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81. 发明授权

US5084106A Monoazo lake pigment 失效
标题翻译： MONOAZO湖色
公开(公告)号：US5084106A
公开(公告)日：1992-01-28
申请号：US137264
申请日：1987-12-23
申请人： Nagatoshi Kobayashi , Hirohito Ando
发明人： Nagatoshi Kobayashi , Hirohito Ando
IPC分类号： C09B63/00 , C09B67/00 , C09B67/48
CPC分类号： C09B67/0029 , C09B63/005
摘要： A monoazo lake pigment of the formula (I): ##STR1## whose X-ray diffraction pattern shows a high diffraction intensity at a diffraction angle (2.theta..+-.0.2.degree.; Cu - K.sub..alpha.) of 4.9.degree., moderate diffraction intensities at 18.4.degree., 25.9.degree. and 26.8.degree. and relatively low diffraction intensities at 11.1.degree., 15.3.degree. and 21.2.degree., and printing ink, a paint and plastics in which the monoazo lake pigment is contained.

82. 发明授权

US5011690A Spheroidal silica 失效
标题翻译：球状二氧化硅
公开(公告)号：US5011690A
公开(公告)日：1991-04-30
申请号：US202563
申请日：1988-06-06
申请人： Michael J. Garvey , Ian C. Griffiths , John H. S. Rennie
发明人： Michael J. Garvey , Ian C. Griffiths , John H. S. Rennie
IPC分类号： C01B33/18 , A01N25/12 , A61K8/25 , A61K9/14 , A61K9/16 , A61L9/04 , A61Q13/00 , A61Q19/00 , B01J13/04 , C01B33/12 , C01B33/187 , C09B63/00 , C09C1/30 , C11D3/12
CPC分类号： C11D3/124 , A01N25/12 , A61K8/25 , A61K9/143 , A61K9/1611 , A61K9/1694 , A61L9/046 , A61Q19/00 , B01J13/046 , C09B63/00 , C09C1/30 , A61K2800/412 , A61Q13/00 , C01P2004/32 , C01P2004/61 , C01P2006/14 , C01P2006/16 , C01P2006/17 , C01P2006/80 , Y10T428/2989
摘要： Porous spheroidal silica having a particle size in the range 1 to 400 microns, axial ratios of 1:1 to 1:12 has up to 50% by weight of the SiO.sub.2 of included material, such as for example perfumes, flavoring materials, pigments, germicides, bactericides, fungicides, bleaching agents, skin benefit agents, therapeutic agents, dispersed in the silica as particles or droplets in the size range 0.01 to 10 .mu.m. The spheroids can be made by mixing together an aqueous, stabilized silica sol containing dispersed therein up to 50% by weight of the silica of an included material and an aqueous solution of a non-adsorbing polymer to form a phase separated system comprising silica droplets containing included material in a polymer-rich continuous phase and condensing the silica sol to aggregate the droplets to form silica spheroids containing the dispersed included material. The included material can be released in use by e.g. wetting, attrition, dissolution, pH change, heating.

83. 发明授权

US4980458A Mixed sodium, ammonium and/or calcium salt crystals of laked monoazo disulfonated pyrazolone pigments 失效
标题翻译：浸渍的单偶氮二磺化吡唑啉酮颜料的混合的钠，铵和/或钙盐晶体
公开(公告)号：US4980458A
公开(公告)日：1990-12-25
申请号：US349907
申请日：1989-05-08
申请人： Stefan Hari , Arnold Grubenmann , Andreas Burkhard
发明人： Stefan Hari , Arnold Grubenmann , Andreas Burkhard
IPC分类号： C09B67/48 , C08K5/22 , C08K5/23 , C08K5/41 , C08K5/42 , C09B63/00 , C09B67/22 , C09B69/02
CPC分类号： C09B67/0051 , C09B69/02 , Y10S534/01
摘要： Mixed crystals of at least two different compounds of formula I ##STR1## wherein R is --CH.sub.3, phenyl, --COOCH.sub.3, --COOCH.sub.3, --COOC.sub.2 H.sub.5, --NHCO--C.sub.1 -C.sub.4 alkyl or --CONH--C.sub.1 -C.sub.4 alkyl, M.sup.+ and M.sub.1.sup.+ are each independently of the other an alkali metal cation, an alkaline earth metal cation or a heavy metal cation or NH.sub.4.sup.+ ; wherein X, Y, X' and Y' are each independently hydrogen, halogen, --CH.sub.3, --C.sub.2 H.sub.5, --OCH.sub.3, --OC.sub.2 H.sub.5, --NO.sub.2 or the group of formula --NHCO--C.sub.1 -C.sub.4 alkyl, wherein at least two of the cations M.sup.+ and M.sub.1.sup.+ in the compounds forming the mixed crystals of formula I are different and the X-ray diffraction patterns of the mixed crystals differ from the X-ray diffraction patterns of the individual components and of their sum. Such mixed crystals are most suitable as pigments for coloring high molecular organic material and are distinguished in particular by surprisingly high color strength and pure shade.
摘要翻译：至少两种不同的式I化合物的混合晶体（I）其中R是-CH 3，苯基，-COOCH 3，-COOCH 3，-COOC 2 H 5，-NHCO-C 1 -C 4烷基或-CONH-C 1 -C 4烷基， M +和M1 +各自独立地为碱金属阳离子，碱土金属阳离子或重金属阳离子或NH4 +; 其中X，Y，X'和Y'各自独立地为氢，卤素，-CH 3，-C 2 H 5，-OCH 3，-OC 2 H 5，-NO 2或式-NHCO-C 1 -C 4烷基的基团，其中至少两个形成式I的混合晶体的化合物中的阳离子M +和M1 +是不同的，并且混晶的X射线衍射图与各个组分的X射线衍射图和它们的和不同。这种混合晶体最适合作为着色高分子有机材料的颜料，特别是出人意料地高的着色强度和纯净的色调。

84. 发明授权

US4773936A Insoluble pigments and preparation thereof 失效
标题翻译：不溶性颜料及其制备方法
公开(公告)号：US4773936A
公开(公告)日：1988-09-27
申请号：US876558
申请日：1986-06-20
申请人： Howard W. Clark , Tracy E. Chapman , Ronald L. Yates
发明人： Howard W. Clark , Tracy E. Chapman , Ronald L. Yates
IPC分类号： C09B63/00 , C09B67/20 , C09B69/02 , C09C1/02 , C09C3/08
CPC分类号： C09B67/0061 , C09B63/00 , C09B69/02
摘要： A water-insoluble pigment comprising a complex of a water-insoluble inorganic substrate exhibiting anion exchange properties, a water-soluble dye, and an anionic amphipathic material is disclosed.
摘要翻译：公开了一种包含显示出阴离子交换性质的水不溶性无机底物的络合物的水不溶性颜料，水溶性染料和阴离子两亲性材料。

85. 发明授权

US4772331A Flaky colored pigments, methods for their production, and their use in cosmetic compositions 失效
标题翻译：片状着色颜料，其制备方法及其在化妆品组合物中的用途
公开(公告)号：US4772331A
公开(公告)日：1988-09-20
申请号：US922901
申请日：1986-10-24
申请人： Tamio Noguchi , Takaji Watanabe
发明人： Tamio Noguchi , Takaji Watanabe
IPC分类号： C09B67/08 , A61K8/11 , A61Q1/02 , C04B14/36 , C08J7/04 , C09B63/00 , C09B67/02 , C09B67/22 , C09C1/00 , C09C1/28 , C09C1/40 , C09C1/42 , C09C3/00 , C09C3/08 , C09C3/10 , C04B14/20 , A61K7/035
CPC分类号： C09C1/405 , A61K8/0254 , A61K8/26 , A61K8/8129 , A61K8/8176 , A61K8/86 , A61Q1/02 , C09B63/00 , C09B67/0033 , C09B67/0097 , C09C1/0015 , C09C1/28 , C09C1/32 , C09C1/42 , C09C3/006 , A61K2800/412 , A61K2800/436 , A61K2800/614 , C01P2004/03 , C01P2004/20 , C01P2004/61 , C01P2004/62 , C01P2006/60 , C01P2006/90 , C09C2200/102 , C09C2200/301 , C09C2200/409 , C09C2200/507 , Y10S514/844
摘要： Colored flaky colored pigments are obtained by uniformly adhering a finely divided color pigment onto a flaky substrate by the use of an high molecular weight organic compound as a binder.
摘要翻译：通过使用高分子量有机化合物作为粘合剂，将细碎的着色颜料均匀地粘附在片状基材上，得到着色的片状着色颜料。

86. 发明授权

US4670486A Polymer composition pigmented with copper or nickel complexes of ligands containing a semicarbazone moiety 失效
标题翻译：用含有缩氨基脲部分的配体的铜或镍络合物着色的聚合物组合物
公开(公告)号：US4670486A
公开(公告)日：1987-06-02
申请号：US745034
申请日：1985-06-13
申请人： Georg Cseh , Paul Lienhard
发明人： Georg Cseh , Paul Lienhard
IPC分类号： C09B45/14 , C08K5/00 , C08K5/23 , C09B56/00 , C09B45/48 , C09B63/00 , C09B67/20 , C09D3/48
CPC分类号： C09B56/00 , C08K5/0091 , C08K5/23 , Y10S8/09 , Y10S8/92 , Y10S8/928
摘要： High molecular weight organic material is effectively colored by the incorporation therein of a copper or nickel complex of the ligand compound of formula I ##STR1## wherein A is an isocyclic or heterocyclic aromatic moiety, R is H, halogen, lower alkyl or alkoxy, R.sub.1 is H, lower alkyl, phenyl or substituted phenyl, and B is H, lower alkyl, ureido or substituted ureido, guanidino, anilino, benzamido or a heterocyclic aromatic moiety.
摘要翻译：高分子量有机材料通过掺入式I配体化合物（I）的铜或镍络合物而有效着色，其中A是一个环状或杂环芳族部分，R是H，卤素，低级烷基或烷氧基，R 1为H，低级烷基，苯基或取代的苯基，B为H，低级烷基，脲基或取代的脲基，胍基，苯胺基，苯甲酰氨基或杂环芳族部分。

87. 发明授权

US4652313A Aqueous lake pigment suspension 失效
标题翻译：水性色淀悬浮液
公开(公告)号：US4652313A
公开(公告)日：1987-03-24
申请号：US664320
申请日：1984-10-24
申请人： Patrick Den Boer , Richard F. Heinze , Benjamin L. Meyers , Barendra C. Mallik
发明人： Patrick Den Boer , Richard F. Heinze , Benjamin L. Meyers , Barendra C. Mallik
IPC分类号： C09B63/00 , A23L5/40 , A61K9/28 , A61K9/34 , C09B67/20 , C09B67/46 , C09D17/00 , C09D105/00 , C09D121/00 , C09D3/10
CPC分类号： A61K9/28 , C09D17/001
摘要： This invention relates to a pigment suspension usable for film coating tablets and the like, comprising lake pigment particles, a polymeric colloid, a viscosity lowering agent, which permits a higher concentration of pigment particles in the pigment suspension, and an aqueous solvent. A typical pigment suspension comprises a lake pigment, titanium dioxide, a natural gum, sodium tartrate, and water.
摘要翻译：本发明涉及可用于薄膜包衣片等的颜料悬浮液，其包含颜料悬浮液中颜料颗粒较高浓度的色淀颗粒，聚合物胶体，降粘剂，以及水性溶剂。典型的颜料悬浮液包含色淀颜料，二氧化钛，天然胶，酒石酸钠和水。

88. 发明授权

US4628082A Derivatives of azobarbituric acid or salts or complexes thereof 失效
标题翻译：偶氮巴比妥酸的衍生物或其盐或配合物
公开(公告)号：US4628082A
公开(公告)日：1986-12-09
申请号：US734364
申请日：1985-05-14
申请人： Manfred Lorenz , Karl H. Schundehutte
发明人： Manfred Lorenz , Karl H. Schundehutte
IPC分类号： C09B27/00 , C09B29/00 , C09B29/52 , C09B45/00 , C09B45/14 , C09B63/00 , C09B67/20 , C09B67/22 , C09B29/036 , C09B45/22
CPC分类号： C09B67/0033 , C09B27/00 , C09B29/0051 , C09B29/3673 , C09B45/00 , C09B45/14 , C09B63/00 , C09B67/006 , Y10S534/04
摘要： Azobarbituric acid derivatives characterized in that in their free acid form they have the following tautomeric structure are disclosed: ##STR1## The azobarbituric acid derivatives are characterized in that X and Y rings can each carry one or two substituents from the series comprising .dbd.O, .dbd.S, .dbd.NR.sub.7, --NR.sub.6 R.sub.7, --OR.sub.6, --SR.sub.6, --COOR.sub.6, --CN, --CONR.sub.6 R.sub.7, --SO.sub.2 R.sub.8, ##STR2## alkyl, cycloalkyl, aryl and aralkyl, the total number of the endocyclic and exocyclic double bonds for each of the rings X and Y being three.The new azobarbituric acid derivatives are other than those of azobarbituric acid, azouracil and uracil-5-azobarbituric acid and their salts. The compounds are useful as pigments which pigments are useful for pigmented paints, in printing inks, distempers or emulsion paints, inter alia.
摘要翻译：偶氮巴比妥酸衍生物的特征在于其游离酸形式具有以下互变异构结构：偶氮巴比妥酸衍生物的特征在于，X和Y环各自可以带有一个或两个包含= O， = S，= NR7，-NR6R7，-OR6，-SR6，-COOR6，-CN，-CONR6R7，-SO2R8，烷基，环烷基，芳基和芳烷基，每个的内环和外环双键的总数的环X和Y为三个。新偶氮巴比妥酸衍生物与偶氮巴比妥酸，氮尿嘧啶和尿嘧啶-5-偶氮巴比妥酸及其盐类不同。这些化合物可用作颜料，其颜料可用于着色涂料，印刷油墨，碲化物或乳液漆等。

89. 发明授权

US4486237A Composite pigments and process for their preparation 失效
标题翻译：复合颜料及其制备方法
公开(公告)号：US4486237A
公开(公告)日：1984-12-04
申请号：US468121
申请日：1983-02-22
申请人： Camillo Paffoni , Luigi Balducci , Giorgio Bottaccio , Marcello Pieroni
发明人： Camillo Paffoni , Luigi Balducci , Giorgio Bottaccio , Marcello Pieroni
IPC分类号： C09B25/00 , C09B29/00 , C09B29/01 , C09B29/15 , C09B29/36 , C09B63/00 , C09B67/08 , C09B67/22 , C09C1/00 , C09C1/40 , C04B31/40
CPC分类号： C09B63/00 , C09B25/00 , C09B29/00 , C09B29/0007 , C09B29/103 , C09B29/36 , C09B67/0033 , C09C1/0084 , C01P2004/80 , C01P2006/12 , C01P2006/60
摘要： Novel composite pigments containing both organic and inorganic portions have been produced.These pigments consist of an inorganic binary titanium dioxide/aluminum hydrate component, in a percent quantity comprised between 70% and 95% by weight, the remaining organic component amounting to between 5% and 30% by weight, consisting of an organic dye selected from the group consisting of azoic and quinophtalonic compounds, containing in their structure at least one carboxylic and/or sulphonic, substantially salified, acid function.The pigments are obtained according to a co-precipitation process, under substantially alkaline controlled pH conditions, of the acid organic dye together with the aluminum hydroxide (hydrated aluminum), by acidification of a solution and/or an aqueous dispersion of the acid organic dye in sodium aluminate, in the presence of titanium dioxide, at from 40.degree. C. to about 80.degree. C., and by a subsequent lacquering by treatment with an aqueous solution of an alkaline-earth metal salt (Ca, Mg, Ba, Sr) or of a Mn, Zn salt.The above-mentioned pigments are insoluble in water and in common organic solvents. They possess, moreover, a good dyeing power, an excellent stability under heat, a good fastness to light, a good fastness to bases and acids, to migration in plastic materials and stability to over varnishing in the stove, etc. Lastly, they may be obtained with different degrees of covering power.Thus, the pigments find a preferential application in varnishing products, air-drying and stove-baked enamels, in the pigmentation of plastic materials, in inks and in the beprinting of fabrics, etc., by means of conventional applicational methods.
摘要翻译：已经制备了含有有机部分和无机部分的新型复合颜料。这些颜料由无机二元二氧化钛/铝水合物成分组成，其含量为70％至95％（重量），剩余有机成分为5％至30％（重量），由选自该组由偶氮和喹啉酮化合物组成，其结构含有至少一种羧酸和/或磺酸，基本上盐化的酸功能。根据酸性有机染料与氢氧化铝（水合铝）一起的共沉淀法，在碱性控制的pH条件下，通过酸性有机染料的水溶液和/ 在铝酸钠存在下，在二氧化钛的存在下，在40℃至约80℃，然后通过用碱土金属盐（Ca，Mg，Ba，Sr ）或Mn，Zn盐。上述颜料不溶于水和普通的有机溶剂。此外，它们具有良好的染色力，在热下具有优异的稳定性，良好的耐光牢度，良好的碱和酸牢度，在塑料材料中的迁移以及在炉子上过度的稳定性等。最后，它们可以获得不同程度的覆盖力。因此，通过常规应用方法，颜料可以在上漆产品，空气干燥和炉烘烤的搪瓷，塑料材料着色，油墨和织物的印刷等方面得到优先应用。

90. 发明授权

US4360460A Novel azo dyes having a 4-sulfo-5-aminomethyl naphthalene coupling moiety 失效
标题翻译：具有4-磺基-5-氨基甲基萘偶联部分的新型偶氮染料
公开(公告)号：US4360460A
公开(公告)日：1982-11-23
申请号：US217277
申请日：1980-12-16
申请人： Rudolf Hurter
发明人： Rudolf Hurter
IPC分类号： C09B29/00 , C07C67/00 , C07C301/00 , C07C303/06 , C07C309/47 , C09B29/01 , C09B29/095 , C09B43/12 , C09B62/006 , C09B62/008 , C09B62/04 , C09B62/085 , C09B62/095 , C09B62/24 , C09B62/245 , C09B62/28 , C09B62/47 , C09B62/473 , C09B62/477 , C09B62/51 , C09B62/515 , C09B63/00
CPC分类号： C09B62/006 , C09B29/0014 , C09B29/0955 , C09B62/043
摘要： Dyestuff intermediates of the formula ##STR1## wherein R.sub.1 represents hydrogen, an alkyl radical of 1 to 8 carbon atoms or a phenyl radical, R.sub.2 represents hydrogen or an acyl radical and Z represents hydrogen or a sulfo group, and the use thereof for the manufacture of azo dyes of the formula ##STR2## wherein D represents the radical of a coupling component, R.sub.1 represents hydrogen, an alkyl radical of 1 to 8 carbon atoms or a phenyl radical, and R.sub.2 represents hydrogen or an acyl radical, or of azo dyes of the formula ##STR3## wherein K is the radical of a coupling component, Z represents hydrogen or the sulfo group, and R.sub.2 represents hydrogen or an acyl radical.
摘要翻译：其中R 1表示氢，1〜8个碳原子的烷基或苯基，R 2表示氢或酰基，Z表示氢或磺基，其制备方法的用途其中D表示偶联组分的基团，R 1表示氢，1至8个碳原子的烷基或苯基，R 2表示氢或酰基，或偶氮染料其中K是偶合组分的基团，Z表示氢或磺基，R2表示氢或酰基。

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