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71. 发明授权

US4740627A Synthesis of E,Z-11-tetradecen-1-al 失效
标题翻译： E，Z-11-十四碳烯-1-基的合成
公开(公告)号：US4740627A
公开(公告)日：1988-04-26
申请号：US53297
申请日：1987-05-21
申请人： Jim D. Byers , Charles A. Drake
发明人： Jim D. Byers , Charles A. Drake
IPC分类号： C07C45/29 , C07C45/30 , C07C47/21 , C07C41/06
CPC分类号： C07C47/21 , C07C45/29 , C07C45/292 , C07C45/305 , Y02P20/582
摘要： The present invention pertains to a process for making a E,Z-11-tetradecen-1-al containing from 80 to 83 mole percent of the E isomer and from 17 to 20 mole percent of the Z isomer which exhibits pheromone-like activity for the spruce bud worm (choristoneura fumiferana).
摘要翻译：本发明涉及一种制备含有80-83％（摩尔）E异构体的E，Z-11-十四碳烯-1-醇的方法，以及17-20％（摩尔）Z异构体，其表现出信息素样活性，云杉芽蠕虫（choristoneura fumiferana）。

72. 发明授权

US4607131A Isolation of 3-methyl-1-butene from a hydrocarbon stream 失效
标题翻译：从烃流中分离3-甲基-1-丁烯
公开(公告)号：US4607131A
公开(公告)日：1986-08-19
申请号：US696362
申请日：1985-01-31
申请人： Charles A. Drake
发明人： Charles A. Drake
IPC分类号： C07C7/171 , C07C7/17
CPC分类号： C07C7/171
摘要： A process for recovering 3-methyl-1-butene from a hydrocarbon stream by treating the stream with sulfuric acid to remove compounds which form azeotropes with 3-methyl-1-butene and separating the remaining stream.
摘要翻译：通过用硫酸处理物流以除去与3-甲基-1-丁烯形成共沸物并分离剩余物流的化合物，从烃流中回收3-甲基-1-丁烯的方法。

73. 发明授权

US4596783A Hydrogenation catalysts and selective hydrogenation therewith 失效
公开(公告)号：US4596783A
公开(公告)日：1986-06-24
申请号：US780749
申请日：1985-09-27
申请人： Charles A. Drake
发明人： Charles A. Drake
IPC分类号： B01J23/62 , B01J27/232 , B01J31/02 , B01J31/04 , C07C17/354
CPC分类号： B01J31/0244 , B01J23/628 , B01J31/04 , C07C17/354 , B01J2231/645 , B01J27/232
摘要： Selective hydrogenation process is provided employing as catalyst a composition consisting essentially of elemental palladium on calcium carbonate support with lead acetate and an aromatic amine oxide. Very high selectivities to cis-olefinic compounds from acetylenic compounds is achieved employing the catalyst of the invention.

74. 发明授权

US4587229A Catalyst for the production of allyl acetate 失效
标题翻译：用于生产乙酸烯丙酯的催化剂
公开(公告)号：US4587229A
公开(公告)日：1986-05-06
申请号：US663629
申请日：1984-10-22
申请人： Charles A. Drake , Stephen E. Reiter
发明人： Charles A. Drake , Stephen E. Reiter
IPC分类号： B01J23/644 , B01J23/58 , B01J21/08 , B01J23/64
CPC分类号： B01J23/6447 , C07C67/055
摘要： A process and catalyst for the acetoxylation of propylene, said catalyst consisting essentially of palladium, bismuth, and rubidium on a support.
摘要翻译：用于丙烯的乙酰氧基化的方法和催化剂，所述催化剂基本上由载体上的钯，铋和铷组成。

75. 发明授权

US4575575A Catalysts and process for olefin conversion 失效
标题翻译：催化剂和烯烃转化方法
公开(公告)号：US4575575A
公开(公告)日：1986-03-11
申请号：US596984
申请日：1984-04-05
申请人： Charles A. Drake , Robert E. Reusser
发明人： Charles A. Drake , Robert E. Reusser
IPC分类号： B01J23/30 , C07C6/04 , C07C6/06
CPC分类号： B01J23/30 , C07C6/04 , C07C6/06
摘要： A process for disproportionation of olefins is disclosed employing a novel catalyst comprising a silica support treated with an oxide or oxide precursor of tungsten and a Group I oxide or compound convertible to the oxide in admixture with a double bond isomerization catalyst.
摘要翻译：公开了一种用于歧化烯烃的方法，其使用包含由钨和氧化物氧化物前体处理的二氧化硅载体的新型催化剂，以及与双键异构化催化剂混合可转化为氧化物的第I族氧化物或化合物。

76. 发明授权

US4559111A Azeotropic purification of Z-11-hexadecenal 失效
标题翻译： Z-11-十六烯醛共沸净化
公开(公告)号：US4559111A
公开(公告)日：1985-12-17
申请号：US684208
申请日：1984-12-20
申请人： Charles A. Drake
发明人： Charles A. Drake
IPC分类号： B01D3/38 , C07C45/27 , C07C45/84 , B01D3/36 , C07C47/21
CPC分类号： C07C45/27 , B01D3/38 , C07C45/84
摘要： Production of essentially pure Z-11-hexadecenal by azeotropic distillation is described. Contacting a mixture of Z-11-hexadecenal, hexadecene and hexadecadiene with dimethylsulfoxide and subjecting the blend to azeotropic distillation allows for the removal of hydrocarbon impurities from the aldehyde. Contacting a mixture of Z-11-hexadecenal and hexadecenol with a C.sub.2 -C.sub.4 glycol and subjecting the blend to azeotropic distillation conditions allows for the recovery of a glycol-aldehyde azeotrope from which essentially pure aldehyde is readily recovered. A mixture comprising Z-11-hexadecenal, hexadecene, hexadecadiene and hexadecenol can be sequentially treated according to the above-described azeotropic distillation steps in order to provide essentially pure Z-11-hexadecenal.
摘要翻译：描述了通过共沸蒸馏生产基本上纯的Z-11-十六烯醛。将Z-11-十六碳烯，十六碳烯和十六碳二烯与二甲基亚砜的混合物接触并使共混物进行共沸蒸馏，可以从醛中除去烃类杂质。将Z-11-十六碳烯和十六碳烯醇的混合物与C 2 -C 4二元醇接触并使共混物共沸蒸馏条件允许回收二醇 - 醛共沸物，从其中容易回收基本上纯的醛。可以根据上述共沸蒸馏步骤依次处理包含Z-11-十六碳烯醛，十六碳烯，十六碳二烯和十六碳烯醇的混合物，以提供基本上纯的Z-11-十六烯醛。

77. 发明授权

US4490567A Catalyst and process for dehydrating 2-alcohols 失效
标题翻译：用于脱水2-醇的催化剂和方法
公开(公告)号：US4490567A
公开(公告)日：1984-12-25
申请号：US366513
申请日：1982-04-08
申请人： Charles A. Drake
发明人： Charles A. Drake
IPC分类号： B01J23/10 , B01J23/12 , C07C1/24 , C07C11/113 , C07C1/00
CPC分类号： C07C11/113 , B01J23/10 , B01J23/12 , C07C1/24 , C07C2521/04 , C07C2523/10 , C07C2523/12
摘要： Novel catalysts are disclosed for the selective dehydration of 2-alcohols to .alpha.-olefins. In one case, the catalyst comprises at least one catalytic metal oxide on a low surface area aluminum oxide-containing support. In another case, the catalyst comprises a mixture of thorium oxide and cerium oxide on a base treated aluminum oxide containing support. There is also disclosed a novel process for obtaining high purity 4-methyl-1-pentene involving the dehydration of 4-methyl-2-pentanol followed by disproportionation with ethylene.
摘要翻译：公开了用于将2-醇选择性脱水至α-烯烃的新型催化剂。在一种情况下，催化剂在低表面积的含氧化铝的载体上包含至少一种催化金属氧化物。在另一种情况下，催化剂包含氧化钍和二氧化铈的混合物在基底处理的含氧化铝载体上。还公开了一种获得高纯度4-甲基-1-戊烯的新方法，涉及4-甲基-2-戊醇的脱水，随后用乙烯进行歧化。

78. 发明授权

US4487970A Cleavage of hydroperoxides 失效
标题翻译：氢过氧化物的裂解
公开(公告)号：US4487970A
公开(公告)日：1984-12-11
申请号：US500679
申请日：1983-06-03
申请人： Charles A. Drake
发明人： Charles A. Drake
IPC分类号： B01J27/12 , C07C37/08 , C07C45/53 , C07C409/14
CPC分类号： C07C409/14 , B01J27/12 , C07C37/08 , C07C407/00 , C07C45/53 , C07C2101/16 , Y02P20/52
摘要： Secondary-alkyl substituted benzene hydroperoxides are cleaved to form phenols and ketones by contacting the secondary-alkyl substituted benzene hydroperoxide with a catalyst consisting essentially of about 3:1 to 1:10 by weight of SbF.sub.5 and graphite in the presence of an aromatic or ketone solvent at a temperature of from about 0.degree.-100.degree. C.
摘要翻译：通过使仲烷基取代的苯氢过氧化物与基本上由重量比约3:1到1:10的SbF5和石墨在芳族或酮的存在下接触而将仲烷基取代的苯氢过氧化物裂解形成酚和酮溶剂在约0℃-100℃

79. 发明授权

US4440950A Process for preparation of aminobenzaldehydes and aminobenzylketones 失效
标题翻译：氨基苯甲醛和氨基苄基酮的制备方法
公开(公告)号：US4440950A
公开(公告)日：1984-04-03
申请号：US441584
申请日：1982-11-15
申请人： Charles A. Drake
发明人： Charles A. Drake
IPC分类号： C07C85/18
CPC分类号： C07C221/00
摘要： An improved process for the formation of a dihydrocarbylaminobenzaldehyde or dihydrocarbylaminobenzylketone is provided consisting of (a) reacting a N,N-dihydrocarbylaniline and a protected Schiff's base in the presence of water, a carboxylic acid, and an ammonium salt of a carboxylic acid followed by (b) hydrolyzing the resulting reactant product of (a).
摘要翻译：提供了形成二烃基氨基苯甲醛或二烃基氨基苄基酮的改进方法，由（a）在水，羧酸和羧酸铵盐存在下使N，N-二烃基苯胺和受保护的席夫碱反应，然后（b）水解所得的（a）反应产物。

80. 发明授权

US4383940A Catalysts for hydrogenation of unsaturated dinitriles 失效
标题翻译：不饱和二腈的氢化催化剂
公开(公告)号：US4383940A
公开(公告)日：1983-05-17
申请号：US326108
申请日：1981-11-30
申请人： Timothy P. Murtha , Charles A. Drake
发明人： Timothy P. Murtha , Charles A. Drake
IPC分类号： B01J23/46 , B01J35/10 , C07C209/48 , B01J21/08
CPC分类号： C07C209/48 , B01J23/464 , B01J35/10 , B01J35/1019 , B01J35/1042 , B01J35/1061
摘要： Unsaturated dinitriles are hydrogenated to saturated diamines using a rhodium catalyst on a silica support having a surface area larger than 275 m.sup.2 /g, a pore volume of from about 1.0 to 1.5 mL/g and an average pore size of from about 100 to about 175 A. The supported rhodium catalyst is prepared by a method which includes the steps of contacting a silica support having the characteristics described above with a solution or dispersion of rhodium or a reducible compound of rhodium, and then subjecting the impregnated silica support to vacuum treatment.
摘要翻译：使用表面积大于275m 2 / g，孔体积为约1.0至1.5mL / g，平均孔径为约100至约175的二氧化硅载体上的铑催化剂将不饱和二腈氢化为饱和二胺 A.负载的铑催化剂通过包括以下步骤的方法制备：将具有上述特征的二氧化硅载体与铑或可还原的铑化合物的溶液或分散体接触，然后使浸渍的二氧化硅载体进行真空处理。

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