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1. 发明授权

US08697921B2 Process for purifying wastewaters from the workup of crude aromatic nitro compounds 有权
标题翻译：从芳香族硝基化合物的后处理中净化废水的方法
公开(公告)号：US08697921B2
公开(公告)日：2014-04-15
申请号：US13569806
申请日：2012-08-08
申请人： Petra Deckert , Leo Denissen , Bart Van De Voorde , Julia Leschinski , Stefan Robert Deibel , Matthias Fankhaenel , Samuel Neto
发明人： Petra Deckert , Leo Denissen , Bart Van De Voorde , Julia Leschinski , Stefan Robert Deibel , Matthias Fankhaenel , Samuel Neto
IPC分类号： C07B41/00
CPC分类号： C07C201/16 , C07C205/06
摘要： The invention relates to a process for purifying crude aromatic nitro compounds which originate from the nitration of aromatic compounds, comprising the single or multiple performance of the following wash stage (a): (a) contacting the crude aromatic nitro compound (N-in) with an aqueous phase (W-res) and then separating the phases to obtain an organic phase (N-res) and an aqueous phase (W-res), wherein at least one demulsifier (D) is present in one or more of the wash stages (a).
摘要翻译：本发明涉及一种用于纯化源自芳族化合物硝化的粗芳族硝基化合物的方法，其包括以下洗涤阶段（a）的单次或多次性能：（a）使粗芳族硝基化合物（N-in）（W-res），然后分离相以获得有机相（N-res）和水相（W-res），其中至少一个破乳剂（D）存在于一个或多个洗涤阶段（a）。

2. 发明申请

US20110275858A1 METHOD FOR PRODUCING TOLUYLENEDIAMINE BY HYDROGENATING DINITROTOLUENE 失效
标题翻译：通过加氢精氨酸生产戊烯二胺的方法
公开(公告)号：US20110275858A1
公开(公告)日：2011-11-10
申请号：US13142718
申请日：2009-12-21
申请人： Joana Coelho Tsou , Steffen Oehlenschlaeger , Ekkehard Schwab , Wolfgang Mackenroth , Hartwig Voss , Stefan Maixner , Samuel Neto , Sven Boehmeke , Frederik van Laar
发明人： Joana Coelho Tsou , Steffen Oehlenschlaeger , Ekkehard Schwab , Wolfgang Mackenroth , Hartwig Voss , Stefan Maixner , Samuel Neto , Sven Boehmeke , Frederik van Laar
IPC分类号： C07C209/36
CPC分类号： C07C209/36 , C07C211/50
摘要： A process for preparing tolylenediamine by hydrogenating dinitrotoluene with hydrogen in the presence of a suspended catalyst in a vertically upright reactor (1), at the upper end of which is arranged a motive jet nozzle (2) through which the reaction mixture drawn off from the reactor bottom, via an external loop, is sprayed into the upper region of the reactor (1) and then flows into a central inserted tube (4) which is arranged in the longitudinal direction of the reactor, flows through the latter from the top downward and flows upward again outside the inserted tube (4) in an internal loop motion, with a heat exchanger (6) in the interior of the reactor (1), through which cooling water flows, and absorbs some of the heat of reaction as it does so, with a feed for the dinitrotoluene at the upper end of the reactor (1) and a feed for the hydrogen at the lower end of the reactor (1), and wherein, in addition to the heat exchanger (6) arranged in the interior of the reactor (1), a further heat exchanger (W) is used in the external loop, in which water absorbs the rest of the heat of reaction by indirect heat exchange with the reaction mixture, which comprises utilizing the heat of reaction to raise steam with a pressure of at least 4 bar gauge by performing the hydrogenation of dinitrotoluene to tolylenediamine at a temperature of ≧180° C.
摘要翻译：一种通过在悬浮催化剂存在下用氢气将二硝基甲苯氢化在垂直直立反应器（1）中制备甲苯二胺的方法，其上端设置有动力喷嘴（2），反应混合物从其中排出反应器底部通过外部环路喷射到反应器（1）的上部区域中，然后流入沿着反应器的纵向布置的中心插入管（4），其从顶部向下流动并且在反应器（1）的内部具有热交换器（6），内部循环运动再次向外流过插入的管（4），冷却水通过该换热器（6）流过，并吸收一些反应热用反应器（1）上端的二硝基甲苯进料和反应器（1）下端的氢气进料，并且其中除了设置在反应器（1）的下端的热交换器反应器（1）的内部，一个furt 她的热交换器（W）用于外部回路中，其中水通过与反应混合物的间接热交换吸收剩余的反应热，其中包括利用反应热量以至少4的压力升高蒸汽通过在≥180℃的温度下进行二硝基甲苯氢化成甲苯二胺来测定。

3. 发明授权

US07985705B2 Three-layered, four-layered, or five-layered catalyst systems for producing phthalic anhydride 有权
标题翻译：用于生产邻苯二甲酸酐的三层，四层或五层催化剂体系
公开(公告)号：US07985705B2
公开(公告)日：2011-07-26
申请号：US12708181
申请日：2010-02-18
申请人： Sebastian Storck , Jürgen Zühlke , Samuel Neto , Frank Rosowski
发明人： Sebastian Storck , Jürgen Zühlke , Samuel Neto , Frank Rosowski
IPC分类号： B01J31/36 , C07D307/89
CPC分类号： C07C51/313 , B01J23/002 , B01J23/22 , B01J27/198 , B01J35/0006 , B01J35/10 , B01J35/1009 , B01J35/1014 , B01J2523/00 , C07C51/265 , C07C63/16 , B01J2523/15 , B01J2523/47 , B01J2523/53 , B01J2523/55 , B01J2523/51
摘要： Catalyst systems for preparing phthalic anhydride by means of gas-phase oxidation of o-xylene and/or naphthalene, and a process for preparing phthalic anhydride using the catalyst systems.
摘要翻译：通过邻二甲苯和/或萘的气相氧化制备邻苯二甲酸酐的催化剂体系，以及使用催化剂体系制备邻苯二甲酸酐的方法。

4. 发明申请

US20100210857A1 Three-Layered or Four-Layered Catalyst Systems for Producing Phthalic Anhydride 有权
标题翻译：用于生产邻苯二甲酸酐的三层或四层催化剂体系
公开(公告)号：US20100210857A1
公开(公告)日：2010-08-19
申请号：US12708181
申请日：2010-02-18
申请人： Sebastian Storck , Jürgen Zühlke , Samuel Neto , Frank Rosowski
发明人： Sebastian Storck , Jürgen Zühlke , Samuel Neto , Frank Rosowski
IPC分类号： C07D307/89
CPC分类号： C07C51/313 , B01J23/002 , B01J23/22 , B01J27/198 , B01J35/0006 , B01J35/10 , B01J35/1009 , B01J35/1014 , B01J2523/00 , C07C51/265 , C07C63/16 , B01J2523/15 , B01J2523/47 , B01J2523/53 , B01J2523/55 , B01J2523/51
摘要： Catalyst systems for preparing phthalic anhydride by means of gas-phase oxidation of o-xylene and/or naphthalene, and a process for preparing phthalic anhydride using the catalyst systems
摘要翻译：通过邻二甲苯和/或萘的气相氧化制备邻苯二甲酸酐的催化剂体系，以及使用催化剂体系制备邻苯二甲酸酐的方法

5. 发明申请

US20080312450A1 Method for Start-Up of Oxidation Catalysts 审中-公开
标题翻译：氧化催化剂启动方法
公开(公告)号：US20080312450A1
公开(公告)日：2008-12-18
申请号：US11994516
申请日：2006-06-30
申请人： Samuel Neto , Frank Rosowski , Sebastian Storck , Juergen Zuehlke , Hans-Martin Allmann , Thomas Lautensack , Rainer Steeg
发明人： Samuel Neto , Frank Rosowski , Sebastian Storck , Juergen Zuehlke , Hans-Martin Allmann , Thomas Lautensack , Rainer Steeg
IPC分类号： C07D213/79 , C07C27/10 , C07D307/60 , C07D307/89 , C07C51/16
CPC分类号： C07D307/34 , B01J23/002 , B01J2523/00 , C07C51/265 , C07C51/313 , C07C63/16 , B01J2523/15 , B01J2523/47 , B01J2523/53 , B01J2523/55 , B01J2523/824
摘要： Methods comprising: providing an oxidation catalyst bed; and starting up the oxidation catalyst at a temperature of 360° C. to 400° C. with an amount of air of 1.0 to 3.5 standard m3/h and a hydrocarbon loading of 20 to 65 g/standard m3, such that a hot spot having a temperature of 390° C. to
摘要翻译：方法包括：提供氧化催化剂床; 并在360℃至400℃的温度下启动氧化催化剂，空气量为1.0-3.5标准立方米/小时，烃装载量为20至65克/标准立方米，使得热点在催化剂床的前7-20％中形成温度为390℃至<450℃的温度。

6. 发明申请

US20070135302A1 Mehtod for the production of a catalyst for gas-phase oxidations by the coating of support materials in a fluid bed apparatus 审中-公开
标题翻译： Mehtod用于通过在流化床装置中涂覆支撑材料来生产用于气相氧化的催化剂
公开(公告)号：US20070135302A1
公开(公告)日：2007-06-14
申请号：US10573480
申请日：2004-09-24
申请人： Samuel Neto , Wolfgang Rummel , Sebastien Storck , Jurgen Zuhlke , Frank Rosowski
发明人： Samuel Neto , Wolfgang Rummel , Sebastien Storck , Jurgen Zuhlke , Frank Rosowski
IPC分类号： B01J23/00
CPC分类号： B01J2/16 , B01J2/006 , B01J23/22 , B01J35/0006 , B01J35/002 , B01J35/1014 , B01J37/0009 , B01J37/0221 , B01J37/0232 , B01J37/0244
摘要： The invention relates to a process for producing a catalyst for gas-phase oxidations, which comprises weighing a particulate inert support having a total mass of Msupport into a fluidized-bed apparatus, providing an aqueous suspension of a catalytically active material or sources therefor and a binder having a binder content of Bsusp, fluidizing the inert support by introduction of a gas stream heated to a temperature of Tgas at a flow rate of Qgas, and spraying the suspension at a rate of Qsusp onto the fluidized inert support. When Qgas, Qsusp, Bsusp, Msupport and Tgas are selected within the ranges 3000≦Qgas [m3/h]≦9000, 1000≦Qsusp [g/min]≦3500, 2≦Bsusp [% by weight]≦18, 60≦Msupport [kg]≦240. 75≦Tgas [° C.]≦120 so that a parameter K defined as K=0.020 Qgas−0.055 Qsusp+7.500 Bsusp−0.667 Msupport+2.069 Tgas−7satisfies the relationship 127.5≦K≦202, high-quality coatings can be produced and the formation of twins made up of support particles adhering to one another can be avoided.
摘要翻译：本发明涉及一种用于生产气相氧化催化剂的方法，该方法包括将具有总质量的载体的颗粒惰性载体称重到流化床装置中，提供水悬浮液催化活性材料或其来源以及具有粘合剂含量为B susp susp susp susp susp a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a Q气体的流速，并以悬浮液的速度将悬浮液喷雾到流化的惰性载体上。当气体气体时，Q 1，B 2，B 3，M 3，N 2，在3000以下范围内选择气体[m 3 / h] <= 9000,1000 <= Q [g / min ] <= 3500，2 <= B [重量％] <= 18,60 <= M [kg] = 240。 75 <= T [°C] <= 120，使得定义为<？in-line-formula description =“In-Line Formulas”end =“lead”？> K = 0.020 Q气体-0.055 Q + +7.500 B＆lt;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp; 气体-7 <？在线公式描述=“在线公式”end =“tail”？>满足关系127.5 <= K <= 202，可以生产高品质涂层并形成可以避免由彼此粘附的支撑颗粒构成的双胞胎。

7. 发明申请

US20070093384A1 Gas phase oxidation catalyst with defined vanadium oxide particle size distribution 有权
标题翻译：气相氧化催化剂具有规定的氧化钒粒度分布
公开(公告)号：US20070093384A1
公开(公告)日：2007-04-26
申请号：US10573481
申请日：2004-09-24
申请人： Sebastian Storck , Jurgen Zuhlke , Samuel Neto , Frank Rosowski , Wolfgang Rummel
发明人： Sebastian Storck , Jurgen Zuhlke , Samuel Neto , Frank Rosowski , Wolfgang Rummel
IPC分类号： B01J23/22
CPC分类号： C07C51/313 , B01J23/002 , B01J23/22 , B01J27/198 , B01J35/023 , B01J37/0219 , B01J37/0221 , B01J2523/00 , C07C51/265 , C07C63/16 , B01J2523/15 , B01J2523/47 , B01J2523/53 , B01J2523/55
摘要： A process is described for producing a catalyst for gas-phase oxidations, in which a suspension of TiO2 and V2O5 particles is applied to a fluidized inert support, wherein at least 90% by volume of the V2O5 particles have a diameter of 20 μm or less and at least 95% by volume of the V2O5 particles have a diameter of 30 μm or less. The defined particle size distribution of the V2O5 allows a high coating efficiency.
摘要翻译：描述了一种制备用于气相氧化的催化剂的方法，其中施加TiO 2和V 2 O 5 O 5颗粒的悬浮液涉及一种流化惰性载体，其中至少90％（体积）的V 2 O 5 O 3颗粒的直径为20μm或更小，至少95体积％ V 2 O 5颗粒的直径为30μm或更小。 V 2 O 5 O 5的限定的粒度分布允许高涂层效率。

8. 发明授权

US08609899B2 Process for preparing toluenediamine by hydrogenation of dinitrotoluene 有权
标题翻译：通过氢化二硝基甲苯制备甲苯二胺的方法
公开(公告)号：US08609899B2
公开(公告)日：2013-12-17
申请号：US13109399
申请日：2011-05-17
申请人： Andreas Raichle , Joana Coelho Tsou , Samuel Neto , Ulrich Penzel , Steffen Oehlenschlaeger , Michael Zoellinger , Holgar Braunsberg , Stefanie Haase , Johannes Buettner
发明人： Andreas Raichle , Joana Coelho Tsou , Samuel Neto , Ulrich Penzel , Steffen Oehlenschlaeger , Michael Zoellinger , Holgar Braunsberg , Stefanie Haase , Johannes Buettner
IPC分类号： C07C209/00
CPC分类号： C07C209/36 , C07C211/49
摘要： The invention relates to a process for the continuous preparation of toluenediamine by liquid-phase hydrogenation of dinitrotoluene by means of hydrogen in the presence of a suspended, nickel-comprising catalyst in a reactor with a product isolation unit downstream of the reactor to give a product output from the reactor comprising a liquid phase comprising toluenediamine and dinitrotoluene, in which the nickel-comprising catalyst is suspended, wherein the concentration of dinitrotoluene in the liquid phase of the product output from the reactor in the region between the reactor and the downstream product isolation unit is set to a value in the range from 1 to 200 ppm by weight, based on the total weight of the liquid phase of the product output from the reactor.
摘要翻译：本发明涉及通过在反应器中的悬浮的含镍催化剂存在下，借助于氢气对二硝基甲苯进行液相氢化来连续制备甲苯二胺的方法，该反应器具有在反应器下游的产物隔离单元以产生产物从包括甲苯二胺和二硝基甲苯的液相的反应器输出，其中悬浮有含镍催化剂，其中在反应器和下游产物隔离之间的区域中从反应器输出的产物的液相中二硝基甲苯的浓度基于从反应器输出的产物的液相的总重量，单位设定在1至200重量ppm的范围内的值。

9. 发明申请

US20110295039A1 PROCESS FOR PREPARING TOLUENEDIAMINE BY HYDROGENATION OF DINITROTOLUENE 有权
标题翻译：通过氢化西妥昔单抗制备托洛西胺的方法
公开(公告)号：US20110295039A1
公开(公告)日：2011-12-01
申请号：US13109399
申请日：2011-05-17
申请人： Andreas Raichle , Joana Coelho Tsou , Samuel Neto , Ulrich Penzel , Steffen Oehlenschläger , Michael Zöllinger , Holgar Braunsberg , Stefanie Haase , Johannes Büttner
发明人： Andreas Raichle , Joana Coelho Tsou , Samuel Neto , Ulrich Penzel , Steffen Oehlenschläger , Michael Zöllinger , Holgar Braunsberg , Stefanie Haase , Johannes Büttner
IPC分类号： C07C209/36
CPC分类号： C07C209/36 , C07C211/49
摘要： The invention relates to a process for the continuous preparation of toluenediamine by liquid-phase hydrogenation of dinitrotoluene by means of hydrogen in the presence of a suspended, nickel-comprising catalyst in a reactor with a product isolation unit downstream of the reactor to give a product output from the reactor comprising a liquid phase comprising toluenediamine and dinitrotoluene, in which the nickel-comprising catalyst is suspended, wherein the concentration of dinitrotoluene in the liquid phase of the product output from the reactor in the region between the reactor and the downstream product isolation unit is set to a value in the range from 1 to 200 ppm by weight, based on the total weight of the liquid phase of the product output from the reactor.
摘要翻译：本发明涉及通过在反应器中的悬浮的含镍催化剂存在下，借助于氢气对二硝基甲苯进行液相氢化来连续制备甲苯二胺的方法，该反应器具有在反应器下游的产物隔离单元以产生产物从包括甲苯二胺和二硝基甲苯的液相的反应器输出，其中悬浮有含镍催化剂，其中在反应器和下游产物隔离区域之间从反应器输出的产物的液相中二硝基甲苯的浓度基于从反应器输出的产物的液相的总重量，单位设定在1至200重量ppm的范围内的值。

10. 发明授权

US07462727B2 Multimetal oxide containing silver, vanadium and a promoter metal and use thereof 失效
标题翻译：含有银，钒和助催化剂金属的多金属氧化物及其用途
公开(公告)号：US07462727B2
公开(公告)日：2008-12-09
申请号：US10566019
申请日：2004-07-23
申请人： Samuel Neto , Hartmut Hibst , Frank Rosowski , Sebastian Storck
发明人： Samuel Neto , Hartmut Hibst , Frank Rosowski , Sebastian Storck
IPC分类号： C07D307/89 , C07C51/255 , C07C51/16 , B01J23/00
CPC分类号： C07C51/313 , B01J23/002 , B01J23/682 , B01J23/688 , B01J35/002 , B01J35/1014 , B01J35/1019 , B01J37/0045 , B01J37/0223 , B01J2523/00 , C01G31/006 , C07C51/265 , C07C63/16 , B01J2523/18 , B01J2523/3712 , B01J2523/55 , B01J2523/72 , B01J2523/47
摘要： A multimetal oxide of the formula I, Aga-cQbMcV2Od*e H2O, I where a is from 0.3 to 1.9, Q is an element selected from among P, As, Sb and/or Bi, is from 0 to 0.3, M is a metal selected from among Nb, Ce, W, Mn, Ta, Pd, Pt, Ru and/or Rh, c is from 0.001 to 0.5, with the proviso that (a-c)≧0.1, d is a number which is determined by the valence and abundance of the elements other than oxygen in the formula I and e is from 0 to 20, and also precatalysts and catalysts produced therefrom for the partial oxidation of aromatic hydrocarbons are described.
摘要翻译：式I的多金属氧化物，<？in-line-formula description =“In-Line Formulas”end =“lead”→> Aga-cQbMcV2Od * e H2O，I <？in-line-formula description =“In- 其中a为0.3〜1.9，Q为选自P，As，Sb和/或Bi的元素，为0〜0.3，M为选自Nb， Ce，W，Mn，Ta，Pd，Pt，Ru和/或Rh，c为0.001至0.5，条件是（ac）> = 0.1，d为由化合价描述了式I中的氧以外的元素和e为0至20，并且还描述了由其制备的用于芳族烃的部分氧化的预催化剂和催化剂。

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