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1. 发明申请

US20180244836A1 INITIATORS AND USE THEREOF FOR CATIONIC PHOTOPOLYMERIZATION 审中-公开
公开(公告)号：US20180244836A1
公开(公告)日：2018-08-30
申请号：US15757008
申请日：2016-09-02
申请人： Technische Universitaet Wien , Albert-Ludwigs-Universitaet Freiburg , Polymer Competence Center Leoben GmbH
发明人： Robert LISKA , Daniel BOMZE , Ingo KROSSING , Patrick KNAACK
IPC分类号： C08G59/68 , C08G65/10 , C01F7/50 , C01F7/02
CPC分类号： C08G59/682 , C01F7/02 , C01F7/50 , C08G59/68 , C08G59/687 , C08G65/105
摘要： The invention relates to the use of aryliodonium and/or arylsulfonium salts of the tetrakis(perfluoro-t-butyloxy)aluminate anion of the following formula (I): as cationic initiators cleavable by light and/or free radicals for polymerizing cationically polymerizable monomers.

2. 发明申请

US20150166352A1 PROCESSES FOR THE RECOVERY OF FLUORIDE AND SILICA PRODUCTS AND PHOSPHORIC ACID FROM WET-PROCESS PHOSPHORIC ACID FACILITIES AND CONTAMINATED WASTE WATERS 有权
标题翻译：从湿法处理的磷酸设备和污染的废水中回收氟化物和二氧化硅产品和磷酸的方法
公开(公告)号：US20150166352A1
公开(公告)日：2015-06-18
申请号：US14416261
申请日：2013-07-21
申请人： K-TECHNOLOGIES, INC.
发明人： William W. Berry , Thomas E. Baroody
IPC分类号： C01B33/10 , C05B7/00 , C02F1/42 , C01B25/222
CPC分类号： C01B33/103 , B01J41/05 , B01J41/14 , B01J49/57 , C01B25/222 , C01B33/10 , C01C1/162 , C01F7/50 , C02F1/42 , C02F2001/422 , C02F2101/105 , C02F2101/14 , C02F2103/10 , C02F2103/34 , C02F2303/16 , C05B7/00
摘要： In particular, in alternative embodiments, the invention provides for a method to recover silicofluoride and phosphate species from wastewaters, or barometric condenser waters, that are typically utilized in wet-process phosphoric acid facilities. The species are recovered via a continuous ion exchange approach that allows for economic recovery of the materials and especially with the silicofluoride component allows for the production of valuable industrial materials such as hydrofluoric acid and other fluoride salts as well as industrial-grade precipitated silica materials. Return of the treated waste water to the phos-acid plant allows for optimization of reagent usage.
摘要翻译：特别地，在替代实施例中，本发明提供了一种通常用于湿法磷酸设备的废水或大气冷凝器水回收氟化硅和磷酸盐物质的方法。该物质通过连续离子交换方法回收，其允许材料的经济回收，特别是与氟硅化合物组分允许生产有价值的工业材料如氢氟酸和其它氟化物盐以及工业级沉淀二氧化硅材料。将经处理的废水返回到磷酸装置允许优化试剂用量。

3. 发明授权

US08388925B2 Methods for producing aluminum trifluoride 有权
标题翻译：生产三氟化铝的方法
公开(公告)号：US08388925B2
公开(公告)日：2013-03-05
申请号：US12969058
申请日：2010-12-15
申请人： Puneet Gupta , Satish Bhusarapu
发明人： Puneet Gupta , Satish Bhusarapu
IPC分类号： C01F7/50
CPC分类号： C01F7/50 , C01B33/10705
摘要： Methods for producing aluminum trifluoride by acid digestion of fluoride salts of alkali metal or alkaline earth metal and aluminum, optionally, in the presence of a source of silicon; methods for producing silane that include acid digestion of by-products of silane production to produce aluminum trifluoride.
摘要翻译：通过酸性消除碱金属或碱土金属和铝的氟化物盐，任选地在硅源存在下生产三氟化铝的方法; 制造硅烷的方法，其包括硅烷生产副产物的酸消化以产生三氟化铝。

4. 发明授权

US5723097A Method of treating spent potliner material from aluminum reduction cells 失效
标题翻译：从铝还原电池处理废瓷砖材料的方法
公开(公告)号：US5723097A
公开(公告)日：1998-03-03
申请号：US569271
申请日：1995-12-08
申请人： Robert J. Barnett , Michael B. Mezner
发明人： Robert J. Barnett , Michael B. Mezner
IPC分类号： C01B7/19 , C01C1/244 , C01F7/14 , C01F7/50 , C01F7/56 , C01F11/24 , C01F11/46 , C03C1/00 , C04B7/24 , C04B35/185 , C04B35/622 , C22B21/00 , C01F7/04 , C01B7/22
CPC分类号： C04B33/1324 , C01B7/191 , C01C1/244 , C01F11/24 , C01F11/46 , C01F7/141 , C01F7/50 , C01F7/56 , C03C1/002 , C04B33/138 , C04B35/185 , C04B35/62204 , C04B7/24 , C22B21/0046 , C22B21/0069 , C04B2235/3217 , C04B2235/445 , C04B2235/448 , Y02P40/145 , Y02P40/69
摘要： A method of treating spent potliner material from aluminum reduction cells is disclosed. The spent potliner material is introduced into a sulfuric acid digester to produce a gas component including hydrogen fluoride and hydrogen cyanide and a slurry component including carbon, silica, alumina, sodium sulfate, iron, calcium and magnesium. The gas component is recovered and heated an effective amount to eliminate hydrogen cyanide and produce a remaining gas component including CO.sub.2, H.sub.2 O, nitrogen oxides and HF. The remaining gas component is directed through a water scrubber to form hydrofluoric acid, and the hydrofluoric acid is admixed with aluminum hydroxide to create aluminum fluoride. The slurry component is rinsed with water to separate a first solid fraction containing carbon, alumina and silica from a second liquid faction. The pH of the liquid fraction is adjusted to first create and separate aluminum hydroxide and then to separate sodium sulfate. Finally, the solid fraction is admixed with an alumina/silica mix and then subjected to an elevated temperature in an oxygen-rich atmosphere to oxidize the carbon and vitrify the alumina and silica into refractory material.
摘要翻译：公开了一种从铝还原电池处理废钽材料的方法。将废弃的老化剂材料引入硫酸消化器中以产生包括氟化氢和氰化氢的气体组分和包括碳，二氧化硅，氧化铝，硫酸钠，铁，钙和镁的淤浆组分。回收气体组分并加热有效量以除去氰化氢并产生包括CO 2，H 2 O，氮氧化物和HF的剩余气体组分。剩余的气体组分被引导通过水洗涤器以形成氢氟酸，并将氢氟酸与氢氧化铝混合以产生氟化铝。用水冲洗浆料组分以从第二液体分离含有碳，氧化铝和二氧化硅的第一固体部分。调节液体部分的pH以首先产生和分离氢氧化铝，然后分离硫酸钠。最后，将固体部分与氧化铝/二氧化硅混合物混合，然后在富氧气氛中升高温度以氧化碳，并将氧化铝和二氧化硅玻璃化成耐火材料。

5. 发明授权

US5558847A Process for recovering aluminium and fluorine from fluorine containing waste materials 失效
标题翻译：从含氟废料中回收铝和氟的工艺
公开(公告)号：US5558847A
公开(公告)日：1996-09-24
申请号：US435279
申请日：1995-05-05
申请人： Henning Kaaber , Mogens Mollgaard
发明人： Henning Kaaber , Mogens Mollgaard
IPC分类号： C01F7/30 , C01F7/50 , C01F7/00
CPC分类号： C01F7/30 , C01F7/50
摘要： Aluminum and fluorine are recovered from fluorine containing waste materials from the production of aluminum metal (FCWM) as ALF.sub.2 OH hydrate by a process comprising: leaching FCWM with dilute sulphuric acid at a pH value within the range of 0-3; if needed adding aluminum in an acid soluble form; adjusting the pH value of the aqueous phase to a value within the range 3.7-4.1 at the end of the leaching period by addition of a caustic aqueous solution; precipitating silica at a temperature not exceeding 60.degree. C.; separating the reaction mixture into a solid phase containing precipitated silica and non-soluble residues of the FCWM and a purified solution; and precipitating AlF.sub.2 OH hydrate from the purified solution at a temperature within the range 90.degree.-100.degree. C. and at a pH value not exceeding about 4.1 by controlled continuous addition of an aqueous caustic solution. Reducing and/or non-oxidizing operating conditions are maintained during all these process steps. The precipitated AlF.sub.2 OH may be calcined at a temperature within the range 500.degree.-600.degree. C to produce AlF.sub.3, Al.sub.2 O.sub.3, which is expedient for use in processes for the production of aluminum metal by electrolytic production of alumina.
摘要翻译：通过包括以下步骤的方法从生产铝金属（FCWM）作为ALF2OH水合物从含氟废料中回收铝和氟，所述方法包括：在pH值为0-3的范围内用稀硫酸浸出FCWM; 如果需要加入酸溶性形式的铝; 通过加入苛性水溶液将水相的pH值在浸出期结束时调节至3.7-4.1范围内的值; 在不超过60℃的温度下沉淀二氧化硅; 将反应混合物分离成含有沉淀二氧化硅和FCWM的不溶性残留物的固相和纯化溶液; 并通过控制连续加入苛性碱水溶液，在90℃-100℃的温度和不超过约4.1的pH下从纯化溶液中沉淀出AlF2OH水合物。在所有这些处理步骤期间，维持还原和/或非氧化操作条件。沉淀的AlF 2 OH可以在500-600℃范围内的温度下煅烧，以生产AlF 3，Al 2 O 3，这有利于通过电解生产氧化铝生产铝金属的方法。

6. 发明授权

US5242670A Method for hydrofluoric acid digestion of silica/alumina matrix material for the production of silicon tetrafluoride, aluminum fluoride and other residual metal fluorides and oxides 失效
标题翻译：用于生产四氟化硅，氟化铝和其他残留金属氟化物和氧化物的二氧化硅/氧化铝基体材料的氢氟酸消解方法
公开(公告)号：US5242670A
公开(公告)日：1993-09-07
申请号：US907854
申请日：1992-07-02
申请人： Ronald C. Gehringer
发明人： Ronald C. Gehringer
IPC分类号： C01B9/08 , C01B33/107 , C01D3/02 , C01F7/50
CPC分类号： C01B9/08 , C01B33/10705 , C01F7/50
摘要： A process for hydrofluoric acid digestion of inorganic silica/alumina matrix material for the production of silicon tetrafluoride and aluminum fluoride comprises the initial step of reacting the matrix material with hydrofluoric acid, to form silicon tetrafluoride gas and a solution/slurry containing aluminum fluoride, undigested oxides, and additional soluble and insoluble fluoride materials. The silicon tetrafluoride gas is purified of contaminants by condensing out impurities in cold traps and reacted with aqueous sodium fluoride to form a solution/slurry of fluorosilicate salt which is delivered to a filter press to separate sodium fluorosilicate powder from the solution/slurry. The sodium fluorosilicate powder is dried and delivered to a kiln at a temperature of about 600.degree. C. to 650.degree. C. to form substantially pure silicon tetrafluoride gas and sodium fluoride powder for collection. Recovery of aluminum fluoride is obtained by washing the solution/slurry containing aluminum fluoride, undigested oxides and additional soluble and insoluble fluoride materials with water to completely dissolve all water soluble materials; separating all undissolved materials by a filter press and drying the remaining solution containing aluminum fluoride and other water soluble fluorides in an evaporator while condensing water and excess hydrofluoric acid vapors in a condenser; recovering the aluminum fluoride or heavy metal fluorides from the dried solution and/or collecting high purity hydrofluoric acid from the liquid condensate by fractional distillation.
摘要翻译：用于生产四氟化硅和氟化铝的无机二氧化硅/氧化铝基质材料的氢氟酸消解方法包括使基质材料与氢氟酸反应的初始步骤，以形成四氟化硅气体和含氟化铝的溶液/浆液，未消化氧化物和其他可溶和不溶性氟化物材料。通过将冷阱中的杂质冷凝并与氟化钠水溶液反应形成氟硅酸盐的溶液/浆液，将四氟化硅气体纯化，将其输送到压滤机中以从溶液/浆液中分离氟硅酸盐粉末。将氟硅酸钠粉末干燥并在约600℃至650℃的温度下输送到窑中，以形成基本上纯的四氟化硅气体和用于收集的氟化钠粉末。通过用水洗涤含有氟化铝，未消化的氧化物和其他可溶性和不溶性氟化物材料的溶液/浆料，以完全溶解所有的水溶性物质，获得氟化铝。通过压滤机分离所有未溶解的材料并在蒸发器中干燥含有氟化铝和其它水溶性氟化物的剩余溶液，同时冷凝冷凝器中的水和过量氢氟酸蒸气; 从干燥溶液中回收氟化铝或重金属氟化物，和/或通过分馏从液体冷凝物中收集高纯度氢氟酸。

7. 发明授权

US5236690A Process for chemical vapor purification of group IIIA metal fluorides 失效
标题翻译： IIIA族金属氟化物的化学气相纯化工艺
公开(公告)号：US5236690A
公开(公告)日：1993-08-17
申请号：US648678
申请日：1991-01-31
申请人： Robert C. Folweiler , Barry C. Farnsworth
发明人： Robert C. Folweiler , Barry C. Farnsworth
IPC分类号： C01B9/08 , C01F7/50 , C01G15/00
CPC分类号： C01B9/08 , C01F7/50 , C01G15/00 , Y10S423/12
摘要： A chemical vapor purification process for preparing metal fluorides. The process involves melting a metal selected from the metals forming fluorides suitable for use in fluoride glass and thermodynamically partitionable from cation contaminants, for example aluminum, gallium, or indium. Chlorine, bromine, or iodine is bubbled through a stoichiometric excess of the melt, under reaction conditions selected to result in generation of a gaseous halide of the metal. The gaseous halide is then isolated from the melt and reacted with a gaseous fluorinating agent to form a solid fluoride of the metal.
摘要翻译：一种用于制备金属氟化物的化学气相纯化方法。该方法涉及熔化选自形成适用于氟化物玻璃的氟化物的金属中的金属，并且可以从热阳离子污染物（例如铝，镓或铟）热分解。在选择的反应条件下，氯，溴或碘鼓泡通过化学计量过量的熔体，以产生金属的气态卤化物。然后将气态卤化物与熔体分离，并与气态氟化剂反应形成金属的固体氟化物。

8. 发明授权

US5118887A Process for isomerization of hydrochlorofluorocarbons 失效
标题翻译：氢氯氟烃异构化方法
公开(公告)号：US5118887A
公开(公告)日：1992-06-02
申请号：US676279
申请日：1991-03-28
申请人： Susumu Okazaki , Masatsune Ogura , Yasunobu Mochizuki
发明人： Susumu Okazaki , Masatsune Ogura , Yasunobu Mochizuki
IPC分类号： B01J27/12 , B01J27/125 , C01F7/50 , C07B61/00 , C07C17/00 , C07C17/358 , C07C19/08 , C07C19/10 , C07C19/12
CPC分类号： C01F7/50 , B01J27/12 , B01J27/125 , C07C17/358
摘要： A partially fluorinated alumina catalyst having a determined component, which is obtained by calcining an Al.sub.2 O.sub.3.nH.sub.2 O(n=0 to 3) containing fibril of polytetrafluoroethylene, provides an excellent catalyst for the isomerization of HCFCs.

9. 发明授权

US4983373A Process for the production of high purity zirconium tetrafluoride and other fluorides 失效
标题翻译：用于生产高纯度四氟化锆和其他氟化物的方法
公开(公告)号：US4983373A
公开(公告)日：1991-01-08
申请号：US276271
申请日：1988-11-23
申请人： Howard P. Withers, Jr. , Andrew J. Woytek , John T. Lileck
发明人： Howard P. Withers, Jr. , Andrew J. Woytek , John T. Lileck
IPC分类号： C01G1/06 , C01B9/08 , C01F7/50 , C01G25/04 , C01G27/04
CPC分类号： C01F7/50 , C01B9/08 , C01G25/04 , C01G27/04
摘要： High purity metal fluorides (ZrF.sub.4, HfF.sub.4, AlF.sub.3) are produced by incomplete reaction of metal or their compounds with elemental fluorine and subsequent elevated temperature sublimation of the metal fluoride from the reaction products wherein unreacted metal or metal compounds act as "getters" to convert volatile impurity metal fluorides to non-volatile metals or metal compounds.

10. 发明授权

US4857294A Process for the preparation of metal fluorides usable for the production of fluoride glasses 失效
标题翻译：用于制备可用于生产氟化物玻璃的金属氟化物的方法
公开(公告)号：US4857294A
公开(公告)日：1989-08-15
申请号：US76309
申请日：1987-07-22
申请人： Martine Bridenne Alaux , Hubert Marquet-Ellis , Nelly Keller , Gerard Folcher, deceased
发明人： Martine Bridenne Alaux , Hubert Marquet-Ellis , Nelly Keller , Gerard Folcher, deceased
IPC分类号： B01J4/00 , B01J12/02 , C01B9/08 , C01F7/50 , C01G25/04 , C03C3/32
CPC分类号： C03C3/325 , B01J12/02 , B01J4/00 , C01B9/08 , C01F7/50 , C01G25/04
摘要： A process for the preparation of metal fluorides usable for the production of fluoride glasses consists of reacting in an organic liquid medium, such as toluene, (a) a compound of said metal chosen from among the gaseous compounds thereof, the compounds of said metal soluble in the organic liquid medium and the compounds of said metal in solution in an organic solvent miscible with said medium, and (b) a fluorinating agent chosen from among the gaseous fluorinating agents, the fluorinating agents which are partly soluble in the organic medium and the fluorinating agents which are partly soluble in an organic solvent miscible with said medium, to form a fluoride of said metal, the organic liquid medium being such that it reacts neither with the compound of the metal, nor with the fluorinating agent and does not dissolve the fluoride formed. To prepare the zirconium tetrafluoride, it is possible to introduce in toluene, gaseous Zr(BH.sub.4).sub.4 entrained by argon from the container and HF vapor also entrained by the argon from the other container. ZrF.sub.4 precipitates in the toluene and is separated on the filter.
摘要翻译：用于制备可用于生产氟化物玻璃的金属氟化物的方法包括在有机液体介质如甲苯中反应，（a）选自其气态化合物的所述金属的化合物，所述金属可溶的化合物在有机液体介质中和所述金属在溶液中与可与所述介质混溶的有机溶剂中的化合物，和（b）选自气态氟化剂的氟化剂，部分可溶于有机介质的氟化剂和部分可溶于与所述介质混溶的有机溶剂的氟化剂，形成所述金属的氟化物，所述有机液体介质既不与金属化合物也不与氟化剂反应，并且不溶解氟化物形成。为了制备四氟化锆，可以在甲苯中引入来自容器的氩气夹带的气态Zr（BH4）4和也被来自另一个容器的氩气的HF蒸气。 ZrF 4在甲苯中沉淀并在过滤器上分离。

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