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1. 发明授权

US4517141A Production of microcapsules having walls of polyaddition products of water-insoluble polyamines with water-soluble polyisocyanate adducts 失效
标题翻译：生产具有水不溶性聚胺与水溶性多异氰酸酯加合物的加聚产物壁的微胶囊
公开(公告)号：US4517141A
公开(公告)日：1985-05-14
申请号：US506451
申请日：1983-06-21
申请人： Manfred Dahm , Norbert Weimann , Ulrich Nehen , Hanns P. Muller , Gert Jabs , Albert Awater , James M. Barnes
发明人： Manfred Dahm , Norbert Weimann , Ulrich Nehen , Hanns P. Muller , Gert Jabs , Albert Awater , James M. Barnes
IPC分类号： B01J13/16 , B41M5/165 , C08G18/32 , C08G18/80 , B01J13/02
CPC分类号： C08G18/8083 , B01J13/16 , B41M5/165 , C08G18/3253 , Y10S428/914 , Y10S430/104 , Y10T428/2985 , Y10T428/2989
摘要： Microcapsules having a hydrophobic core material and capsule walls formed by the reaction of water-insoluble polyamines with water-soluble bisulphite adducts of polyisocyanates, a process for the production thereof which is characterized in that a mixture of a hydrophobic core material and water-insoluble polyamines is emulsified in water or in an aqueous protective colloid solution to the required particle size, water-soluble bisulphite adducts of polyisocyanates in the form of powders or aqueous solutions are added and the mixture is left to react to completion at temperatures of from 1.degree. to 140.degree. C., and applications thereof.
摘要翻译：具有疏水性芯材的微胶囊和通过水不溶性多胺与多异氰酸酯的水溶性亚硫酸氢盐加合物的反应形成的胶囊壁，其制造方法，其特征在于，疏水性芯材料与水不溶性多胺在水中或在水性保护胶体溶液中乳化至所需的粒度，加入粉末或水溶液形式的多异氰酸酯的水溶性亚硫酸氢盐加合物，使混合物在1℃至 140℃，及其应用。

2. 发明授权

US4383051A Process for the preparation of polyurethane plastics using dianhydro-hexite diols 失效
标题翻译：使用二氢 - 己二醇二醇制备聚氨酯塑料的方法
公开(公告)号：US4383051A
公开(公告)日：1983-05-10
申请号：US357118
申请日：1982-03-11
申请人： Holger Meyborg , Kuno Wagner , James M. Barnes , Herbert Salzburg
发明人： Holger Meyborg , Kuno Wagner , James M. Barnes , Herbert Salzburg
IPC分类号： C08L65/00 , C08G18/00 , C08G18/10 , C08G18/32 , C08G18/65 , C08L7/00 , C08L21/00 , C08L67/00 , C08L77/00 , C08G18/14
CPC分类号： C08G18/6511 , C08G18/10 , C08G18/3218
摘要： A process for the preparation of homogeneous and cellular polyurethane plastics by the reaction of(a) organic polyisocyanates;(b) compounds containing at least 2 Zerewitinoff-active hydrogen atoms and having molecular weights of from 400 to 10,000;(c) chain extenders, and, optionally, additional(d) short-chained compounds containing at least 2 Zerewitinoff-active hydrogen atoms and having a molar mass of from 32 to 400, as well as, optionally,(e) catalysts, blowing agents and other known additives,is described, which is characterized in that 1,4-3,6-dianhydro-hexites, preferably 1,4-3,6-dianhydro-D-sorbitol and/or 1,4-3,6-dianhydro-D-mannitol, optionally mixed with lower molecular weight compounds, preferably with polyols having a molecular weight of from 62 to 400, particularly preferably butane diol-1,4 are used as the chain extenders. The new chain extenders produce high quality elastomers and foams.
摘要翻译：通过（a）有机多异氰酸酯的反应制备均匀和细胞聚氨酯塑料的方法; （b）含有至少2个Zerewitinoff-活性氢原子并且分子量为400至10,000的化合物; （c）扩链剂，以及任选地，含有至少2个Zerewitinoff-活性氢原子并且具有32-400摩尔质量的另外的（d）短链化合物，以及任选的（e）催化剂，吹制其特征在于1,4-3,6-二脱水 - 己酸，优选1,4-3,6-二脱氢-D-山梨糖醇和/或1,4-3,6 - 二水-D-甘露糖醇，任选地与较低分子量的化合物混合，优选使用分子量为62至400的多元醇，特别优选丁二醇-1,4作为扩链剂。新的增链剂生产高品质的弹性体和泡沫。

3. 发明授权

US5159046A Process for the preparation of highly elastic plastics 失效
标题翻译：制备高弹性塑料的方法
公开(公告)号：US5159046A
公开(公告)日：1992-10-27
申请号：US543649
申请日：1990-06-26
申请人： Gerhard Grogler , Andreas Ruckes , Richard Kopp , Heinrich Hess , Robert Eiben , James M. Barnes
发明人： Gerhard Grogler , Andreas Ruckes , Richard Kopp , Heinrich Hess , Robert Eiben , James M. Barnes
IPC分类号： C07C275/62 , C07C273/18 , C08G18/70 , C08G18/78 , C08G18/80
CPC分类号： C07C273/1809 , C07C273/1872 , C08G18/703 , C08G18/707 , C08G18/7818 , C08G18/8045
摘要： The present invention relates to a process for the preparation of a modified 1,5-naphthylene diisocyanate containing urea and biuret groups comprising reacting(a) 1,5-naphthylene diisocyanate in molten form with(b) a mixture comprising about 0.02 to about 0.5 mole of water per mole of 1,5-naphthylene diisocyanate and about 1 to about 10 parts for each part of water of an organic solvent.The present invention further relates to a process for the preparation of elastomeric moldings comprising reacting by the one-shot or prepolymer process at an isocyanate index of 70 to 130 a modified 1,5-naphthylene diisocyanate containing urea and biuret groups with compounds containing at least two isocyanate-reactive groups and having a molecular weight in the range from about 500 to about 10,000 and, optionally, organic compounds containing isocyanate-reactive groups and having a molecular weight in the range from 60 to 499.
摘要翻译：本发明涉及一种制备含脲和缩二脲基团的改性的1,5-亚萘基二异氰酸酯的方法，包括使（a）熔融形式的1,5-亚萘基二异氰酸酯与（b）约0.02至约0.5的混合物摩尔水/摩尔1,5-亚萘基二异氰酸酯和约1至约10份的每份有机溶剂的水。本发明还涉及一种制备弹性体模制品的方法，其包括通过一步或预聚物方法在异氰酸酯指数为70至130的情况下使含有脲和缩二脲基团的改性的1,5-亚萘基二异氰酸酯与至少含有化合物两个异氰酸酯反应性基团，分子量在约500至约10,000的范围内，以及任选的含有异氰酸酯反应性基团并且分子量在60至499范围内的有机化合物。

4. 再颁专利

USRE33748E Process for the preparation of polyurethane plastics using dianhydro-hexite diols 失效
公开(公告)号：USRE33748E
公开(公告)日：1991-11-19
申请号：US733284
申请日：1985-05-10
申请人： Holger Meyborg , Kuno Wagner , James M. Barnes , Herbert Salzburg
发明人： Holger Meyborg , Kuno Wagner , James M. Barnes , Herbert Salzburg
IPC分类号： C08L65/00 , C08G18/00 , C08G18/10 , C08G18/32 , C08G18/65 , C08L7/00 , C08L21/00 , C08L67/00 , C08L77/00
CPC分类号： C08G18/6511 , C08G18/10 , C08G18/3218
摘要： A process for the preparation of homogeneous and cellular polyurethane plastics by the reaction of(a) organic polyisocyanates;(b) compounds containing at least 2 Zerewitinoff-active hydrogen atoms and having molecular weights of from 400 to 10,000;(c) chain extenders, and, optionally, additional(d) short-chained compounds containing at least 2 Zerewitinoff-active hydrogen atoms and having a molar mass of from 32 to 400, as well as, optionally,(e) catalysts, blowing agents and other known additives,is described, which is characterized in that 1,4-3,6-dianhydro-hexites, preferably 1,4-3,6-dianhydro-D-sorbitol and/or 1,4-3,6-dianhydro-D-mannitol, optionally mixed with lower molecular weight compounds, preferably with polyols having a molecular weight of from 62 to 400, particularly preferably butane diol-1,4 are used as the chain extenders. The new chain extenders produce high quality elastomers and foams.

5. 发明授权

US4639478A Bismorpholines, a process for their preparation and their use for protection against hydrolysis 失效
标题翻译：双蝎子，它们的制备方法及其用于防止水解的用途
公开(公告)号：US4639478A
公开(公告)日：1987-01-27
申请号：US857014
申请日：1986-04-29
申请人： Peter Haas , James M. Barnes , Wilhelm Goyert
发明人： Peter Haas , James M. Barnes , Wilhelm Goyert
IPC分类号： C07D498/04 , C08K5/35 , C08K5/15
CPC分类号： C07D498/04 , C08K5/35
摘要： The present invention relates to 2,3,2',3'-bis-morpholine derivatives corresponding to the formula ##STR1## The present invention also relates to a process for the preparation of these derivatives and to their use as hydrolysis protective agents for synthetic polymers containing ester groups and/or carbonate groups. Preferred synthetic polymers are polyurethanes.
摘要翻译：本发明涉及对应于式的2,3,2'，3'-双 - 吗啉衍生物本发明还涉及制备这些衍生物的方法及其作为合成的水解保护剂的用途含有酯基和/或碳酸酯基团的聚合物。优选的合成聚合物是聚氨酯。

6. 发明授权

US4605729A Process for the production of polyetherester polyols and the products and use thereof 失效
标题翻译：生产聚醚醚多元醇及其产品及其用途的方法
公开(公告)号：US4605729A
公开(公告)日：1986-08-12
申请号：US784071
申请日：1985-10-04
申请人： James M. Barnes , Werner Betz
发明人： James M. Barnes , Werner Betz
IPC分类号： C08G18/42 , C08G18/48 , C08G63/668 , C08G63/66
CPC分类号： C08G18/4252 , C08G18/4244 , C08G18/4887 , C08G63/668
摘要： The invention provides a process for the production of polyetherester polyols which have hydroxyester groups terminally bound via ester groups to high molecular weight polyether polyol segments. These are produced by first reacting high molecular weight polyoxyalkylene ether polyols with molecular weights of from about 400 to 10,000 with an excess of dicarboxylic acids, dicarboxylic acid anhydrides or dicarboxylic acid esters, and then reacting the intermediate product in a further stage with an excess of diols, based on carboxyl groups.The new, high molecular weight polyetherester polyols thus consist of polyoxyalkylene ether segments, which have terminal ester segments in each case with terminal hydroxyl groups per end group.Moreover, the use is claimed of the high molecular weight polyetherester polyols as polyhydroxyl compounds for forming polyurethanes.
摘要翻译：本发明提供了一种生产聚酯多元醇的方法，所述聚醚酯多元醇具有通过酯基终止结合到高分子量聚醚多元醇链段上的羟基酯基团。这些是通过首先使分子量为约400至10,000的高分子量聚氧化烯醚多元醇与过量的二羧酸，二羧酸酐或二羧酸酯反应制备的，然后使中间产物在另一阶段与过量的二醇，基于羧基。因此，新的高分子量聚醚酯多元醇由聚氧化烯醚链段组成，每个端基具有末端羟基的末端酯链段。此外，要求使用高分子量聚醚酯多元醇作为形成聚氨酯的多羟基化合物。

7. 发明授权

US4476253A Process for the preparation of polyurethane elastomers using diols of the anhydro-tetritol series 失效
标题翻译：使用脱水四氢呋喃系列的二醇制备聚氨酯弹性体的方法
公开(公告)号：US4476253A
公开(公告)日：1984-10-09
申请号：US570045
申请日：1984-01-11
申请人： Herbert Salzburg , Holger Meyborg , Wilhelm Goyert , James M. Barnes
发明人： Herbert Salzburg , Holger Meyborg , Wilhelm Goyert , James M. Barnes
IPC分类号： C08G18/10 , C08G18/32 , C08G18/14
CPC分类号： C08G18/3218 , C08G18/10
摘要： Polyurethane elastomers are made by reacting organic polyisocyanates with compounds having at least two groups containing isocyanate-reactive hydrogen atoms and a molecular weight of from 400 to 10,000 and a 1,4-monoanhydro-tetritol in accordance with techniques known to those in the art. Known chain-lengthening agents, auxiliaries and additives may be included in the reaction mixture. The reaction mixtures employed in the process of the present invention have a longer pot life than prior art reaction mixtures. The elastomers produced by this process are shrink stable.
摘要翻译：根据本领域已知的技术，聚氨酯弹性体是通过有机多异氰酸酯与具有至少两个含异氰酸酯反应性氢原子和分子量为400至10,000的化合物和1,4-单羟基 - 氢化四醇反应制备的。已知的增链剂，助剂和添加剂可以包括在反应混合物中。在本发明方法中使用的反应混合物具有比现有技术的反应混合物更长的适用期。由该方法生产的弹性体收缩稳定。

8. 发明授权

US4808691A Polyether-polycarbonate diols and processes for their production and use 失效
标题翻译：聚醚 - 聚碳酸酯二醇及其生产和使用的方法
公开(公告)号：US4808691A
公开(公告)日：1989-02-28
申请号：US193303
申请日：1988-05-11
申请人： Klaus Konig , James M. Barnes
发明人： Klaus Konig , James M. Barnes
IPC分类号： C08G18/42 , C08G18/44 , C08G64/00 , C08G64/18 , C08G64/20 , C08G18/32
CPC分类号： C08G18/44 , C08G64/183 , C08G2101/0033
摘要： Polyether polycarbonate diols based on 1,6-hexanediol and having a molecular weight of from 500 to 12,000 are made by etherifying 50-100 mole % 1,6-hexane-diol in the presence of 0-50 mole % of specified diols and reacting the resultant polyether with a compound selected from diarylcarbonates, dialkyl carbonates, dioxolanones, hexanediol bischlorocarbonic acid esters, phosgene and urea. These diols are particularly useful in the production of polyurethanes having improved physical properties.
摘要翻译：基于1,6-己二醇并具有500至12,000分子量的聚醚聚碳酸酯二醇通过在0-50摩尔％的特定二醇的存在下醚化50-100摩尔％的1,6-己二醇来制备，并使得到的聚醚与选自碳酸二芳基酯，碳酸二烷基酯，二氧戊环酮，己二醇双氯碳酸酯，光气和尿素的化合物组成。这些二醇在具有改进的物理性能的聚氨酯的生产中特别有用。

9. 发明授权

US4755334A Process for the continuous production of articles or coatings with contours of complicated shape 失效
标题翻译：用于连续生产具有复杂形状轮廓的制品或涂层的方法
公开(公告)号：US4755334A
公开(公告)日：1988-07-05
申请号：US741513
申请日：1985-06-05
申请人： Wolfgang Grimm , James M. Barnes
发明人： Wolfgang Grimm , James M. Barnes
IPC分类号： B29C39/16 , B29C39/14 , B29C39/20 , B29C39/24 , B29C39/26 , B29D30/54 , B29K75/00 , B29L9/00 , B29L29/00 , B29L30/00 , B29C41/30 , B29C41/52
CPC分类号： B29C39/20 , B29C39/14 , B29C39/148 , B29C39/24 , B29D30/54 , B29K2105/0002 , B29K2105/101 , B29L2031/324 , B29L2031/7092 , Y10S264/74
摘要： The present invention is directed to a process for the continuous production of articles or coatings with contours wherein a liquid material is introduced at one end into the mold cavity formed between at least two travelling continous shaping faces, said material being cured in the mold cavity and subsequently removed from the mold, characterized in that (i) the travelling faces are moved downwards at least in the region of the material feed, (ii) the stream of material supplied is moved to and fro transversely to the direction of advance of the faces, and (iii) the quantity of material supplied is controlled so as to fill the mold cavity with a uniform coating and an apparatus for use therein.
摘要翻译：本发明涉及用于连续生产具有轮廓的制品或涂层的方法，其中液体材料在一端被引入形成在至少两个行进的连续成形面之间的模腔中，所述材料在模腔中固化，随后从模具中取出，其特征在于，（i）行进面至少在材料供给的区域中向下移动，（ii）供应的材料流横向于面的前进方向，和（iii）所供应的材料的数量被控制以便以均匀的涂层和用于其中的装置填充模腔。

10. 发明授权

US4619985A Process for the production of deactivated suspensions of finely-divided polyisocyanates in relatively high molecular weight compounds, deactivated suspensions and use thereof for the production of polyurethanes 失效
标题翻译：在相对高分子量化合物中制备细分多异氰酸酯的失活悬浮液的方法，失活的悬浮液及其用于生产聚氨酯的用途
公开(公告)号：US4619985A
公开(公告)日：1986-10-28
申请号：US732028
申请日：1985-05-08
申请人： Heinrich Hess , Gerhard Grogler , Richard Kopp , James M. Barnes
发明人： Heinrich Hess , Gerhard Grogler , Richard Kopp , James M. Barnes
IPC分类号： C08G18/00 , C08G18/08 , C08G18/30 , C08G18/32 , C08G18/70 , C08G18/72 , C08G18/80 , C09D175/00
CPC分类号： C08G18/707 , C08G18/089 , C08G18/8003 , Y10S528/902
摘要： The present invention is directed to a process for the production of suspensions of finely-divided polyisocyanates which are obtainable by the surface reaction with from 0.1 to 25 equivalent percent of reactive group per NCO of stabilizers in relatively high molecular weight polyols and/or relatively high molecular weight polyamines having molecular weights from 400 to 6,000 optionally with addition of lower molecular weight polyols and/or aromatic amines having molecular weights of from 60 to 399, which are characterized in that unreacted quantities of stabilizers in the suspension are subsequently partially or completely deactivated by addition of substances having an acylating and/or neutralizing and/or alkylating effect and/or adsorbing effect as "deactivators". In particular, mono- and/or polyisocyanates are used as "deactivators". Deactivated suspensions obtainable in this way do not exhibit rising thickening temperatures during the production of polyurethanes, in particular in large-volume shaped articles.The present invention also relates to deactivated suspensions obtainable by the present process and to the use thereof for polyurethane production.
摘要翻译：本发明涉及一种生产细分多异氰酸酯的悬浮液的方法，其可通过表面反应获得，每个NCO为相对高分子量多元醇中的稳定剂为0.1至25当量％的反应性基团和/或相对高的分子量为400至6000的分子量多胺，任选地加入分子量为60至399的较低分子量多元醇和/或芳族胺，其特征在于悬浮液中未反应量的稳定剂随后部分或完全失活通过加入具有酰化和/或中和和/或烷化作用和/或吸附作用的物质作为“失活剂”。特别地，单 - 和/或多异氰酸酯用作“钝化剂”。以这种方式获得的失活悬浮液在聚氨酯生产过程中，尤其是在大体积成型的制品中不会出现增加的增厚温度。本发明还涉及通过本方法获得的失活悬浮体及其用于聚氨酯生产的用途。

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