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1. 发明授权

US4379819A Color-photographic recording material for the silver dye bleach process 失效
标题翻译：用于银染料漂白工艺的彩色照相记录材料
公开(公告)号：US4379819A
公开(公告)日：1983-04-12
申请号：US258263
申请日：1981-04-28
申请人： John Lenoir , Gerald Jan , Mario Fryberg
发明人： John Lenoir , Gerald Jan , Mario Fryberg
IPC分类号： G03C7/02 , C09B29/00 , G03C7/28 , G03C7/29 , G03C1/10
CPC分类号： C09B29/00 , G03C7/29
摘要： A color-photographic recording material for the silver dye bleach process, which contains oil-soluble azo dyes of the formula ##STR1## in which R.sub.1 is hydrogen, alkyl, alkoxy, alkenyl, acyl, carbalkoxy, acylamino, carbamide, sulfonamide, alkylsulfone, arylsulfone, aryloxy, arylsulfonic acid ester, hydroxyl, cyano, nitro or halogen, R.sub.2 is hydrogen, alkyl, alkoxy, carbalkoxy, carbamide, sulfonamide, alkylsulfone, arylsulfone, aryloxy, cyano, nitro or halogen, R.sub.3 is hydrogen, alkyl, alkoxy, phenoxy, sulfonamide, alkylsulfone, sulfonic acid ester, cyano, nitro, halogen, carbalkoxy, carbamide or phosphoric acid diester, R.sub.4 is hydrogen, alkyl, alkoxy, carbalkoxy, carbamide, sulfonamide, acylamino, alkylsulfone, arylsulfone, hydroxyl, cyano, nitro or halogen, R.sub.5 is hydrogen, alkyl or carbalkoxy, X.sub.1 is hydrogen, alkyl, alkoxy, acylamino, alkylsulfonamide or hydroxyl, Y.sub.1 is hydrogen, alkyl, alkoxy, amino, carbalkoxy, arylsulfonamide, acylamino, halogen, hydroxyl or phosphamic acid ester, Z.sub.1 is hydrogen, alkyl, alkoxy, acylamino, acyl, carbalkoxy, alkylsulfonamide or halogen or forms a ring with Y.sub.1, and W.sub.1 is hydrogen, alkyl, alkoxy or halogen. The substituents mentioned can, where relevant, themselves be further substituted.The oil-soluble azo dyes are easily incorporated into silver halide gelatin emulsions and are very stable therein. Because of the good oil-solubility of the azo dyes, very thin layers can be cast in producing photographic materials, and this has an advantageous effect on, for example, the image sharpness.
摘要翻译：一种用于银染料漂白方法的彩色照相记录材料，其包含式（IMAGE）的油溶性偶氮染料，其中R1是氢，烷基，烷氧基，烯基，酰基，烷氧基，酰氨基，氨基酰胺，磺酰胺，烷基砜，芳基砜，芳氧基，芳基磺酸酯，羟基，氰基，硝基或卤素，R2是氢，烷基，烷氧基，烷氧基，氨基酰胺，磺酰胺，烷基砜，芳基砜，芳氧基，氰基，硝基或卤素，R3是氢，烷基，苯氧基，磺酰胺，烷基砜，磺酸酯，氰基，硝基，卤素，烷氧基，氨基甲酰基或磷酸二酯，R4是氢，烷基，烷氧基，烷氧基，氨基酰胺，磺酰胺，酰氨基，烷基砜，芳基砜，羟基，氰基，卤素，R5是氢，烷基或烷氧基，X1是氢，烷基，烷氧基，酰氨基，烷基磺酰胺或羟基，Y1是氢，烷基，烷氧基，氨基，烷氧基，芳基磺酰胺，酰氨基，卤素，羟基或磷酸酯酯，Z1是 hy 氢，烷基，烷氧基，酰氨基，酰基，烷氧基烷氧基，烷基磺酰胺或卤素，或与Y1形成环，而W1为氢，烷基，烷氧基或卤素。所提及的取代基可以在相关的情况下自身被进一步取代。油溶性偶氮染料易于掺入卤化银明胶乳剂中，并且在其中非常稳定。由于偶氮染料的良好的油溶性，可以在生产照相材料时铸造非常薄的层，并且这对于例如图像清晰度具有有利的作用。

2. 发明授权

US4254215A Process for the prevention of darkening and the formation of a sediment in photographic developer solutions 失效
标题翻译：防止变色和照相显影剂溶液中沉淀物形成的方法
公开(公告)号：US4254215A
公开(公告)日：1981-03-03
申请号：US024287
申请日：1979-03-26
申请人： Ekkehard Kramp , John Lenoir , Max Marthaler
发明人： Ekkehard Kramp , John Lenoir , Max Marthaler
IPC分类号： G03C5/305 , G03C5/30 , G03C5/38
CPC分类号： G03C5/305
摘要： A process is described for the prevention of darkening and the formation of a sediment in photographic developer solutions which contain a silver halide developer, a water-soluble silver halide solvent and organic sulfur compounds. The organic sulfur compounds are a combination of (a) an organic thiol compound or thione compound capable of tautomerism and (b) a Bunte salt which contains groups conferring solubility in water. Developer solutions which contain the indicated combination of sulfur compounds are outstandingly stable.
摘要翻译：描述了一种防止变色和在含有卤化银显影剂，水溶性卤化银溶剂和有机硫化合物的照相显影剂溶液中形成沉淀物的方法。有机硫化合物是（a）能够互变异构化的有机硫醇化合物或硫酮化合物的组合，和（b）包含赋予溶于水的基团的Bunte盐的组合。含有指示的硫化合物组合的显影剂溶液显着稳定。

3. 发明授权

US4141734A Photographic developing process 失效
标题翻译：摄影发展过程
公开(公告)号：US4141734A
公开(公告)日：1979-02-27
申请号：US856389
申请日：1977-12-01
申请人： John Lenoir , Max Marthaler
发明人： John Lenoir , Max Marthaler
IPC分类号： C07D239/46 , C07D307/54 , C07D333/24 , G03C5/305 , G03C5/38 , G03C5/50 , G03C7/00 , G03C5/30
CPC分类号： C07D239/47 , C07C323/00 , C07D307/54 , C07D333/24 , G03C5/305 , G03C5/383 , G03C5/50
摘要： A process for developing photographic silver halide material, which has been exposed image-wise is provided. The aqueous developer preparation used contains a developer compound for the silver halide, a water-soluble solvent for the silver halide and an aliphatic, cycloaliphatic, aromatic or heterocyclic di- or trisulphide. These preparations remain clear over a long period of time during which they do not lose their effectiveness by becoming turbid or by sedimentation of silver. They are of special advantage in continuously operated photographic developing processes.
摘要翻译：提供了已经成像曝光的照相卤化银材料的开发方法。所用的含水显影剂制剂含有用于卤化银的显影剂化合物，卤化银的水溶性溶剂和脂族，脂环族，芳族或杂环二 - 或三硫化物。这些制剂在长时间内保持清晰，在此期间，它们不会因浑浊或沉淀银而失去效力。它们在持续运行的照相显影工艺中具有特别的优点。

4. 发明授权

US4051123A Sulfonic-acid-group containing disazo dyestuffs 失效
标题翻译：含磺酸基的双偶氮染料
公开(公告)号：US4051123A
公开(公告)日：1977-09-27
申请号：US606395
申请日：1975-08-21
申请人： Bernhard Piller , John Lenoir , Alfred Froehlich , Thomas Stauner , Paul Tschopp
发明人： Bernhard Piller , John Lenoir , Alfred Froehlich , Thomas Stauner , Paul Tschopp
IPC分类号： C09B35/00 , C09B43/08 , C09B43/16 , C09B45/00 , G03C7/29 , C09B35/22 , C09B35/24 , C09B35/30 , C09B35/34
CPC分类号： C09B45/00 , C09B35/00 , C09B43/085 , C09B43/16 , G03C7/29
摘要： In a first main aspect azo dyestuffs of the formula ##STR1## wherein A, B, X and Y are certain substituents, in a second main aspect azo dyestuffs of the formula ##STR2## wherein B' represents certain substituents and in a third main aspect azo dyestuffs of the formulaA.sub.1 --N.dbd.N--B.sub.1 --NH--CO--X.sub.1 --Y--Z.sub.1 --OC--HN--B.sub.1 --N.dbd.N--A.sub.1wherein A.sub.1, B.sub.1, X.sub.1, Z.sub.1 and Y are certain substituents as well as the use of said azo dyestuffs in photographic material are disclosed.
摘要翻译：在第一主要方面，式IMA图的偶氮染料其中A，B，X和Y是某些取代基，在第二主要方面，式IMAMA的偶氮染料其中B'表示某些取代基，在第三个主要方面式A1-N = N-B1-NH-CO-X1-Y-Z1-OC-HN-B1-N = N-A1的偶氮染料其中A1，B1，X1，Z1和Y是某些取代基，公开了在照相材料中使用所述偶氮染料。

5. 发明授权

US4575482A Photographic silver dye bleach materials containing formyl-substituted azo compounds as image dyes 失效
标题翻译：含有甲酰基取代偶氮化合物的摄影银染料漂白剂作为影像染料
公开(公告)号：US4575482A
公开(公告)日：1986-03-11
申请号：US552220
申请日：1983-11-14
申请人： John Lenoir
发明人： John Lenoir
IPC分类号： G03C7/02 , C09B29/01 , C09B29/06 , C09B29/08 , C09B29/36 , C09B29/44 , C09B31/00 , C09B31/02 , C09B69/00 , G03C7/28 , C09B29/085 , C09B31/043 , G03C5/44
CPC分类号： C09B69/007 , C09B29/0003 , C09B29/06 , C09B29/0836 , C09B29/3643 , C09B29/3691 , C09B31/00
摘要： Photographic materials which comprise, on a base, at least one layer containing an azo dyestuff of the formula ##STR1## in which R.sub.1 is hydrogen, an alkylsulfone, halogen, cyano or nitro, R.sub.2 is hydrogen, halogen, cyano or nitro, R.sub.3 is hydrogen, alkyl, halogen, cyano or nitro, B.sub.1 is an aromatic ring system, K.sub.1 is an aromatic amine and m.sub.1 is 1 or 2.
摘要翻译：在基底上包含至少一层含有式“IMAGE”的偶氮染料的摄影材料，其中R 1是氢，烷基砜，卤素，氰基或硝基，R 2是氢，卤素，氰基或硝基，R 3是氢，烷基，卤素，氰基或硝基，B1为芳环体系，K1为芳香胺，m1为1或2。

6. 发明授权

US4202698A Quinoxalines and their use in photographic processes 失效
标题翻译：喹喔啉及其在摄影过程中的应用
公开(公告)号：US4202698A
公开(公告)日：1980-05-13
申请号：US15384
申请日：1979-02-26
申请人： Gerald Jan , Remon Hagen , John Lenoir
发明人： Gerald Jan , Remon Hagen , John Lenoir
IPC分类号： C07D241/42 , G03C7/28 , G03C7/00 , G03C1/76
CPC分类号： C07D241/42 , G03C7/28
摘要： Quinoxalines of the formula ##STR1## are provided, in which R.sub.1 and R.sub.2 independently are lower alkyl R.sub.3 is lower alkyl, --CH.sub.2 OR.sub.5, --CH.sub.2 NRR', --CH.sub.2 OCOR, --CH.sub.2 Cl, --CH.sub.2 Br, --CH.sub.2 SR, --CH.sub.2 O(CH.sub.2).sub.p OR, --CH.sub.2 PO(OR.sub.5).sub.2, --CH.sub.2 PO(OR.sub.6).sub.2, --CH.sub.2 SO.sub.3 R.sub.6, --O(CH.sub.2).sub.m OR, --O(CH.sub.2).sub.p SO.sub.3 R.sub.6 or --(OCH.sub.2 CH.sub.2).sub.n OAr, R.sub.4 is hydrogen, lower alkyl or alkoxy when R.sub.3 is other than lower alkyl, or R.sub.4 is --OH, --NRR', --NHCOR, --NHCOAr', --NHSO.sub.2 R.sub.5 or --NHSO.sub.2 Ar', R and R' independently are hydrogen or lower alkyl, R.sub.5 is lower alkyl, R.sub.6 is hydrogen, an alkali metal cation or --N.sup..sym. (R).sub.4, Ar is aryl or sulphonated aryl, Ar' is aryl or substituted aryl, m is 3 or 4, n is 1 to 3 and p is 2 to 4.The quinoxalines are useful as bleach catalysts, especially as dye bleach catalysts, for the photographic silver dye bleach process.
摘要翻译：提供式“IMAGE”的喹喔啉，其中R1和R2独立地是低级烷基，R3是低级烷基，-CH2OR5，-CH2NRR'，-CH2OCOR，-CH2Cl，-CH2Br，-CH2SR，-CH2O（CH2）pOR， -CH 2 PO（OR 5）2，-CH 2 PO（OR 6）2，-CH 2 SO 3 R 6，-O（CH 2）m OR，-O（CH 2）p SO 3 R 6或 - （OCH 2 CH 2）nOAr，R 4是氢，低级烷基或烷氧基，低级烷基或R4是-OH，-NRR'，-NHCOR，-NHCOAr'，-NHSO2R5或-NHSO2Ar'，R和R'独立地是氢或低级烷基，R5是低级烷基，R6是氢，碱金属阳离子或-N（+）（R）4，Ar为芳基或磺化芳基，Ar'为芳基或取代芳基，m为3或4，n为1至3，p为2至4.喹喔啉可用作漂白催化剂，特别是作为染料漂白催化剂，用于照相银染料漂白工艺。

7. 发明授权

US4118232A Photographic material containing sulphonic acid group containing disazo dyestuffs 失效
标题翻译：含有磺酸基的双偶氮染料的摄影材料
公开(公告)号：US4118232A
公开(公告)日：1978-10-03
申请号：US777867
申请日：1977-03-15
申请人： Bernhard Piller , John Lenoir , Alfred Froehlich , Thomas Stauner , Paul Tschopp
发明人： Bernhard Piller , John Lenoir , Alfred Froehlich , Thomas Stauner , Paul Tschopp
IPC分类号： C09B35/00 , C09B43/08 , C09B43/12 , C09B43/16 , C09B45/00 , G03C7/29 , G03G17/02 , G03C1/10
CPC分类号： C09B43/12 , C09B35/00 , C09B43/085 , C09B43/16 , C09B45/00 , G03C7/29 , G03G17/02
摘要： The invention is directed essentially to photographic material containing, on a carrier, a layer with azo dyestuffs of the formula ##STR1## wherein A, B, X and Y are certain substituents, in a second main aspect azo dyestuffs of the formula ##STR2## wherein B' represents certain substituents and in a third main aspect azo deystuffs of the formulaA.sub.1 --N.dbd.N--B.sub.1 --NH--CO--X.sub.1 --Y--Z.sub.1 --OC--HN--B.sub.1 --N.dbd.N--A.sub.1wherein A.sub.1, B.sub.1, X.sub.1, Z.sub.1 and Y are certain substituents.The photographic materials provide advantages stemming from the use of the dyestuffs of the invention which are distinguished by particularly high fastness to light coupled with excellent bleachability, good resistance to diffusion and advantageous color strength.
摘要翻译：本发明主要涉及在载体上含有具有下式的偶氮染料的层的照相材料：其中A，B，X和Y是某些取代基，在第二主要方面，式IMAMA的偶氮染料其中B'表示某些取代基，在第三主要方面，式A1-N = N-B1-NH-CO-X1-Y-Z1-OC-HN-B1-N = N-A1的偶氮胶囊其中A1，B1 X1，Z1和Y是某些取代基。

8. 发明授权

US4521591A Oil-soluble disazo dyes and their use in color-photographic recording materials for the silver dye bleach process 失效
标题翻译：油溶性双偶氮染料及其在彩色摄影记录材料中用于银染料漂白工艺
公开(公告)号：US4521591A
公开(公告)日：1985-06-04
申请号：US346785
申请日：1982-02-08
申请人： Gerald Jan , John Lenoir
发明人： Gerald Jan , John Lenoir
IPC分类号： G03C7/02 , C09B35/02 , G03C7/28 , G03C7/29 , C09B35/10 , C09B35/215 , C09B35/233 , C09B35/28
CPC分类号： C09B35/02 , G03C7/29
摘要： Compounds of the formula ##STR1## in which X.sub.1 is hydrogen, alkyl, alkoxy, --NL.sub.1 COM.sub.1, in which L.sub.1 is hydrogen or alkyl and M.sub.1 is alkyl or alkoxy, or is --NL.sub.1 P(O)(OG.sub.1).sub.2, in which G.sub.1 is alkyl, or is alkylsulfonamide or hydroxyl, Y.sub.1 is hydrogen, alkyl, alkoxy, carbalkoxy, N-alkyl-substituted or N,N-dialkyl-substituted amino or --NL.sub.2 COM.sub.2, in which L.sub.2 is hydrogen or alkyl and M.sub.2 is alkyl or alkoxy, Z.sub.1 is hydrogen, alkyl, alkoxy, --NL.sub.2 COM.sub.3, in which M.sub.3 is alkyl, or is carbalkoxy or halogen or represents those atoms which are required to form a ring with Y.sub.1, W.sub.1 is hydrogen, alkyl or alkoxy, R.sub.1 and R.sub.2 independently of one another are hydrogen, halogen, cyano, nitro or --SO.sub.2 U.sub.3, in which U.sub.3 is alkyl or phenyl, R.sub.3 is hydrogen or alkyl or, if R.sub.4 is a direct chemical bond, the two radicals R.sub.3 together are a link member and R.sub.4 is a direct chemical bond or a link member, and at least two of the substituents W.sub.1, X.sub.1, Y.sub.1 and Z.sub.1 are other than hydrogen. The compounds can be used with particular advantage as image dyes, for example in photographic materials for the silver dye bleach process. Color images with excellent color reproduction are obtained.
摘要翻译：其中X1是氢，烷基，烷氧基，-NL1COM1，其中L1是氢或烷基，M1是烷基或烷氧基，或是-NL1P（O）（OG1）2，其中G1是烷基或烷基磺酰胺或羟基，Y1是氢，烷基，烷氧基，烷氧基，N-烷基取代或N，N-二烷基取代的氨基或-NL2COM2，其中L2是氢或烷基，M2是烷基或烷氧基， Z1是氢，烷基，烷氧基，-NL2COM3，其中M3是烷基，或是烷氧基或卤素，或代表与Y1形成环所需的那些原子，W1是氢，烷基或烷氧基，R1和R2独立于一个另一个是氢，卤素，氰基，硝基或-SO 2 U 3，其中U 3是烷基或苯基，R 3是氢或烷基，或者如果R 4是直接化学键，则两个基团R 3一起是连接基团，并且R 4是直接的化学键或连接构件，并且至少两个取代基W1，X1，Y1和Z1不是氢。这些化合物可以特别有利地用作图像染料，例如用于银染料漂白方法的照相材料。获得具有优异色彩再现的彩色图像。

9. 发明授权

US4409143A Monoazo dyes containing phosphamic acid diester groups 失效
标题翻译：含有氨基酸二酯基团的单偶氮染料
公开(公告)号：US4409143A
公开(公告)日：1983-10-11
申请号：US258245
申请日：1981-04-28
申请人： John Lenoir , Gerald Jan
发明人： John Lenoir , Gerald Jan
IPC分类号： G03C7/02 , C09B29/08 , C09B29/085 , C09B29/36 , C09B29/44 , C09B31/043 , G03C7/28 , G03C7/29 , C09B29/09 , C09B29/26 , G03C1/10
CPC分类号： C09B29/0836 , C09B29/3643 , C09B29/3686 , C09B31/043 , G03C7/29 , Y10S534/02
摘要： Azo dyes of the formula in which X.sub.1 and X.sub.2 independently of one another are alkyl, cycloalkyl, alkenyl, aryl or aralkyl, Y.sub.1 is hydrogen or alkyl, Y.sub.2 is hydrogen, alkyl, alkenyl or aryl or together with Y.sub.1 stands for the atoms required to complete a ring, Z.sub.1 is hydrogen, alkyl, alkenyl, alkoxy, aryl, aryloxy, alkylmercapto, arylmercapto, halogen, cyano, carbalkoxy or stands for the atoms which together with Y.sub.1 form a ring, and D.sub.1 is the radical of a heterocyclic azo component such as a thienyl, thiazolyl, benzthiazolyl, pyrazolyl or imidazolyl radical, or is phenyl optionally substituted by alkyl, cycloalkyl, alkoxy, alkenyl, electronegative substituents such as halogen, cyano, nitro or carboxylic acid, alkyl- or phenylsulfone or N-alkyl or N,N-dialkyl-substituted sulfonamido, can be used as image dyes in photographic silver dye-bleach materials, or for dyeing textile materials.
摘要翻译：其中X1和X2彼此独立地是烷基，环烷基，烯基，芳基或芳烷基，Y1是氢或烷基，Y2是氢，烷基，烯基或芳基或与Y1一起代表所需的原子完成一个环，Z1是氢，烷基，烯基，烷氧基，芳基，芳氧基，烷基巯基，芳基巯基，卤素，氰基，烷氧基或代表与Y1一起形成环的原子，D1是杂环偶氮组分例如噻吩基，噻唑基，苯并噻唑基，吡唑基或咪唑基，或者是任选被烷基，环烷基，烷氧基，烯基，电负性取代基如卤素，氰基，硝基或羧酸取代的苯基，烷基或苯基砜或N-烷基或 N，N-二烷基取代的亚磺酰氨基可用作照相银染料漂白材料中的图像染料，或染色纺织材料。

10. 发明授权

US3957860A Process for the manufacture of nuclear-sulphonated compounds 失效
标题翻译：制备核化合物的方法
公开(公告)号：US3957860A
公开(公告)日：1976-05-18
申请号：US480082
申请日：1974-06-17
申请人： John Lenoir
发明人： John Lenoir
IPC分类号： C09B1/24 , C07C143/56 , C07C143/64 , C07C149/40
CPC分类号： C09B1/24
摘要： This invention relates to a process for the manufacture sulphonated compounds. Aromatically unsaturated amines are reacted with sulphamic acid or its derivatives at temperatures between 20.degree. and 250.degree.C in the presence of an aprotic solvent and a catalyst.

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