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71. 发明申请

US20150014586A1 METHOD OF MAKING QUANTUM DOTS 有权
标题翻译：制作量子的方法
公开(公告)号：US20150014586A1
公开(公告)日：2015-01-15
申请号：US14284292
申请日：2014-05-21
申请人： QD VISION, INC.
发明人： WENHAO LIU , CRAIG BREEN
IPC分类号： C30B7/14 , C30B7/08 , H01L33/28 , C30B29/68 , C30B29/48 , C30B7/00 , C30B19/12
CPC分类号： C30B7/14 , B22F1/0018 , B22F1/025 , B22F9/24 , B82Y20/00 , B82Y30/00 , B82Y40/00 , C22C1/1026 , C22C20/00 , C30B7/005 , C30B7/08 , C30B19/12 , C30B29/48 , C30B29/68 , H01L21/02557 , H01L21/0256 , H01L21/02601 , H01L21/02628 , H01L33/28 , Y10S977/774 , Y10S977/892 , Y10S977/896 , Y10S977/95
摘要： Quantum dots and methods of making quantum dots are provided.
摘要翻译：提供量子点和制造量子点的方法。

72. 发明申请

US20130199439A1 DEVICE AND METHOD FOR CRYSTALLIZING INORGANIC OR ORGANIC SUBSTANCES 有权
标题翻译：用于结晶无机或有机物质的装置和方法
公开(公告)号：US20130199439A1
公开(公告)日：2013-08-08
申请号：US13821053
申请日：2011-09-15
申请人： Monika Spano
发明人： Monika Spano
IPC分类号： C30B7/08
CPC分类号： C30B7/08 , C30B7/00 , C30B29/54 , C30B29/58 , Y10T117/1004
摘要： A device for crystallising a molecule to be crystallised, which includes: at least one crystallisation cell that includes a crystallisation chamber for receiving a first solution S1 containing the molecule to be crystallised and the crystal seeds thereof, a dialysis membrane, and a container to be filled with a second solution S2 that contains constituents selected from the group containing crystallisation agents, additives and buffers; and at least one image acquisition means. The crystallisation device is characterized in that it includes: at least one addition means arranged to add, to the container, constituents selected from the group containing crystallisation agents, additives and buffers of solution S2; and/or at least one sampling means arranged to collect, from the container, all or a portion of solution S2. The invention also relates to a crystallisation method.
摘要翻译：一种用于使待结晶的分子结晶的装置，其包括：至少一个结晶池，其包括用于接收含有待结晶分子的第一溶液S1和其晶体种子的结晶室，透析膜和容器填充含有选自含有结晶剂，添加剂和缓冲剂的组分的成分的第二溶液S2; 和至少一个图像获取装置。结晶装置的特征在于其包括：至少一个添加装置，其被设置成向容器中添加选自含有结晶剂的组的组分，溶液S2的添加剂和缓冲剂; 和/或至少一个采样装置，其布置成从容器收集溶液S2的全部或一部分。本发明还涉及一种结晶方法。

73. 发明申请

US20130108853A1 BNA CRYSTAL 有权
标题翻译： BNA水晶
公开(公告)号：US20130108853A1
公开(公告)日：2013-05-02
申请号：US13807187
申请日：2011-06-10
申请人： Mikiko Saito , Takashi Notake , Hiroaki Minamide , Hiromasa Ito
发明人： Mikiko Saito , Takashi Notake , Hiroaki Minamide , Hiromasa Ito
IPC分类号： C30B7/08 , G02F1/355
CPC分类号： C30B7/08 , C07B2200/13 , C07C211/52 , C30B7/00 , C30B7/005 , C30B29/54 , G02F1/3551
摘要： An object of the present invention is to produce a non-conventional high-quality BNA single crystal. Another object of the present invention is to provide a process for producing the above-described high-quality BNA single crystal. Specifically, the present invention provides a BNA crystal characterized by having a half-value width of diffraction peak X-ray intensity of 100 seconds or less in a rocking curve measurement by X-ray diffraction method.
摘要翻译：本发明的目的是生产非传统的高品质BNA单晶。本发明的另一个目的是提供一种制备上述高品质BNA单晶的方法。具体地，本发明提供一种特征在于通过X射线衍射法的摇摆曲线测定中的衍射峰X射线强度的半值宽度为100秒以下的BNA晶体。

74. 发明申请

US20110203515A1 Device for crystal growth at intermediate temperatures using controlled semi-active cooling 审中-公开
标题翻译：使用受控半主动冷却在中间温度下晶体生长的装置
公开(公告)号：US20110203515A1
公开(公告)日：2011-08-25
申请号：US12931288
申请日：2011-01-29
申请人： Michael Krautter
发明人： Michael Krautter
IPC分类号： C30B7/08 , C30B35/00 , B01F13/08
CPC分类号： C30B7/08 , B01F13/0827 , B01F13/0872 , C30B29/14 , C30B35/00 , Y10T117/1008
摘要： A crystal growing cell which has computerized temperature control and agitation means to inhibit crystal nucleation. The temperature is controlled semi-actively, i.e., by monitoring the temperature with a thermistor and balancing ambient heat loss with heat added to the system by heating resistors or heating elements. When the chemical is completely dissolved by heating the mixture to a temperature above the saturation temperature, the temperature is lowered. At the saturation temperature the temperature is initially reduced slowly to avoid crystal nucleation. The saturation temperature of the initial solution is selected to be at an intermediate temperature which is high enough that the amount of dissolved material is large enough to produce a large crystal or large crystal clusters, yet not so high that the solubility curve has a large slope and therefore requires a high degree of temperature control to avoid crystal nucleation in the solution. Use of the cell with a variety of chemical solutions, each having the same saturation temperature, facilitates optimization while maintaining a simple, low cost design.
摘要翻译：具有计算机化的温度控制和搅拌的晶体生长池意味着抑制晶体成核。半主动地控制温度，即通过用热敏电阻监测温度，并通过加热电阻或加热元件平衡环境热损失与加入系统的热量。当化学品通过将混合物加热至高于饱和温度的温度完全溶解时，温度降低。在饱和温度下，温度最初缓慢降低以避免晶体成核。初始溶液的饱和温度选择为足够高的中间温度，使得溶解的材料的量足够大以产生大的晶体或大的晶体簇，但不太高，使得溶解度曲线具有大的斜率因此需要高度的温度控制以避免溶液中的晶体成核。使用具有各种具有相同饱和温度的各种化学溶液的电池便于优化，同时保持简单，低成本的设计。

75. 发明申请

US20110142741A1 CRYSTAL GROWTH IN SOLUTION UNDER STATIC CONDITIONS 有权
标题翻译：在静态条件下的解决方案中的晶体生长
公开(公告)号：US20110142741A1
公开(公告)日：2011-06-16
申请号：US12517928
申请日：2007-12-03
申请人： Alain Jean Theodore Ibanez , Julien Raphael Zaccaro
发明人： Alain Jean Theodore Ibanez , Julien Raphael Zaccaro
IPC分类号： C30B7/08 , C01B25/30
CPC分类号： C30B7/08 , C30B29/14 , C30B35/00 , Y10T117/1024
摘要： A method for growing crystals in solution is suitable for the rapid, controlled and effective preparation of crystals of large dimensions from a solution supersaturated with a compound. The crystal growth is carried out under static conditions. To do this: the growth is performed in a crystallisation chamber kept at a constant temperature Tc, which chamber is in fluid communication with a saturation chamber at a temperature Ts, similarly constant and different from Tc, with solubility of the compound at the temperature Ts greater than the solubility of the compound at the temperature Tc. A continuous circulation of the solution between the crystallisation and saturation chambers is established, thus maintaining a constant supersaturation rate within the crystallisation chamber. Furthermore, the circulating solution is subjected to a treatment for eliminating and inhibiting the formation of aggregates, enabling the nucleation of parasitic crystallites to be inhibited.
摘要翻译：在溶液中生长晶体的方法适用于从化合物过饱和的溶液中快速，有控制和有效地制备大尺寸晶体。晶体生长在静态条件下进行。为了做到这一点：在保持恒温Tc的结晶室中进行生长，该室与饱和室在温度Ts下流动连通，温度Ts类似地恒定且不同于Tc，化合物在温度Ts下的溶解度大于化合物在温度Tc下的溶解度。建立溶液在结晶室和饱和室之间的连续循环，从而在结晶室内维持恒定的过饱和速率。此外，对循环溶液进行消除和抑制聚集体形成的处理，能够抑制寄生微晶的成核。

76. 发明申请

US20110088613A1 PROCESS FOR CONTROLLING THE GROWTH OF A RALOXIFENE HYDROCHLORIDE CRYSTAL 审中-公开
标题翻译：控制盐酸氯吡格雷晶体生长的方法
公开(公告)号：US20110088613A1
公开(公告)日：2011-04-21
申请号：US12996794
申请日：2008-06-09
申请人： Massimo Ferrari , Manuel Alberelli , Alberto Ambrosini
发明人： Massimo Ferrari , Manuel Alberelli , Alberto Ambrosini
IPC分类号： C30B7/08
CPC分类号： C07D333/56
摘要： A process is described for controlling the growth of a raloxifene hydrochloride crystal i.e. for the control of raloxifene hydrochloride crystal size, comprising the steps of: a) heating under reflux a mass comprising crystalline raloxifene hydrochloride, methanol and water for a time of about 10 minutes; b) cooling the mass to 30-35° C., and c) checking the crystal size, in which steps a), b) and c) are repeated for a number of cycles n, until the desired crystal size is obtained.
摘要翻译：描述了一种用于控制盐酸雷洛昔芬晶体的生长的方法，即用于控制盐酸雷洛昔芬晶体尺寸，包括以下步骤：a）在回流下将包含结晶雷洛昔芬盐酸盐，甲醇和水的物质加热约10分钟 ; b）将质量冷却至30-35℃，和c）检查晶体尺寸，其中步骤a），b）和c）重复多次循环n，直到获得所需的晶体尺寸。

77. 发明申请

US20050238568A1 Method of synthesizing colloidal nanocrystals 有权
标题翻译：胶态纳米晶体的合成方法
公开(公告)号：US20050238568A1
公开(公告)日：2005-10-27
申请号：US11024823
申请日：2004-12-30
申请人： Kui Yu , John Ripmeester
发明人： Kui Yu , John Ripmeester
IPC分类号： C01B13/32 , C01B17/20 , C01B19/00 , C01B25/14 , C01G1/00 , C01G1/12 , C01G11/00 , C30B7/08 , C30B29/46
CPC分类号： B82Y30/00 , C01B13/328 , C01B17/20 , C01B19/007 , C01G1/00 , C01G1/12 , C01G11/00 , C01P2002/72 , C01P2002/84 , C01P2002/86 , C01P2004/64 , Y10S977/773 , Y10S977/774 , Y10S977/775 , Y10S977/813 , Y10S977/824 , Y10S977/825
摘要： A method of making nanocrystals involves adding a chalocogen source to a hot solution of a metal-containing non-organometallic compound, such as CdO, in a first ligand solvent, such as TOP, and preferably subsequently cooling the resulting mixture to a lower temperature to grow the nanocrystals at said lower temperature. The method can involve either one ligand or two-ligand systems.
摘要翻译：制备纳米晶体的方法包括在第一配体溶剂例如TOP中将含有金属的非有机金属化合物（例如CdO）的热溶液加入致胞菌源，优选随后将所得混合物冷却至较低温度至在较低温度下生长纳米晶体。该方法可以包括一个配体或两个配体体系。

78. 发明授权

US06929693B2 Single crystals, method for making single crystals by growth in solution and uses 失效
标题翻译：单晶，溶液中生长制备单晶的方法及用途
公开(公告)号：US06929693B2
公开(公告)日：2005-08-16
申请号：US10415351
申请日：2001-11-07
申请人： Vitali Tatartchenko
发明人： Vitali Tatartchenko
IPC分类号： C30B7/00 , C30B7/08
CPC分类号： C30B7/00 , C30B29/14 , Y10S117/902
摘要： The invention relates to a tetragonal single crystal (1, 11) of composition: Z(H,D)2MO4 where Z is an element or a group of elements, or a mixture of elements and/or of groups of elements chosen from the group K, N(H,D)4, Rb, Ce where M is an element chosen from the group P, As and where (H,D) is hydrogen and/or deuterium comprising an approximately parallelepipedal region of large dimensions, especially one in which the length of each of the edges of the faces, AC1, AC2, AC3, is greater than or equal to 200 mm, in particular greater than or equal to 500 mm, which crystal is obtained by crystal growth from solution, from an approximately parallelepipedal single-crystal seed (2, 22) whose edges of the faces have lengths of AG1, AG2, AG3.
摘要翻译：本发明涉及组成如下的四方晶单晶（1,11）：<？in-line-formula description =“In-line Formulas”end =“lead”？> Z（H，D）？MO formulas <<<

79. 发明授权

US06872249B2 Synthesis of colloidal nanocrystals 有权
标题翻译：胶体纳米晶体的合成
公开(公告)号：US06872249B2
公开(公告)日：2005-03-29
申请号：US09971780
申请日：2001-10-04
申请人： Xiaogang Peng , Zuoyan Peng , Lianhua Qu
发明人： Xiaogang Peng , Zuoyan Peng , Lianhua Qu
IPC分类号： C01B19/04 , C01B19/00 , C30B5/00 , C30B7/00 , H01L33/00 , H01L33/08 , H01L33/28 , C30B7/08
CPC分类号： H01L33/08 , B82Y30/00 , C01B19/007 , C01P2002/84 , C01P2004/04 , C01P2004/64 , C30B5/00 , C30B7/00 , C30B29/605 , H01L33/0087 , H01L33/28
摘要： A method of synthesizing colloidal nanocrystals is disclosed using metal oxides or metal salts as a precursor. The metal oxides or metal salts are combined with a ligand and then heated in combination with a coordinating solvent. Upon heating, the metal oxides or salts are converted to stable soluble metal complexes. The metal complexes are formed by cationic species combining with the ligands and/or with the coordinating solvent. Finally, an elemental chalcogenic precursor, for example, Se, Te, or S, is introduced into the soluble metal complex to complete the formation of the nanocrystals at a controllable rate. High-quality CdSe, CdTe, and CdS nanocrystals are produced when CdO is used as the cadmium precursor. With the present method, the size, size distribution, and shape (dots or rods) of the resulting nanocrystals can be controlled during growth. For example, the resulting nanocrystals are nearly monodisperse without any size separation. Further, the method represents a major step towards a green chemistry approach for synthesizing high-quality semiconductor nanocrystals.
摘要翻译：公开了使用金属氧化物或金属盐作为前体的合成胶态纳米晶体的方法。将金属氧化物或金属盐与配体结合，然后与配位溶剂组合加热。加热时，金属氧化物或盐转化为稳定的可溶性金属配合物。金属络合物由与配体和/或配位溶剂结合的阳离子物质形成。最后，将元素硫属前体，例如Se，Te或S引入到可溶性金属络合物中，以可控速率完成纳米晶体的形成。当CdO用作镉前体时，产生了高质量的CdSe，CdTe和CdS纳米晶体。使用本方法，可以在生长期间控制所得纳米晶体的尺寸，尺寸分布和形状（点或棒）。例如，所得到的纳米晶体几乎是单分散的，没有任何尺寸的分离。此外，该方法代表了用于合成高质量半导体纳米晶体的绿色化学方法的主要步骤。

80. 发明授权

US5788765A Crystals for ultraviolet light filters 失效
标题翻译：紫外光过滤器晶体
公开(公告)号：US5788765A
公开(公告)日：1998-08-04
申请号：US709398
申请日：1996-08-30
申请人： Narsingh B. Singh , William D. Partlow , Steven Strauch , Albert M. Stewart , John F. Jackovitz , David W. Coffey
发明人： Narsingh B. Singh , William D. Partlow , Steven Strauch , Albert M. Stewart , John F. Jackovitz , David W. Coffey
IPC分类号： C30B7/00 , C30B7/08
CPC分类号： C30B7/00 , C30B29/10
摘要： Crystals formed of a solid-solution of K.sub.2 Ni(SO.sub.4).sub.2 6H.sub.2 O provide very good materials for filtering ultraviolet light and will not deteriorate in temperatures as high as 110.degree. C. They are particularly useful in sensing devices which seek to identify the presence of ultraviolet light in the UV missile warning band.
摘要翻译：由K2Ni（SO4）26H2O的固溶体形成的晶体提供了非常好的过滤紫外线的材料，并且不会在高达110℃的温度下劣化。它们特别适用于寻求识别紫外线的存在的设备在紫外线导弹警告带。

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