键或碳 - 碳双键; 其中R1，R1'，R1“，R1”，R1“，R3，R5，R5'，R5”，R5“，R5”和R6表示氢或甲基，条件：（i）R1，R1'，R1“，R1”和R1“”中的至少四个为氢; 和（ii）R5，R5'，R5“，R5”和R5“中的至少四个表示氢; （ⅰ）具有以下结构的甲醛：（ⅱ）具有以下结构的亚烷基二氧基或二烷氧基甲基：（ⅲ）具有以下结构的羟基甲基：（ⅳ）具有以下结构的乙酰氧基甲基：其中R7和R8分别代表C1-C4低级烷基或R7和R8一起代表C2-C4亚烷基; 其中由以下各项表示的线：[++++]是（i）当R 7和R 8一起为C 2 -C 4亚烷基时的碳 - 碳单键或（ii）当R7和R8分别表示C1 -C4低级烷基。

9. 发明授权

US4576742A Perfume uses of reactive product containing mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives 失效
公开(公告)号：US4576742A
公开(公告)日：1986-03-18
申请号：US570100
申请日：1984-01-12
申请人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
发明人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
IPC分类号： A24B15/34 , C07C47/347 , C07C47/445 , A61K7/46 , C11B9/00
CPC分类号： A24B15/345 , C07C47/347 , C07C47/445
摘要： Described are mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives having the generic structure: ##STR1## wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond; wherein R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '", R.sub.1 "", R.sub.3, R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '", R.sub.5 "" and R.sub.6 represent hydrogen or methyl with the provisos:(i) at least four of R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '" and R.sub.1 "" are hydrogen; and (ii) at least four of R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '" and R.sub.5 "" represent hydrogen;and wherein Z represents one of the moieties;(i) carboxaldehyde having the structure: ##STR2## (ii) alkylene dioxy or dialkoxy methyl having the structure: ##STR3## (iii) hydroxy methyl having the structure: ##STR4## (iv) acetoxymethyl having the structure: ##STR5## and wherein R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl or R.sub.7 and R.sub.8 taken together represent C.sub.2 -C.sub.4 alkylene; wherein the line represented by:[++++]is either (i) a carbon-carbon single bond when R.sub.7 and R.sub.8 taken together are C.sub.2 -C.sub.4 alkylene or (ii) no bond at all when R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl. Also described are processes for preparing such mono-oxomethyl substituted polyhydrodimethanonaphthalene derivative, and processes for using the above defined mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives, for their organoleptic properties and compositions containing said mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives including perfumes, perfumed articles (such as solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfumed polymers, fabric softeners and cosmetic powders), foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, smoking tobaccos and smoking tobacco articles.

10. 发明授权

US4476042A Mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives, organoleptic uses thereof and processes for preparing same 失效
公开(公告)号：US4476042A
公开(公告)日：1984-10-09
申请号：US546384
申请日：1983-10-28
申请人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
发明人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
IPC分类号： A24B15/34 , C07C47/347 , C07C47/445 , A61K7/46 , C11B9/00
CPC分类号： A24B15/345 , C07C47/347 , C07C47/445
摘要： Described are mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives having the generic structure: ##STR1## wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond; wherein R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '", R.sub.1 "", R.sub.3, R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '", R.sub.5 "" and R.sub.6 represents hydrogen or methyl with the provisos:(i) at least four of R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '" and R.sub.1 "" are hydrogen; and (ii) at least four of R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '" and R.sub.5 "" represent hydrogen;and wherein Z represents one of the moieties:(i) carboxaldehyde having the structure: ##STR2## (ii) alkylene dioxy or dialkoxy methyl having the structure: ##STR3## (iii) hydroxy methyl having the structure: ##STR4## (iv) acetoxymethyl having the structure: ##STR5## and wherein R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl or R.sub.7 and R.sub.8 taken together represent C.sub.2 -C.sub.4 alkylene; wherein the line represented by:[++++]is either (i) a carbon-carbon single bond when R.sub.7 and R.sub.8 taken together are C.sub.2 -C.sub.4 alkylene or (ii) no bond at all when R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl. Also described are processes for preparing such mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives, and processes for using the above defined mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives for their organoleptic properties and compositions containing said mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives including perfumes, perfumed articles (such as solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfumed polymers, fabric softeners and cosmetic powders), foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, smoking tobaccos and smoking tobacco articles.

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