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61. 发明授权

US07846318B2 Polyaluminum chloride and aluminum chlorohydrate, processes and compositions: high-basicity and ultra high-basicity products 有权
标题翻译：聚氯化铝和氯化铝水合物，工艺和组成：高碱度和超高碱度的产品
公开(公告)号：US07846318B2
公开(公告)日：2010-12-07
申请号：US11619483
申请日：2007-01-03
申请人： William E. Pratt , Joseph J. Stevens , Peter G. Symons
发明人： William E. Pratt , Joseph J. Stevens , Peter G. Symons
IPC分类号： C25D5/34 , C25B1/24 , B01D61/00 , C01B17/45 , C01B17/46
CPC分类号： C01F7/56 , A61K8/26 , A61Q15/00 , B01D61/44 , C01B9/02 , C01G23/02 , C01G25/04 , C01G49/10
摘要： The invention relates generally to processes for the production of high-basicity and ultra-high basicity polyaluminum chlorides including aluminum chlorohydrate. The processes can produce products of a wide range of basicities and are particularly useful in producing high basicity products. The process can produce a wide range of solution concentrations and are particularly useful in producing high solution concentrations. The processes described generate high purity products, which are free of by-product salt(s). The processes described herein can also be utilized to produce enhanced efficacy polyaluminum chlorides including aluminum chlorohydrate. When compared to conventional processes for manufacturing these compounds the processes disclosed herein are unique in so far as the disclosed processes do not require aluminum metal as a starting material. The products of the processes are suitable in applications including water purification, catalysts, and antiperspirants. In addition, the invention is directed to the products prepared by the processes described herein.
摘要翻译：本发明一般涉及生产包括氯化铝水合物在内的高碱度和超高碱性聚氯化铝的方法。该工艺可生产各种碱性产品，特别适用于生产高碱度产品。该方法可产生大范围的溶液浓度，特别适用于生产高溶液浓度。所述方法产生不含副产物盐的高纯度产物。本文所述的方法也可用于产生包括氯化铝水合物的增强效力的聚氯化铝。与用于制造这些化合物的常规方法相比，本文公开的方法是独特的，只要所公开的方法不需要铝金属作为起始材料即可。该方法的产品适用于包括水净化，催化剂和止汗剂在内的应用。此外，本发明涉及通过本文所述方法制备的产品。

62. 发明申请

US20100061919A1 PRODUCTION OF POLYALUMINUM CHLORIDE FROM BASIC ALUMINUM CHLORIDE AND SODIUM ALUMINATE VIA ULTRASONIC PROCESSING 审中-公开
标题翻译：通过超声处理从碱性氯化铝和铝酸钠生产氯化铝
公开(公告)号：US20100061919A1
公开(公告)日：2010-03-11
申请号：US12207665
申请日：2008-09-10
申请人： LEVI JAMES GROVE , Kevin Edward Janak
发明人： LEVI JAMES GROVE , Kevin Edward Janak
IPC分类号： C01F7/56 , C01B17/45 , B01J19/10
CPC分类号： C01F7/56 , B01J19/10 , C01F7/002 , C01P2002/86
摘要： A method is provided for the production of a stable mid- and high-basicity polyaluminum chloride and polyaluminum chlorosulfate, respectively from sodium aluminate and aluminum chloride or low- or mid-basicity polyaluminum chloride by ultrasonic processing of the reactants. The method overcomes the formation of gels and insoluble precipitates that typically form when mixing sodium aluminate and aluminum chloride and the formation of sodium chloride, which is insoluble in high concentration polyaluminum chloride solutions. The invention eliminates the cumbersome extended heating periods previously required to deal with the formation of insoluble aluminum oxide precipitates in batches of polyaluminum chloride produced from sodium aluminate and aluminum chloride using high-shear mixing. Also because the use of ultrasonic processing reduces the amount of aluminum oxide generated, a batch heating cycle is avoided which reduces the energy costs associated with the production of polyaluminum chloride and thereby allows the process to be run as a continuous process rather than a batch process.
摘要翻译：提供了一种通过反应物的超声波处理分别从铝酸钠和氯化铝或低或中碱性聚氯化铝生产稳定的中，高碱性聚氯化铝和聚氯化铝的方法。该方法克服了当混合铝酸钠和氯化铝时形成的凝胶和不溶性沉淀物的形成以及不溶于高浓度聚氯化铝溶液的氯化钠的形成。本发明消除了以前需要的麻烦的延长的加热时间，以处理由铝酸钠和氯化铝制成的一批聚氯化铝中使用高剪切混合物形成不溶性氧化铝沉淀物。此外，由于使用超声波处理减少了生成的氧化铝的量，因此避免了批量加热循环，这降低了与聚氯化铝的生产相关的能量成本，从而允许该工艺作为连续工艺而不是间歇工艺运行。

63. 发明申请

US20070224109A1 Metal chlorides and metals obtained from metal oxide containing materials 有权
标题翻译：从含金属氧化物的材料中获得的金属氯化物和金属
公开(公告)号：US20070224109A1
公开(公告)日：2007-09-27
申请号：US11386852
申请日：2006-03-23
申请人： Richard Chaifetz , Gregory Matusewitch , Corey Morton , Jason Phillips
发明人： Richard Chaifetz , Gregory Matusewitch , Corey Morton , Jason Phillips
IPC分类号： C01B9/02 , B01J8/00
CPC分类号： C01B9/02 , B01J2219/00006 , C01F7/56 , C01G1/06 , C01G23/022 , C01G49/10 , C22B5/00 , C25C3/06
摘要： Method and apparatus for preparing at least one metal chloride from metal oxide containing material comprising calcining the metal oxide containing material under temperature conditions sufficient to obtain a calcined product comprising at least one metal oxide; and selectively chlorinating the calcined product to form at least one metal chloride.
摘要翻译：用于从含有金属氧化物的材料制备至少一种金属氯化物的方法和装置，包括在足以获得包含至少一种金属氧化物的煅烧产物的温度条件下煅烧含金属氧化物的材料; 并选择性地氯化煅烧产物以形成至少一种金属氯化物。

64. 发明授权

US07087220B2 High pH antiperspirant compositions of enhanced efficacy 失效
标题翻译：具有增强功效的高pH止汗组合物
公开(公告)号：US07087220B2
公开(公告)日：2006-08-08
申请号：US10857493
申请日：2004-05-28
申请人： Zijun Li
发明人： Zijun Li
IPC分类号： A61Q15/00 , A61Q19/00 , A61K8/00 , A61K8/02
CPC分类号： A61K8/28 , A61Q15/00 , C01F7/56 , C01P2002/87
摘要： Aluminum and aluminum-zirconium antiperspirant compositions of enhanced efficacy and a pH value of at least 3.5 are provided that are made by reaction with insoluble, strongly alkaline strontium or calcium salts. The aluminum and aluminum-zirconium strontium or calcium compositions show high pH values with characteristic HPLC Band III to Band II ratios of at least 0.5. The basic aluminum halohydrate (or nitrate) solutions typically have aluminum to anion ratio of less that 1.9. The solution compositions are stable with respect to both HPLC Band III to Band II ratio and viscosity at concentrations of about 20% to about 40% by weight of anhydrous solid. The solid state compositions form hard sticks with low irritation, at low metal to chloride ratios of about 0.9 to about 1.2.
摘要翻译：提供了增强效力和至少3.5的pH值的铝和铝 - 锆止汗组合物，其通过与不溶性强碱性锶或钙盐的反应制备。铝和铝 - 锆锶或钙组合物显示高pH值，具有至少0.5的特征HPLC带III至带II比率。碱性卤化铝铝（或硝酸盐）溶液的铝阴离子比例通常小于1.9。溶液组合物相对于HPLC Band III至Band II比率和在约20重量％至约40重量％的无水固体的浓度下的粘度是稳定的。固态组合物形成具有低刺激性的硬棒，低金属氯化物比为约0.9至约1.2。

65. 发明申请

US20030138389A1 Deodorants and antiperspirants 失效
标题翻译：除臭剂和止汗剂
公开(公告)号：US20030138389A1
公开(公告)日：2003-07-24
申请号：US10322959
申请日：2002-12-18
申请人： Clariant GmbH
发明人： Peter Klug , Norbert Roesch , Karl Werner Reiser
IPC分类号： A61K007/38
CPC分类号： C01F7/56 , A61K8/26 , A61Q15/00 , C01P2006/80
摘要： Deodorants and antiperspirants comprising aluminum chlorohydrates according to the formula I Al2(OH)nClznullnull(I)where n is a number between 4.5 and 5.1 and z is a number between 1.5 and 0.9 and nnullz is always 6, with an iron content of less than 20 ppm, preferably less than 10 ppm, based on the dry substance.
摘要翻译：除臭剂和止汗剂，其包含根据式I Al 2（OH）nClz（I）的氯化铝酸盐，其中n为4.5至5.1之间的数，z为1.5至0.9之间的数，并且n + z为6，并且铁含量为小于20ppm，优选小于10ppm。

66. 发明授权

US06241958B1 Process for preparing sulfate-containing basic solutions of polyaluminumchloride 失效
标题翻译：制备聚氯化铝的含硫酸盐碱性溶液的方法
公开(公告)号：US06241958B1
公开(公告)日：2001-06-05
申请号：US08107656
申请日：1993-08-12
申请人： Gerhard Haake , Gunter Geiler , Frank Haupt
发明人： Gerhard Haake , Gunter Geiler , Frank Haupt
IPC分类号： C01B1745
CPC分类号： C01F7/007 , C01F7/56 , C01P2004/61 , C02F1/5245
摘要： The process of preparing a solution of basic sulfate-containing polyaluminum chloride includes digesting an aluminum-containing substance with hydrochloric acid to form a resulting solution and an insoluble residue; filtering the resulting solution to separate the insoluble residue therefrom and to form a solids-free solution; concentrating the solids-free solution by evaporation to form a concentrated solution having an AlCl3 content of about 30 percent by weight; recovering AlCl3·6 H2O from the concentrated solution by crystallization; thermally decomposing the recovered AlCl3·6 H2O by heating at 150 to 200° C. so as to form a solid basic aluminum chloride containing Al and OH in a molar ratio of OH/Al of 1.35:1 to 2.25:1; dissolving the solid basic aluminum chloride in an aqueous sulfuric acid solution and heat-treating at 40 ° C. to 70 ° C. for 1 to 3 hours to form a solution of basic sulfate-containing polyaluminum chloride having a sulfate content of 1 to 6 percent by weight, an aluminum concentration of 3 to 10 percent by weight and a molar ratio of OH/Al in the solution of the basic sulfate-containing polyaluminum chloride from 1.05:1 to 1.95:1.
摘要翻译：制备含碱性硫酸盐的聚氯化铝溶液的方法包括用盐酸消化含铝物质以形成所得溶液和不溶残留物; 过滤所得溶液以从其中分离不溶性残余物并形成无固体的溶液; 通过蒸发浓缩无固体溶液以形成AlCl 3含量为约30重量％的浓缩溶液; 通过结晶从浓缩溶液中回收AlCl3.6H2O; 通过在150至200℃下加热热分解回收的AlCl 3·6H 2 O，以形成OH / Al摩尔比为1.35:1至2.25:1的Al和OH的固体碱性氯化铝; 将固体碱性氯化铝溶解在硫酸水溶液中，并在40℃至70℃下热处理1至3小时，以形成硫酸盐含量为1至6的含碱性硫酸盐的聚氯化铝溶液重量百分比，铝浓度为3〜10重量％，碱性硫酸盐聚合氯化铝溶液中OH / Al的摩尔比为1.05：1〜1.95：1。

67. 发明授权

US06217840B1 Production of fumed silica 失效
标题翻译：生产煅制二氧化硅
公开(公告)号：US06217840B1
公开(公告)日：2001-04-17
申请号：US09374546
申请日：1999-08-13
申请人： Robert J. Barnett , Michael B. Mezner
发明人： Robert J. Barnett , Michael B. Mezner
IPC分类号： C01B3312
CPC分类号： C01B7/191 , C01B7/193 , C01B33/18 , C01C1/244 , C01D5/00 , C01F7/141 , C01F7/26 , C01F7/50 , C01F7/56 , C01F11/24 , C01F11/46 , C03C1/002 , C04B7/24 , C04B18/0481 , C04B35/185 , C04B35/62204 , C22B21/0015 , C22B21/0046 , C22B21/0069 , Y02P10/234 , Y02P40/145 , Y02W30/91
摘要： A method for producing fumed silica and a fluorine-containing product from a source of silica in solid form and a solid material containing fluorine, the solid material selected from the group consisting of sodium aluminum tetrafluoride, cryolite, aluminum fluosilicate ammonium bifluoride, sodium aluminum silicofluoride, and sodium fluosilicate. The method comprises the steps of digesting the silica in solid form and the solid material selected from the group consisting of sodium aluminum tetrafluoride, cryolite, aluminum fluosilicate, ammonium bifluoride, sodium aluminum silicofluoride, and sodium flurosilicate in a sulfuric acid digester. The digestion step produces a first gas component comprised of silicon tetrafluoride, hydrogen fluoride and water vapor. The first gas component is removed from the digester. The gas component recovered from the digester is heated to a temperature sufficiently high to convert the silicon tetrafluoride to fumed silica in the presence of the hydrogen fluoride and the finned silica is separated from the hydrogen fluoride.
摘要翻译：从固体形式的二氧化硅源和含氟的固体材料制造热解法二氧化硅和含氟产物的方法，选自四氟化铝铝，冰晶石，氟硅酸铵二氟化铝，硅铝酸钠的固体材料，和氟硅酸钠。该方法包括以下步骤：在硫酸蒸煮器中消化固体形式的二氧化硅和选自四氟化铝铝，冰晶石，氟硅酸铝，氟化铵铵，氟硅酸钠，氟硅酸钠的固体物质。消化步骤产生由四氟化硅，氟化氢和水蒸气组成的第一气体组分。将第一气体成分从蒸煮器中取出。将从蒸煮器回收的气体组分加热到足够高的温度，以在氟化氢存在下将四氟化硅转化成热解法二氧化硅，并且将氟化铁与氟化氢分离。

68. 发明授权

US06217836B1 Recovering carbon, silica and alumina from spent potliner 失效
标题翻译：从废锅炉中回收碳，二氧化硅和氧化铝
公开(公告)号：US06217836B1
公开(公告)日：2001-04-17
申请号：US09201196
申请日：1998-11-30
申请人： Robert J. Barnett , Michael B. Mezner
发明人： Robert J. Barnett , Michael B. Mezner
IPC分类号： C01F700
CPC分类号： C01B7/191 , C01C1/244 , C01F5/22 , C01F7/141 , C01F7/50 , C01F7/56 , C01F11/24 , C01F11/46 , C03C1/002 , C04B7/24 , C04B18/0481 , C04B33/1324 , C04B33/1325 , C04B33/138 , C04B35/185 , C04B35/62204 , C04B2235/3217 , C04B2235/402 , C04B2235/445 , C04B2235/448 , C22B21/0046 , C22B21/0069 , Y02P10/212 , Y02P20/129 , Y02P40/145 , Y02P40/69 , Y02W30/91 , C04B20/023
摘要： Spent potliner from aluminum reduction cells is treated, for example, with sulfuric acid to recover carbon, silica and alumina or to recover a vitrified product of silca and alumina.
摘要翻译：例如用硫酸处理来自铝还原电池的废料浆，以回收碳，二氧化硅和氧化铝，或回收硅藻和氧化铝的玻璃化产物。

69. 发明授权

US06187275B1 Recovery of AlF3 from spent potliner 失效
标题翻译：从废锅炉中回收AlF3
公开(公告)号：US06187275B1
公开(公告)日：2001-02-13
申请号：US09201197
申请日：1998-11-30
申请人： Robert J. Barnett , Michael B. Mezner
发明人： Robert J. Barnett , Michael B. Mezner
IPC分类号： C01F700
CPC分类号： C01B7/191 , C01C1/244 , C01F5/22 , C01F7/141 , C01F7/50 , C01F7/56 , C01F11/24 , C01F11/46 , C03C1/002 , C04B7/24 , C04B18/0481 , C04B33/1324 , C04B33/1325 , C04B33/138 , C04B35/185 , C04B35/62204 , C04B2235/3217 , C04B2235/402 , C04B2235/445 , C04B2235/448 , C22B21/0046 , C22B21/0069 , Y02P10/212 , Y02P20/129 , Y02P40/145 , Y02P40/69 , Y02W30/91 , C04B20/023
摘要： A method of recovering AlF3 from spent potliner using an acid digest to form gaseous HF which is converted to hydrofluoric acid and reacted with alumina trihydrate to form AlF3.
摘要翻译：使用酸消化法从废釜中回收AlF 3以形成气态HF的方法，其转化为氢氟酸并与三水合氧化铝反应以形成AlF 3。

70. 发明授权

US6123908A Method of treating spent potliner material from aluminum reduction cells 失效
标题翻译：从铝还原电池处理废瓷砖材料的方法
公开(公告)号：US6123908A
公开(公告)日：2000-09-26
申请号：US277804
申请日：1999-03-27
申请人： Robert J. Barnett , Michael B. Mezner
发明人： Robert J. Barnett , Michael B. Mezner
IPC分类号： C01B7/19 , C01C1/244 , C01F5/22 , C01F7/14 , C01F7/50 , C01F7/56 , C01F11/24 , C01F11/46 , C03C1/00 , C04B7/24 , C04B18/04 , C04B35/185 , C04B35/622 , C22B21/00 , C01C3/00 , C22B23/00 , C22B26/20
CPC分类号： C01C1/244 , C01B7/191 , C01F11/24 , C01F11/46 , C01F5/22 , C01F7/141 , C01F7/50 , C01F7/56 , C03C1/002 , C04B18/0481 , C04B33/1324 , C04B33/1325 , C04B35/185 , C04B35/62204 , C04B7/24 , C22B21/0046 , C22B21/0069 , Y02P10/212 , Y02P40/145 , Y02P40/69 , Y02W30/91
摘要： A process of treating spent potliner material from aluminum reduction cells and recovering useful products. In the process of the present invention, spent potliner material is introduced into an acid digester containing, for example, sulfuric acid. As a result of this step, a gas component is produced which includes hydrogen fluoride, silicon tetrafluoride and hydrogen cyanide. Also, a slurry component is produced which includes carbon, a refractory material including silica, alumina, sodium compounds such as sodium sulfate, aluminum compounds such as aluminum sulfate, iron compounds such as iron sulfate, magnesium and calcium compounds such as magnesium and calcium sulfate. The slurry component remains in the digester after the gas component is removed. The gas component is recovered and heated an effective amount to convert or decompose the silicon tetrafluoride to fumed silica, hydrogen cyanide to a remaining gas component including CO.sub.2, H.sub.2 O, and nitrogen oxides, as well as HF gas. The remaining gas component is directed through a water scrubber in which the HF gas is converted to liquid hydrofluoric acid. The hydrofluoric acid is then admixed with alumina trihydrate to form aluminum fluoride (a commercially useful end product) and water.
摘要翻译：一种从铝还原细胞处理废瓷砖材料并回收有用产品的方法。在本发明的方法中，将废瓷砖材料引入含有例如硫酸的酸性消化器中。作为该步骤的结果，产生包括氟化氢，四氟化硅和氰化氢的气体组分。另外，还制造了包含碳，耐火材料，包括二氧化硅，氧化铝，钠化合物如硫酸钠，铝化合物如硫酸铝，铁化合物如硫酸铁，镁和钙化合物如镁和硫酸钙的浆料组分。在除去气体成分后，浆料成分保留在蒸煮器中。回收气体组分并加热有效量，以将四氟化硅转化或分解成热解法二氧化硅，氰化氢转化为包括CO 2，H 2 O和氮氧化物的剩余气体组分以及HF气体。剩余的气体组分被引导通过水洗涤器，其中HF气体转化为液体氢氟酸。然后将氢氟酸与三水合氧化铝混合以形成氟化铝（商业上有用的最终产物）和水。

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