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1. 发明授权

US5262566A Process for the preparation of optically active a-hydroxycarboxylic acids 失效
标题翻译：光学活性α-羟基羧酸的制备方法
公开(公告)号：US5262566A
公开(公告)日：1993-11-16
申请号：US988569
申请日：1992-12-10
申请人： Klaus-Helmut Mohrs , Axel Carstens , Dieter Hoppe
发明人： Klaus-Helmut Mohrs , Axel Carstens , Dieter Hoppe
IPC分类号： C07B53/00 , C07C51/06 , C07C59/54 , C07C59/56 , C07C59/72 , C07D263/04 , C07C59/40 , C07D263/52
CPC分类号： C07D263/04 , C07C59/54 , Y02P20/55
摘要： The invention relates to a process for the preparation of optically active .alpha.-hydroxycarboxylic acids characterised in that carbamates are first reacted in the presence of a selective base and of a chelate-forming diamine to give a carbanion complex compound, this is then dia- or enantioselectively deprotonated, then substituted with CO.sub.2 and, as a final step, the heterocyclic protective group is eliminated.
摘要翻译：本发明涉及一种制备光学活性α-羟基羧酸的方法，其特征在于氨基甲酸酯首先在选择性碱和螯合形成二胺的存在下反应，得到碳负离子络合物，然后将其直接或对映选择性去质子化，然后用CO 2代替，作为最后一步，消除了杂环保护基。

2. 发明授权

US5223633A Preparation of sec. or tert. alcohols 失效
标题翻译：准备秒或叔。醇类
公开(公告)号：US5223633A
公开(公告)日：1993-06-29
申请号：US837713
申请日：1992-02-19
申请人： Dieter Hoppe , Petra Tebben , Folker Hintze , Thomas Raffel
发明人： Dieter Hoppe , Petra Tebben , Folker Hintze , Thomas Raffel
IPC分类号： C07C29/40 , C07C31/27 , C07D263/52 , C07F7/08 , C07F7/22
CPC分类号： C07D263/52 , C07C29/40 , C07C31/27 , C07F7/0812 , C07F7/2212 , C07B2200/07 , C07C2101/14 , Y02P20/55
摘要： A process for the preparation of a compound of the formula ##STR1## which comprises deprotonating a carbamate of the formula ##STR2## in an inert solvent with a selective base, in the presence of a chelate-forming diamine to give a compound of the formula ##STR3## and then reacting III in an inert solvent, either with an achiral electrophile of the formula (IV) or (V) or with an optionally prochiral electrophile of the formula (VI) ##STR4## and in the case in which R.sup.1 represents an electrofugic leaving group, optionally again electrophilically substituted with the formation of an acyl anion and renewed deprotonation, and in a last step, solvolytically removing the protecting group --CO--NR.sup.10 R.sup.11.
摘要翻译：一种制备式（I）化合物的方法，该方法包括在惰性溶剂中用选择性碱在形成螯合物的二胺的存在下使式（II）的氨基甲酸酯去质子化至得到式（III）化合物，然后使III在惰性溶剂中与式（IV）或（V）的非手性亲电子试剂反应，或与式（VI）GY的任选的前手性亲电子试剂反应，（Ⅳ）的二氧化碳，（Ⅴ）Ⅵ（VI），在R1表示电气离去基团的情况下，任选地再次以形成酰基阴离子进行亲电取代并重新去质子化，最后一步是溶剂分解保护基-CO-NR10R11。

3. 发明授权

US4496723A Process for the preparation of 7-amino-1-dethia-1-oxa-3-hydroxymethyl-cephem-4-carboxylic acids 失效
标题翻译：制备7-氨基-1-脱硫-1-氧杂-3-羟甲基头孢烯-4-羧酸的方法
公开(公告)号：US4496723A
公开(公告)日：1985-01-29
申请号：US506731
申请日：1983-06-20
申请人： Dieter Hoppe , Heinz-Werner Kleemann
发明人： Dieter Hoppe , Heinz-Werner Kleemann
IPC分类号： A61K31/535 , A61P31/04 , C07D319/06 , C07D405/06 , C07D498/04 , C07D498/14 , C07D505/00 , C07D513/10
CPC分类号： C07D405/06 , C07D319/06 , C07D505/00 , C07D513/10
摘要： Compounds which themselves are antibacterially active and/or which are useful as intermediates for producing antibacterially active materials such as penicillins and cephalosporins are obtained by the following syntheses:Benzyl-2-(2,2-dimethyl-1,3-dioxan-5-ylidene)-2(N-formyl-1)-aminoacetate to benzyl-2,2-dimethylspiro-[1,3-dioxane-5,5'-1',3-thiazoline]-4'-carboxylate to benzyl 2-(2,2-dimethyl-1,3-dioxan-5-ylidene)-2[N-(methylthiomethylene)-amino] acetate to benzyl 2-(trans-3-azido-4-methylthio-2-oxo-1-azetidinyl)-2-(2,2-dimethyl-1,3-dioxan-5-ylidene) acetate to benzyl 2(trans-3-benzoylamino-4-methylthio-1-azetidinyl)-2-(2,2-dimethyl-1,3-dioxan-5-ylidene) acetate to either (1) benzyl 2-(7-oxo-3-phenyl-4-oxa-2,6-diazabicyclo[3.2.0]hept-2-en-6-yl)-2-(2,2-dimethyl-1.3-dioxan-5-ylidene)acetate or (2) benzyl 2-(trans-3-benzoylamino-4-chloro-1-azetidinyl)-2-(2,2-dimethyl-1,3-dioxan-5-ylidene) acetate and then to the product benzyl-7-benzoylamino-1-dethia-1-oxa-3-hydroxymethyl-cephem-4-carboxylate.
摘要翻译：通过以下合成得到本身具有抗菌活性和/或可用作生产抗菌活性物质如青霉素和头孢菌素的中间体的化合物：苄基-2-（2,2-二甲基-1,3-二恶烷-5-基）亚基）-2（N-甲酰基-1） - 氨基乙酸酯向苄基-2,2-二甲基螺 - [1,3-二恶烷-5,5'-1'，3-噻唑啉] -4'-羧基末端加成苄基2 - （2,2-二甲基-1,3-二恶烷-5-亚基）-2 [N-（甲基亚硫代亚甲基） - 氨基]乙酸酯向2-（反式-3-叠氮基-4-甲硫基-2-氧代-1 -2-（2,2-二甲基-1,3-二恶烷-5-亚基）乙酸酯向苄基2（反式-3-苯甲酰基氨基-4-甲硫基-1-氮杂环丁烷基）-2-（2,2-二甲基-1,3-二恶烷-5-亚基）（1）苄基2-（7-氧代-3-苯基-4-氧杂-2,6-二氮杂双环[3.2.0]庚-2-烯-2-酮）吡啶-6-基）-2-（2,2-二甲基-1,3-二恶烷-5-亚基）乙酸酯或（2）2-（反式-3-苯甲酰基氨基-4-氯-1-氮杂环丁烷基）-2-（2 ，2-二甲基-1,3-二氧代-5-亚基）乙酸酯，然后向产物中加入苄基-7-苯甲酰氨基-1-脱硫-1-氧杂-3-羟甲基头孢-4-基羧基吃。

4. 发明授权

US4960462A Acicular, ferromagnetic metal particles essentially consisting of iron, and their preparation 失效
标题翻译：针状，铁磁金属颗粒基本上由铁组成，其制备方法
公开(公告)号：US4960462A
公开(公告)日：1990-10-02
申请号：US284246
申请日：1988-12-14
申请人： Michael W. Mueller , Kalus-Dieter Hoppe , Ekkehard Schwab , Werner Steck , Helmut Auweter , Rainer Feser
发明人： Michael W. Mueller , Kalus-Dieter Hoppe , Ekkehard Schwab , Werner Steck , Helmut Auweter , Rainer Feser
IPC分类号： B22F9/20 , B22F9/22 , G11B5/706 , H01F1/047 , H01F1/06
CPC分类号： G11B5/70615 , B22F9/22
摘要： Acicular, ferromagnetic metal particles which essentially consist of iron and have a nickel content of not more than 0.4% by weight and high values for coercive force and magnetization, and a process for the preparation of these particles. The particles further include zinc, phosphorus in the form of phosphate ions, and silicon in the form of SiO.sub.2.
摘要翻译：针状，铁质金属颗粒，其主要由铁组成且镍含量不超过0.4重量％，矫顽力和磁化强度高，以及制备这些颗粒的方法。颗粒还包括呈磷酸根离子形式的锌，磷和SiO 2形式的硅。

5. 发明授权

US4933004A Preparation of acicular ferromagnetic metal particles of substantially iron 失效
标题翻译：制备基本上铁的针状铁磁性金属颗粒
公开(公告)号：US4933004A
公开(公告)日：1990-06-12
申请号：US11127
申请日：1987-02-05
申请人： Klaus-Dieter Hoppe , Werner Steck , Jenoe Kovacs , Rainer Feser , Helmut Jakusch
发明人： Klaus-Dieter Hoppe , Werner Steck , Jenoe Kovacs , Rainer Feser , Helmut Jakusch
IPC分类号： B22F9/20 , B22F9/22 , C01G49/06 , G11B5/706 , G11B5/712 , H01F1/06
CPC分类号： B82Y30/00 , B22F9/22 , C01G49/06 , G11B5/70615 , G11B5/712 , C01P2002/54 , C01P2004/10 , C01P2004/62 , C01P2004/64 , C01P2006/12 , C01P2006/42
摘要： Ferromagnetic metal particles of substantially iron are prepared by starting from an acicular .alpha.-FeOOH, applying a shape-stabilizing finish to the particle surface, heating at 500.degree.-850.degree. C. and subsequently reducing with gaseous reducing agents at 200.degree.-500.degree. C. to the metal, and starting .alpha.-FeOOH being prepared in the presence of zinc and phosphate ions.
摘要翻译：基本上铁的铁磁性金属颗粒通过从针状α-FeOOH开始制备，对颗粒表面施加形状稳定整理剂，在500-850℃下加热，然后在200-500℃下用气态还原剂还原并且在锌和磷酸根离子存在下制备起始的α-FeOOH。

6. 发明授权

US4879102A Regeneration of wash solutions containing Fe(II) and Fe(III) chelate complexes 失效
标题翻译：含有Fe（II）和Fe（III）螯合物的洗涤液的再生
公开(公告)号：US4879102A
公开(公告)日：1989-11-07
申请号：US251449
申请日：1988-09-30
申请人： Klaus-Dieter Hoppe , Bernd Leutner , Siegfried Schreiner
发明人： Klaus-Dieter Hoppe , Bernd Leutner , Siegfried Schreiner
IPC分类号： B01D53/14 , B01D53/56
CPC分类号： B01D53/1425 , B01D53/14 , B01D53/56
摘要： Wash solutions containing Fe(II) and Fe(III) chelate complexes and used for removing NO.sub.x from waste gases are regenerated by treatment with sodium tetrahydroborate.
摘要翻译：含有Fe（II）和Fe（III）螯合络合物并用于从废气中除去NOx的洗涤溶液通过用四氢硼酸钠处理再生。

7. 发明授权

US06352660B1 Preparation of composite fibers and diaphragms 失效
标题翻译：复合纤维和隔膜的制备
公开(公告)号：US06352660B1
公开(公告)日：2002-03-05
申请号：US09176151
申请日：1998-10-21
申请人： Holger Friedrich , Ulrich Bröckel , Dieter Schläfer , Klaus-Dieter Hoppe , Kurt Hecky , Peter Palm
发明人： Holger Friedrich , Ulrich Bröckel , Dieter Schläfer , Klaus-Dieter Hoppe , Kurt Hecky , Peter Palm
IPC分类号： B29G126
CPC分类号： C25B13/08 , D01D5/24 , D01F1/10 , D01F6/12 , D01F6/62 , D04H1/4209 , D04H1/4318 , D04H1/4382 , D04H1/60 , D04H11/00 , Y10S428/904 , Y10T428/2913 , Y10T428/3154 , Y10T428/31544
摘要： Composite fibers useful for preparing diaphragms are prepared by (a) mixing a PTFE or PTFE copolymer dispersion or powder with a finely divided inorganic material and a fiber forming material, (b) shear heating the resulting mixture to a temperature at which sheared to PTFE or PTFE copolymer becomes flowable without showing signs of decomposition while removing the dispersion medium, if a PTFE or PTFE copolymer dispersion is used, (c) cooling the mixture to below 70° C., (d) mix shearing the mixture at below 70° C. to form composite fibers.
摘要翻译：制备用于制备隔膜的复合纤维通过（a）将PTFE或PTFE共聚物分散体或粉末与细碎的无机材料和纤维形成材料混合来制备，（b）将所得混合物剪切加热至剪切至PTFE或如果使用PTFE或PTFE共聚物分散体，则PTFE共聚物可以流动，而不会分解分解物质，（c）将混合物冷却至低于70℃，（d）将混合物在70℃以下混合形成复合纤维。

8. 发明授权

US5919348A Modification of the flow resistance of diaphragms 失效
标题翻译：修改隔膜的流动阻力
公开(公告)号：US5919348A
公开(公告)日：1999-07-06
申请号：US982441
申请日：1997-12-02
申请人： Holger Friedrich , Klaus-Dieter Hoppe , Bernd Leutner , Dieter Schlafer , Kurt Hecky
发明人： Holger Friedrich , Klaus-Dieter Hoppe , Bernd Leutner , Dieter Schlafer , Kurt Hecky
IPC分类号： C25B13/08 , C25B13/00 , C25B15/00 , C25B1/46
CPC分类号： C25B13/00 , C25B15/00
摘要： The flow resistance of a diaphragm based on a fiber material is modified by treating the diaphragm during or after preparation thereof with a dispersion comprising a fluorine-containing component and optionally with a solution comprising a precursor of ZrO.sub.2.
摘要翻译：基于纤维材料的隔膜的流动阻力通过在包含含氟组分的分散体和任选地含有包含ZrO 2的前体的溶液的制备过程中或之后处理膜来改变。

9. 发明授权

US5077023A Reduction in the rate of oxidation of sulfite solutions 失效
标题翻译：降低亚硫酸盐溶液的氧化速率
公开(公告)号：US5077023A
公开(公告)日：1991-12-31
申请号：US551777
申请日：1990-07-12
申请人： Bernd Leutner , Klaus-Dieter Hoppe , Paul Bever , Matthias Kraume
发明人： Bernd Leutner , Klaus-Dieter Hoppe , Paul Bever , Matthias Kraume
IPC分类号： B01D53/50
CPC分类号： B01D53/501
摘要： The rates of oxidation of sulfite/bisulfite-containing solutions in gas-liquid scrubbers for removing SO.sub.2 from gases are reduced by adding oxidation inhibitors to the solutions in an amount of from 0.02 to 20 mmol per hour and per square meter of exchange area.
摘要翻译：用于从气体中除去SO 2的气液洗涤器中的亚硫酸盐/亚硫酸氢盐溶液的氧化速率通过以每小时0.02至20毫摩尔/平方米的交换面积的量向该溶液中加入氧化抑制剂来降低。

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