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1. 发明申请

US20110203515A1 Device for crystal growth at intermediate temperatures using controlled semi-active cooling 审中-公开
标题翻译：使用受控半主动冷却在中间温度下晶体生长的装置
公开(公告)号：US20110203515A1
公开(公告)日：2011-08-25
申请号：US12931288
申请日：2011-01-29
申请人： Michael Krautter
发明人： Michael Krautter
IPC分类号： C30B7/08 , C30B35/00 , B01F13/08
CPC分类号： C30B7/08 , B01F13/0827 , B01F13/0872 , C30B29/14 , C30B35/00 , Y10T117/1008
摘要： A crystal growing cell which has computerized temperature control and agitation means to inhibit crystal nucleation. The temperature is controlled semi-actively, i.e., by monitoring the temperature with a thermistor and balancing ambient heat loss with heat added to the system by heating resistors or heating elements. When the chemical is completely dissolved by heating the mixture to a temperature above the saturation temperature, the temperature is lowered. At the saturation temperature the temperature is initially reduced slowly to avoid crystal nucleation. The saturation temperature of the initial solution is selected to be at an intermediate temperature which is high enough that the amount of dissolved material is large enough to produce a large crystal or large crystal clusters, yet not so high that the solubility curve has a large slope and therefore requires a high degree of temperature control to avoid crystal nucleation in the solution. Use of the cell with a variety of chemical solutions, each having the same saturation temperature, facilitates optimization while maintaining a simple, low cost design.
摘要翻译：具有计算机化的温度控制和搅拌的晶体生长池意味着抑制晶体成核。半主动地控制温度，即通过用热敏电阻监测温度，并通过加热电阻或加热元件平衡环境热损失与加入系统的热量。当化学品通过将混合物加热至高于饱和温度的温度完全溶解时，温度降低。在饱和温度下，温度最初缓慢降低以避免晶体成核。初始溶液的饱和温度选择为足够高的中间温度，使得溶解的材料的量足够大以产生大的晶体或大的晶体簇，但不太高，使得溶解度曲线具有大的斜率因此需要高度的温度控制以避免溶液中的晶体成核。使用具有各种具有相同饱和温度的各种化学溶液的电池便于优化，同时保持简单，低成本的设计。

2. 发明申请

US20160160380A1 Method for crystal growth in a cell in direct thermal contact with the ambient environment 审中-公开
标题翻译：在与周围环境直接热接触的电池中晶体生长的方法
公开(公告)号：US20160160380A1
公开(公告)日：2016-06-09
申请号：US14545752
申请日：2015-06-15
申请人： Michael Krautter
发明人： Michael Krautter
IPC分类号： C30B7/08
CPC分类号： C30B7/08 , B01F13/0827 , B01F13/0872 , C30B29/14 , C30B35/00 , Y10T117/1008
摘要： A crystal growing cell which has computerized temperature control and agitation means to inhibit crystal nucleation. The temperature is controlled semi-actively, i.e., by monitoring the temperature with a thermistor and balancing ambient heat loss with heat added to the system by heating resistors or heating elements. When the chemical is completely dissolved by heating the mixture to a temperature above the saturation temperature, the temperature is lowered. At the saturation temperature the temperature is initially reduced slowly to avoid crystal nucleation. The saturation temperature of the initial solution is selected to be at an intermediate temperature which is high enough that the amount of dissolved material is large enough to produce a large crystal or large crystal clusters, yet not so high that the solubility curve has a large slope and therefore requires a high degree of temperature control to avoid crystal nucleation in the solution.
摘要翻译：具有计算机化的温度控制和搅拌的晶体生长池意味着抑制晶体成核。半主动地控制温度，即通过用热敏电阻监测温度，并通过加热电阻或加热元件平衡环境热损失与加入系统的热量。当化学品通过将混合物加热至高于饱和温度的温度完全溶解时，温度降低。在饱和温度下，温度最初缓慢降低以避免晶体成核。初始溶液的饱和温度选择为足够高的中间温度，使得溶解的材料的量足够大以产生大的晶体或大的晶体簇，但不太高，使得溶解度曲线具有大的斜率因此需要高度的温度控制以避免溶液中的晶体成核。

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