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1. 发明授权

US5387638A Emulsion composition 失效
标题翻译：乳液组成
公开(公告)号：US5387638A
公开(公告)日：1995-02-07
申请号：US111536
申请日：1993-08-25
申请人： Masato Nakamae , Ken Yuki , Hirotoshi Miyazaki , Hitoshi Maruyama
发明人： Masato Nakamae , Ken Yuki , Hirotoshi Miyazaki , Hitoshi Maruyama
IPC分类号： C08F2/24 , D21H19/58 , D21H19/62 , C08L29/00
CPC分类号： D21H19/62 , C08F2/24 , D21H19/58
摘要： There is disclosed an emulsion composition which comprises an aqueous emulsion (A) obtained by emulsion polymerization of 100 parts by weight of an ethylenically unsaturated monomer in the presence of 1 to 15 parts by weight of a carboxyl group-modified polyvinyl alcohol such as itaconic acid-modified polyvinyl alcohol as the dispersant and a polyamide resin (B) such as polyamide epichlorohydrin. The above emulsion composition has a long pot-life and can easily be made into a film having a high wet strength and being excellent in water resistance, hot water resistance and heat resistance. Accordingly, it can effectively be utilized in a variety of applications including paint coating, adhesive, fiber sizing agent and paper coating.
摘要翻译：公开了一种乳液组合物，其包含在1〜15重量份的羧基改性的聚乙烯醇如衣康酸的存在下，通过100重量份的烯属不饱和单体的乳液聚合获得的水性乳液（A）改性聚乙烯醇作为分散剂，聚酰胺树脂（B）如聚酰胺表氯醇。上述乳液组合物的使用寿命长，可以容易地制成具有高湿强度，耐水性，耐热水性和耐热性优异的膜。因此，它可以有效地用于各种应用，包括涂料涂料，粘合剂，纤维施胶剂和纸张涂布。

2. 发明授权

US5349008A Process for suspension polymerization of vinyl compound 失效
标题翻译：乙烯基化合物的悬浮聚合方法
公开(公告)号：US5349008A
公开(公告)日：1994-09-20
申请号：US778125
申请日：1991-12-04
申请人： Shigeki Takada , Ken Yuki , Hitoshi Maruyama , Taku Tanaka , Kazunari Igarashi
发明人： Shigeki Takada , Ken Yuki , Hitoshi Maruyama , Taku Tanaka , Kazunari Igarashi
IPC分类号： C08F2/20 , C08F2/38 , C08L29/04
CPC分类号： C08F2/20
摘要： Disclosed herein is a process for suspension polymerization of a vinyl polymer which comprises using as the suspending agent a polyvinyl ester polymer having an ionic group at an end thereof or a polyvinyl alcohol polymer having a degree of hydrolysis of 90 mol % or less which is obtained by hydrolysis of the above polyvinyl ester polymer.According to the above-mentioned process, vinyl polymer granules having a sharp granulometric dispersion, high bulk density, high plasticizer absorption and low vinyl monomer residue are obtained.
摘要翻译： PCT No.PCT / JP91 / 00420 Sec。 371 1991年12月4日第 102（e）日期1991年12月4日PCT 1991年3月29日PCT公布。出版物WO91 / 15518 日期为1991年10月17日。本文公开了一种乙烯基聚合物的悬浮聚合方法，其包括使用其末端具有离子基团的聚乙烯基酯聚合物或水解度为90的聚乙烯醇聚合物作为悬浮剂 mol％以下，通过上述聚乙烯基酯聚合物的水解得到。根据上述方法，得到具有尖锐粒度分散，高堆积密度，高增塑剂吸收性和低乙烯基单体残基的乙烯基聚合物颗粒。

3. 发明授权

US5310790A Process for producing polyvinyl ester having a high degree of polymerization and process for producing polyvinyl alcohol having a high degree of polymerization 失效
标题翻译：具有高聚合度的聚乙烯酯的制造方法和具有高聚合度的聚乙烯醇的制造方法
公开(公告)号：US5310790A
公开(公告)日：1994-05-10
申请号：US82162
申请日：1993-06-28
申请人： Toshiaki Sato , Ken Yuki , Junnosuke Yamauchi , Takuji Okaya
发明人： Toshiaki Sato , Ken Yuki , Junnosuke Yamauchi , Takuji Okaya
IPC分类号： C08F2/30 , C08F8/12 , C08F18/04 , C08G63/91
CPC分类号： C08F18/04 , C08F8/12
摘要： Disclosed herein is a new process for producing polyvinyl ester having a high degree of polymerization having an intrinsic viscosity not less than 1.5 dl/g, preferably not less than 2.2 dl/g, and most preferably higher than 3.2 dl/g, said process comprising subjecting vinyl ester monomer to low-temperature emulsion polymerization under specific conditions.Disclosed also herein is a new process for producing polyvinyl alcohol having a high degree of polymerization having an intrinsic viscosity not less than 1.5 dl/g, preferably not less than 2.2 dl/g, and most preferably higher than 3.2 dl/g, said process comprising saponifying in the usual way the polyvinyl ester obtained by low-temperature emulsion polymerization under specific conditions.
摘要翻译：本文公开了一种具有特性粘度不低于1.5dl / g，优选不小于2.2dl / g，最优选高于3.2dl / g的高聚合度的聚乙烯酯的新方法，所述方法包括使乙烯基酯单体在特定条件下进行低温乳液聚合。本文还公开了具有特性粘度不低于1.5dl / g，优选不小于2.2dl / g，最优选高于3.2dl / g的高聚合度的聚乙烯醇的新方法，所述方法包括以通常的方式皂化在特定条件下通过低温乳液聚合获得的聚乙烯酯。

4. 发明授权

US5599870A Aqueous emulsion 失效
标题翻译：水乳液
公开(公告)号：US5599870A
公开(公告)日：1997-02-04
申请号：US407670
申请日：1995-03-21
申请人： Masato Nakamae , Naoki Fujiwara , Kazutoshi Terada , Daisuke Miyake , Ken Yuki , Toshiaki Sato , Hitoshi Maruyama
发明人： Masato Nakamae , Naoki Fujiwara , Kazutoshi Terada , Daisuke Miyake , Ken Yuki , Toshiaki Sato , Hitoshi Maruyama
IPC分类号： B01F17/52 , C08F2/30 , C08L29/00 , C09J133/04 , C08L29/04
CPC分类号： C08F2/30 , C09J133/04 , C08L29/00 , Y10S516/06 , Y10S526/911 , Y10S526/912
摘要： The present invention relates to an aqueous emulsion comprising a dispersant of a modified polyvinyl alcohol with an ethylene unit content of 2 to 9 mol % and a degree of hydrolysis of at least 95 mol %, a dispersoid of a polymer of an ethylenically unsaturated monomer, and a ratio (.eta.2 rpm/.eta.20 rpm) of Brookfield viscosity at 30.degree. C., 2 rpm (.eta.2 rpm) as against Brookfield viscosity at 30.degree. C., 20 rpm (.eta.20 rpm) being 1 to 1.8 when the latter viscosity (.eta.20 rpm) is adjusted to 5,000 to 10,000 mPa.multidot.S.The aqueous emulsion according to the present invention is excellent in structural viscosity (flowability, high speed application performance), provides coated layers with high water resistance and low-temperature stability, and can be suitably used extensively as an adhesive for paper, wood and plastics, as a binder for impregnated paper and non-woven products, as an additive for mortar, as a paint, and in paper and fiber processings.
摘要翻译：本发明涉及含有乙烯单元含量为2〜9mol％，水解度为95mol％以上的改性聚乙烯醇的分散剂，烯键式不饱和单体的聚合物的分散体，并且在30℃下，Brookfield粘度在30℃，2rpm（eta 2rpm）下的Brookfield粘度与20℃下的Brookfield粘度（20rpm）的比（η2rpm /η20rpm）为1至1.8当将后一粘度（η20rpm）调节至5,000至10,000mPaxS。本发明的水性乳液的结构粘度（流动性，高速涂布性）优异，可提供耐水性和低温稳定性的涂布层，可广泛适用于纸，木材，塑料的粘合剂作为浸渍纸和无纺布产品的粘合剂，作为砂浆添加剂，作为涂料，以及纸和纤维加工。

5. 发明授权

US5308910A Composition, adhesive and aqueous emulsion 失效
标题翻译：组合物，粘合剂和水性乳液
公开(公告)号：US5308910A
公开(公告)日：1994-05-03
申请号：US903449
申请日：1992-06-24
申请人： Ken Yuki , Masato Nakamae , Hitoshi Maruyama , Tatsuaki Hattori
发明人： Ken Yuki , Masato Nakamae , Hitoshi Maruyama , Tatsuaki Hattori
IPC分类号： C08G18/62 , C08G18/63 , C09J175/00 , C08L29/04
CPC分类号： C08G18/636 , C08G18/6229 , C08G18/633 , C09J175/00 , C08G2170/80
摘要： There is disclosed a composition which comprises an aqueous emulsion selected from (A-1) aqueous emulsion comprising a dispersoid which comprises a vinyl ester polymer (1) and a copolymer a (meth)acrylic ester and a primary hydroxyl group-containing ethylenically unsaturated monomer (2), the polymer (1) being present principally in the central part of the dispersoid, the copolymer (2) having a glass transition temperature of lower than 50.degree. C. an being present principally in the peripheral part thereof; and a dispersant comprising a vinyl alcohol polymer and (A-2) aqueous emulsion comprising a dispersoid which comprises a copolymer of a hydrophobic unsaturated monomer such as (meth)acrylic ester and a primary hydroxyl group-containing ethylenically unsaturated monomer; and a dispersant comprising a vinyl alcohol polymer having a mercapto group at an end thereof and a (B) polyvalent isocyanate compound. Disclosed also are an adhesive comprising the aforementioned composition and a wooden product which is joined by the use of the adhesive. The above-disclosed adhesive is excellent in initial adhesivity, adhesive strength, water resistance and so forth.
摘要翻译：公开了一种组合物，其包含选自（A-1）水性乳液的水乳液，其包含分散质，其包含乙烯基酯聚合物（1）和共聚物（甲基）丙烯酸酯和含伯羟基的烯属不饱和单体（2）中，聚合物（1）主要存在于分散质的中心部分，共聚物（2）的玻璃化转变温度低于50℃，主要在其周边部分存在; 以及包含乙烯醇聚合物和（A-2）水性乳液的分散剂，其包含分散质，其包含疏水性不饱和单体如（甲基）丙烯酸酯和含伯羟基的烯属不饱和单体的共聚物; 和包含末端具有巯基的乙烯醇聚合物和（B）多价异氰酸酯化合物的分散剂。还公开了包含上述组合物的粘合剂和通过使用粘合剂连接的木制品。上述粘合剂的初始粘合性，粘合强度，耐水性等优异。

6. 发明申请

US20140007866A1 NEBULIZER SYSTEM AND HEATER DEVICE FOR USE IN SAID NEBULIZER SYSTEM 审中-公开
标题翻译：用于实现NEBULIZER系统的NEBULIZER系统和加热器装置
公开(公告)号：US20140007866A1
公开(公告)日：2014-01-09
申请号：US14007005
申请日：2012-01-24
申请人： Ken Yuki , Yoshihisa Haramiishi , Toshihiko Shimotoso
发明人： Ken Yuki , Yoshihisa Haramiishi , Toshihiko Shimotoso
IPC分类号： A61M11/02 , A61M16/10
CPC分类号： A61M11/02 , A61M11/06 , A61M16/1075 , A61M16/109 , A61M16/16 , A61M2205/3368 , A61M2205/3653
摘要： A nebulizer system includes a bottle that has a bottle mouth on top thereof and stores liquid therein, a heater device that is connectable to the bottle mouth, and a nebulizer adapter that is connectable to the heater device. The bottle includes a dip tube that is dipped into the liquid stored therein. An upper end portion of the dip tube is disposed inside a circumferential wall of the bottle mouth with a clearance communicating between an interior and an exterior of the bottle via the bottle mouth. The nebulizer adapter includes a nozzle member that has an orifice for injecting gas, and an aerosol-forming member in a corresponding position with the orifice, the aerosol-forming member sucking up the liquid in the bottle via the dip tube and heater device by a stream of gas injected from the orifice, and generating fine aerosol from the sucked liquid.
摘要翻译：喷雾器系统包括在其顶部具有瓶口并在其中储存液体的瓶子，可连接到瓶口的加热器装置和可连接到加热器装置的雾化器适配器。瓶子包括浸入其中储存的液体中的浸渍管。汲取管的上端部设置在瓶口的周壁内部，其间隙通过瓶口在瓶子的内部和外部之间连通。喷雾器适配器包括具有用于喷射气体的孔口的喷嘴构件和与孔口相对应的位置的气溶胶形成构件，气溶胶形成构件通过汲取管和加热器装置吸取瓶子中的液体，从孔口喷射的气体流，并从吸入的液体产生细小的气溶胶。

7. 发明申请

US20120267566A1 LITHIUM ION SECONDARY BATTERY POSITIVE ELECTRODE MATERIAL 审中-公开
标题翻译：锂离子二次电池正极电极材料
公开(公告)号：US20120267566A1
公开(公告)日：2012-10-25
申请号：US13502423
申请日：2010-10-18
申请人： Tomohiro Nagakane , Ken Yuki , Akihiko Sakamoto , Tetsuo Sakai , Meijing Zou
发明人： Tomohiro Nagakane , Ken Yuki , Akihiko Sakamoto , Tetsuo Sakai , Meijing Zou
IPC分类号： H01M4/58
CPC分类号： H01M4/5825
摘要： Provided is a positive electrode material for a lithium ion secondary battery, including a crystallized glass powder including an olivine-type crystal represented by General Formula LiMxFe1-xPO4 (0≦x
摘要翻译：本发明提供一种锂离子二次电池用正极材料，其具有由通式LiMxFe1-xPO4（0＆nlE; x <1）表示的橄榄石型结晶的结晶化玻璃粉末，M表示选自Nb，Ti， V，Cr，Mn，Co和Ni），其中结晶玻璃粉末在其表面具有非晶层。

8. 发明授权

US5403905A Process for producing polyvinyl ester having a high degree of polymerization and process for producing polyvinyl alcohol having a high degree of polymerization 失效
标题翻译：具有高聚合度的聚乙烯酯的制造方法和具有高聚合度的聚乙烯醇的制造方法
公开(公告)号：US5403905A
公开(公告)日：1995-04-04
申请号：US191185
申请日：1994-02-03
申请人： Toshiaki Sato , Ken Yuki , Junnosuke Yamauchi , Takuji Okaya
发明人： Toshiaki Sato , Ken Yuki , Junnosuke Yamauchi , Takuji Okaya
IPC分类号： C08F2/30 , C08F8/12 , C08F18/04
CPC分类号： C08F18/04 , C08F8/12
摘要： Process for producing polyvinyl ester having a high degree of polymerization and an intrinsic viscosity of from 15 dl g.sup.-1 to 3.2 dl g.sup.-1, and a polyvinyl ester obtained thereby. The process comprises subjecting a vinyl ester monomer to emulsion polymerization using nonionic emulsifiers nonionic-anionic emulsifiers, or anionic emulsifiers and a redox initiator at a temperature of -60.degree. to 15.degree. C.
摘要翻译：具有高聚合度，特性粘度为15dl-1〜3.2dlg-1的聚乙烯酯的制造方法和由此获得的聚乙烯基酯。该方法包括使用非离子乳化剂非离子 - 阴离子乳化剂或阴离子乳化剂和氧化还原引发剂在-60至15℃的温度下使乙烯基酯单体进行乳液聚合。

9. 发明授权

US5164431A Process for producing molded articles 失效
标题翻译：制造模制品的方法
公开(公告)号：US5164431A
公开(公告)日：1992-11-17
申请号：US623679
申请日：1990-12-06
申请人： Akio Mizobe , Kenji Saimen , Sotaro Itadani , Ken Yuki
发明人： Akio Mizobe , Kenji Saimen , Sotaro Itadani , Ken Yuki
IPC分类号： C04B24/26 , C04B28/02
CPC分类号： C04B28/02 , C04B24/2623 , C04B2103/44 , C04B2111/50 , Y02W30/97
摘要： Provided is a process for producing molded articles having excellent flexural strength, flexibility and dimensional stability, which comprises autoclave-curing at not lower than 100.degree. C. an aqueous composition comprising a hydraulic material (A) and a polyvinyl alcohol (B) powder, said polyvinyl alcohol (B) powder being contained in an amount of 0.1 to 20% by weight based on the weight of said hydraulic material (A).Also provided are molded articles comprising a hydraulic material (A) and a polyvinyl alcohol (B), said polyvinyl alcohol (B) being contained in an amount of 0.1 to 20% by weight based on the weight of said hydraulic material (A), said molded article having a structure comprising said polyvinyl alcohol (B) having once dissolved and then solidified being dispersed therein in the form of islands. These molded articles have excellent flexural strength, flexibility and dimensional stability.
摘要翻译：提供一种制造具有优异的弯曲强度，柔软性和尺寸稳定性的成型体的方法，其包括在不低于100℃的高压釜固化下，包含水硬性材料（A）和聚乙烯醇（B）粉末的水性组合物，所述聚乙烯醇（B）粉末的含量相对于所述液压材料（A）的重量为0.1〜20重量％。还提供了包含液压材料（A）和聚乙烯醇（B）的模塑制品，所述聚乙烯醇（B）的含量为所述水硬性材料（A）的重量的0.1-20重量％所述模制品具有包含一旦溶解并随后固化的所述聚乙烯醇（B）以岛状分散在其中的结构。这些模制品具有优异的弯曲强度，柔韧性和尺寸稳定性。

10. 发明授权

US4818788A Process for producing polyvinyl ester having a high degree of polymerization and process for producing polyvinyl alcohol having a high degree of polymerization 失效
标题翻译：具有高聚合度的聚乙烯酯的制造方法和具有高聚合度的聚乙烯醇的制造方法
公开(公告)号：US4818788A
公开(公告)日：1989-04-04
申请号：US79000
申请日：1987-07-29
申请人： Toshiaki Sato , Ken Yuki , Junnosuke Yamauchi , Takuji Okaya
发明人： Toshiaki Sato , Ken Yuki , Junnosuke Yamauchi , Takuji Okaya
IPC分类号： C08F2/24 , C08F2/22 , C08F4/40 , C08F8/12 , C08F16/02 , C08F16/06 , C08F18/00 , C08F18/04 , D01F6/14 , C08F8/00
CPC分类号： C08F18/04 , C08F8/12
摘要： Disclosed herein is a new process for producing polyvinyl ester having a high degree of polymerization having an intrinsic viscosity not less than 1.5 dl/g, preferably not less than 2.2 dl/g, and most preferably higher than 3.2 dl/g, said process comprising subjecting vinyl ester monomer to low-temperature emulsion polymerization under specific conditions.Disclosed also herein is a new process for producing polyvinyl alcohol having a high degree of polymerization having an intrinsic viscosity not less than 1.5 dl/g, preferably not less than 2.2 dl/g, and most preferably higher than 3.2 dl/g, said process comprising saponifying in the usual way the polyvinyl ester obtained by low-temperature emulsion polymerization under specific conditions.
摘要翻译：本文公开了一种具有特性粘度不低于1.5dl / g，优选不小于2.2dl / g，最优选高于3.2dl / g的高聚合度的聚乙烯酯的新方法，所述方法包括使乙烯基酯单体在特定条件下进行低温乳液聚合。本文还公开了具有特性粘度不低于1.5dl / g，优选不小于2.2dl / g，最优选高于3.2dl / g的高聚合度的聚乙烯醇的新方法，所述方法包括以通常的方式皂化在特定条件下通过低温乳液聚合获得的聚乙烯酯。

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