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61. 发明授权

US09444092B2 Potato-shaped graphite particles with low impurity rate at the surface, method for preparing the same 有权
标题翻译：表面杂质比低的马铃薯状石墨颗粒，其制备方法
公开(公告)号：US09444092B2
公开(公告)日：2016-09-13
申请号：US12572510
申请日：2009-10-02
申请人： Abdelbast Guerfi , Fernand Brochu , Kimio Kinoshita , Karim Zaghib
发明人： Abdelbast Guerfi , Fernand Brochu , Kimio Kinoshita , Karim Zaghib
IPC分类号： H01M4/133 , C01B31/04 , G01N27/407 , H01M2/02 , H01M4/04 , H01M4/583 , H01M10/0525 , H01M4/1393 , B01J20/32 , H01M4/96 , H01M4/02 , H01M4/86
CPC分类号： H01M4/133 , B01J20/3204 , B01J20/3236 , B01J20/3293 , C01B32/20 , C01P2002/72 , C01P2004/51 , C01P2004/61 , C01P2006/11 , C01P2006/12 , C01P2006/80 , G01N27/4075 , H01M2/0222 , H01M4/02 , H01M4/0402 , H01M4/0404 , H01M4/0409 , H01M4/1393 , H01M4/583 , H01M4/587 , H01M4/622 , H01M4/623 , H01M4/96 , H01M8/0234 , H01M10/052 , H01M10/0525 , H01M2004/021 , H01M2004/027 , H01M2004/8684 , Y02P70/56 , Y10T428/2918 , Y10T428/2967 , Y10T428/2991
摘要： Modified graphite particles obtained from graphite or based on graphite, the said particles having impurities in their internal structure and having on the surface a low, even nil, rate of an impurity or several impurities. In addition, these particles have at least one of the following characteristics: a tab density between 0.3 and 1.5 g/cc; a potatolike shape; and a granulometric dispersion such that the D90/D10 ratio varies between 2 and 5 and the particles have a size between 1 and 50 μm. These particles can be used for fuel cells, electrochemical generators, or as moisture absorbers and/or oxygen absorbers and they have important electrochemical properties. The electrochemical cells and batteries thus obtained are stable and safe.
摘要翻译：这些颗粒可用于燃料电池，电化学发生器，或作为吸湿剂和/或氧吸收剂，它们具有重要的电化学性能。由此获得的电化学电池和电池是稳定和安全的。

62. 发明申请

US20160185600A1 CARBON MATERIAL, MATERIAL FOR A BATTERY ELECTRODE, AND BATTERY 审中-公开
标题翻译：碳材料，电池电极材料和电池
公开(公告)号：US20160185600A1
公开(公告)日：2016-06-30
申请号：US14908281
申请日：2014-07-28
申请人： SHOWA DENKO K.K.
发明人： Chiaki SOTOWA , Takashi TERASHIMA , Yasuaki WAKIZAKA
IPC分类号： C01B31/02 , H01M4/587 , C01B31/04 , H01M4/1393
CPC分类号： C01B32/05 , C01B32/20 , C01P2002/78 , C01P2002/82 , H01M4/587 , H01M2004/021
摘要： The present invention provides a carbon material and a material for a battery electrode which is suitable for use as an electrode material for an aqueous-electrolyte secondary battery, which material comprises optical structures having a specific shape, and in which material the ratio IG/ID (R value) between the peak intensity (ID) of a peak in a range of 1300 to 1400 cm−1 and the peak intensity (IG) of a peak in a range of 1580 to 1620 cm−1 measured by Raman spectroscopy spectra when particles of the carbon material are measured with Raman microspectrometer is 0.38 or more and 1.2 or less and the average interplanar spacing d002 of plane (002) by the X-ray diffraction method is 0.335 nm or more and 0.338 nm or less; and a secondary battery excellent in charge/discharge cycle characteristics and large current load characteristics.
摘要翻译：本发明提供一种碳材料和电池电极用材料，其适用于水电解质二次电池的电极材料，该材料包括具有特定形状的光学结构，其中材料的比例为IG / ID 在1300〜1400cm -1范围内的峰的峰强度（ID）与通过拉曼光谱测定的1580〜1620cm -1范围的峰的峰强度（IG）之间的差（R值）使用拉曼显微光谱仪测定碳材料的粒子为0.38以上且1.2以下，通过X射线衍射法得到的平面（002）的平均晶面间距d002为0.335nm以上且0.338nm以下，以及充电/放电循环特性和大电流负载特性优异的二次电池。

63. 发明申请

US20160122188A1 AA' STACKED GRAPHITE 有权
标题翻译： AA'堆积石墨
公开(公告)号：US20160122188A1
公开(公告)日：2016-05-05
申请号：US14932804
申请日：2015-11-04
申请人： Korea Institute of Science and Technology
发明人： Jae-Kap LEE , So-Hyung LEE , Jae-Pyoung AHN , Seung-cheol LEE , Wook-Seong LEE
IPC分类号： C01B31/04
CPC分类号： C01B32/20 , C01B2204/04 , C01P2002/78 , C23C16/26 , Y10T428/13 , Y10T428/261 , Y10T428/298 , Y10T428/2982
摘要： Disclosed is AA′ graphite with a new stacking feature of graphene, and a fabrication method thereof. Graphene is stacked in the sequence of AA′ where alternate graphene layers exhibiting the AA′ stacking are translated by a half hexagon (1.23 Å). AA′ graphite has an interplanar spacing of about 3.44 Å larger than that of the conventional AB stacked graphite (3.35 Å) that has been known as the only crystal of pure graphite. This may allow the AA′ stacked graphite to have unique physical and chemical characteristics.
摘要翻译：公开了具有石墨烯的新堆叠特征的AA'石墨及其制造方法。石墨烯以AA'的顺序堆叠，其中呈现AA'层叠的交替石墨烯层被半六边形（1.23）平移。 AA'石墨具有比已知为纯石墨的唯一晶体的常规AB堆叠石墨（3.35埃）的面间距大约3.44埃。这可能使AA的堆积石墨具有独特的物理和化学特性。

64. 发明申请

US20160115032A1 GRAPHENE WITH VERY HIGH CHARGE CARRIER MOBILITY AND PREPARATION THEREOF 审中-公开
标题翻译：石墨具有非常高的承载力移动性和准备
公开(公告)号：US20160115032A1
公开(公告)日：2016-04-28
申请号：US14889786
申请日：2014-05-07
申请人： Max-Planck-Gesellschaft zur Förderung der Wissenschaften e.V.
发明人： Alec WODTKE , Hak Ki YUK
IPC分类号： C01B31/04 , C25D3/38 , C30B25/18 , C30B29/02 , C09K5/14 , B01J21/18
CPC分类号： C01B31/0461 , B01J21/18 , C01B32/186 , C01B32/188 , C01B32/20 , C09K5/14 , C25D3/38 , C30B25/18 , C30B25/186 , C30B29/02
摘要： The present invention relates to a graphene film, which is obtainable by a method comprising the steps of: a) providing a substrate, b) epitaxially growing a metal layer on a surface of the substrate, c) optionally increasing the thickness of the metal layer obtained in step b) by growing a metal onto the epitaxially grown metal layer, d) peeling off the metal layer obtained in step b) or optionally in step c) from the substrate and e) depositing graphene onto at least a part of that surface of the metal layer obtained in step d), which was in contact with the substrate before the peeling off conducted in step d). Such a graphene film has a very high charge carrier mobility, namely, when measured on a SiO2 substrate, of more than 1 1000 cm2/V-sec, of at least 15000 cm2/V-sec, of at least 20000 cm2/V-sec, of at least 25000 cm2/V-sec or even of at least 30000 cm2/V-sec.
摘要翻译：本发明涉及一种石墨烯薄膜，其可通过包括以下步骤的方法获得：a）提供基材，b）在所述基材的表面上外延生长金属层，c）任选地增加所述金属层的厚度通过在外延生长的金属层上生长金属获得步骤b）中获得的步骤b），d）从基板剥离步骤b）或任选地在步骤c）中获得的金属层，以及e）在该表面的至少一部分上沉积石墨烯的步骤d）中获得的金属层，其在步骤d）中进行剥离之前与基板接触。这样的石墨烯薄膜具有非常高的电荷载流子迁移率，即当在SiO 2衬底上测量时，具有至少15000cm 2 / V-sec的至少10000cm2 / V-sec的至少20000cm2 / V- 秒，至少25000cm2 / V-sec或甚至至少30000cm2 / V-sec。

65. 发明申请

US20160096734A2 Method of Producing a Freestanding Thin Film of Nano-Crystalline Carbon 有权
标题翻译：制备纳米晶碳独立薄膜的方法
公开(公告)号：US20160096734A2
公开(公告)日：2016-04-07
申请号：US14560919
申请日：2014-12-04
申请人： FEI Company , Max-Planck-Gesellschaft zur Forderung der Wissenschaften e.V
发明人： Bart Buijsse , Radostin Stoyanov Danev , Kasim Sader
IPC分类号： C01B31/04 , H01J37/31 , H01J37/22
CPC分类号： C01B32/20 , H01J37/20 , H01J37/22 , H01J37/26 , H01J37/31 , H01J2237/3114
摘要： A freestanding thin film of nano-crystalline graphite is described, as well as a method of producing a freestanding thin film of nano-crystalline graphite including: providing a freestanding thin film of amorphous carbon, heating the freestanding thin film to a high temperature in an inert atmosphere or in a vacuum; and allowing the freestanding thin film to cool down, as a result of which a freestanding thin film of nano-crystalline graphite is formed. The films can be used, for example, as phase plates in a Transmission Electron Microscope.
摘要翻译：描述了独立的纳米晶体石墨薄膜，以及制造纳米晶体石墨的独立薄膜的方法，包括：提供独立的无定形碳薄膜，将独立的薄膜加热到高温下惰性气氛或真空中; 并且允许独立的薄膜冷却，由此形成独立的纳米晶体石墨薄膜。这些膜可以用作例如透射电子显微镜中的相位板。

66. 发明授权

US09295979B2 Synthesis of nanosized metal carbides on graphitized carbon as supporting materials for electrocatalysts 有权
标题翻译：在石墨化碳上作为电催化剂的辅助材料合成纳米金属碳化物
公开(公告)号：US09295979B2
公开(公告)日：2016-03-29
申请号：US14002408
申请日：2011-03-01
申请人： Mei Cai , Peikang Shen , Guoqiang He , Zaoxue Yan , Hui Meng , Chunyong He
发明人： Mei Cai , Peikang Shen , Guoqiang He , Zaoxue Yan , Hui Meng , Chunyong He
IPC分类号： B01J27/22 , C01B31/30 , C01B31/34 , C01B31/04 , H01M4/92 , B01J37/08 , B01J37/30 , B01J37/34 , B01J35/00
CPC分类号： B01J27/22 , B01J35/0013 , B01J35/0033 , B01J37/084 , B01J37/30 , B01J37/346 , C01B32/20 , C01B32/90 , C01B32/949 , H01M4/925 , H01M4/926
摘要： Particles of a macro-porous ion exchange resin are dispersed in a solution of a transition metal compound, such as a compound of molybdenum, tungsten, or vanadium. The resin may be composed for anion exchange or cation ion exchange and, correspondingly, anions or cations of the metal are exchanged onto active ion exchange sites on the molecular chains of the resin. The resin is then carbonized and graphitized to form nanometer-size particles of transition metal carbide on particles of graphite. The composite metal carbide and graphite particles are electrically conductive and serve well as support particles for later deposited particles of a platinum group metal or other catalyst material in, for example, a catalytic electrode member in an electrochemical cell.
摘要翻译：大孔离子交换树脂的颗粒分散在过渡金属化合物如钼，钨或钒化合物的溶液中。树脂可以用于阴离子交换或阳离子交换，并且相应地，金属的阴离子或阳离子被交换到树脂的分子链上的活性离子交换位点上。然后将树脂碳化并石墨化以在石墨颗粒上形成纳米尺寸的过渡金属碳化物颗粒。复合金属碳化物和石墨颗粒是导电的，并且用作在例如电化学电池中的催化电极构件中的铂族金属或其它催化剂材料的后续沉积颗粒的支撑颗粒。

67. 发明申请

US20160059444A1 Production of highly conductive graphitic films from polymer films 审中-公开
标题翻译：从聚合物薄膜生产高导电性石墨膜
公开(公告)号：US20160059444A1
公开(公告)日：2016-03-03
申请号：US14121387
申请日：2014-08-29
申请人： Yanbo Wang , Bor Z. Jang , David Burton , Lucy Fu , Aruna Zhamu
发明人： Yanbo Wang , Bor Z. Jang , David Burton , Lucy Fu , Aruna Zhamu
IPC分类号： B29C35/02 , C01B31/04
CPC分类号： C01B31/04 , C01B32/20 , C01P2006/10 , C01P2006/32 , C01P2006/40
摘要： A one-step (direct graphitization) process for producing a graphitic film, comprising directly feeding a precursor polymer film, without going through a carbonization step, to a graphitization zone preset at a graphitization temperature no less than 2,200° C. for a period of residence time sufficient for converting the precursor polymer film to a porous graphitic film having a density from 0.1 g/cm3 to 1.5 g/cm3 and retreating the porous graphitic film from the graphitization zone. Preferably, the precursor polymer film is selected from the group consisting of polyimide, polyamide, phenolic resin, polyoxadiazole, polybenzoxazole, polybenzobisoxazole, polythiazole, polybenzothiazole, polybenzobisthiazole, poly(p-phenylene vinylene), polybenzimidazole, polybenzobisimidazole, polyacrylonitrile, and combinations thereof. Preferably, the precursor polymer film contains an amount of graphene sheets or expanded graphite flakes, preferably from 1% to 90% by weight, sufficient for promoting or accelerating graphitization.
摘要翻译：用于生产石墨膜的一步（直接石墨化）方法，包括直接将前体聚合物膜直接进料到不经过碳化步骤的石墨化区域，石墨化区域以石墨化温度不低于2200℃预设一段时间将前体聚合物膜转化为密度为0.1g / cm 3至1.5g / cm 3的多孔石墨膜，并从石墨化区域中回收多孔石墨膜的足够的停留时间。优选地，前体聚合物膜选自聚酰亚胺，聚酰胺，酚醛树脂，聚恶二唑，聚苯并恶唑，聚苯并双恶唑，聚噻唑，聚苯并噻唑，聚苯并二噻唑，聚（对亚苯基亚乙烯基），聚苯并咪唑，聚苯并双咪唑，聚丙烯腈及其组合。优选地，前体聚合物膜含有足以促进或加速石墨化的量的石墨烯片或膨胀石墨片，优选为1重量％至90重量％。

68. 发明申请

US20160017128A1 CHEMICALLY MULTI-FUNCTIONAL NANOMATERIALS FOR COMPOSITE STRUCTURES AND METHOD OF PRODUCTION THEREOF 审中-公开
标题翻译：用于复合结构的化学多功能纳米材料及其生产方法
公开(公告)号：US20160017128A1
公开(公告)日：2016-01-21
申请号：US14708674
申请日：2015-05-11
申请人： SABANCI ÜNIVERSITESI
发明人： Serkan ÜNAL , Mehmet YILDIZ
IPC分类号： C08K5/5465 , C07C263/16 , C07F7/10 , C08K5/5435 , C07D301/00 , C07F7/08 , C08K5/29 , C08K5/54 , C07C265/00 , C07D303/22
CPC分类号： C08K5/5465 , B82Y30/00 , B82Y40/00 , C01B21/064 , C01B32/152 , C01B32/174 , C01B32/194 , C01B32/20 , C01P2004/13 , C07C263/16 , C07C265/00 , C07D301/00 , C07D303/22 , C07F7/08 , C07F7/0801 , C07F7/0812 , C07F7/10 , C08J5/24 , C08K5/29 , C08K5/5403 , C08K5/5435 , D06M2101/40 , D06M2200/50
摘要： A chemically multi-functional nanomaterial for use as binding agent in composite structures having at least two components chemically different from each other, wherein said chemically multi-functional nanomaterial is provided with a first functional group and at least a second functional group different from said first functional group, is proposed. Also two alternative methods for production of said chemically multi-functional nanomaterial is proposed. Further, a composite structure comprising said chemically multi-functional nanomaterial is proposed.
摘要翻译：一种化学多功能纳米材料，其用作具有化学上不同的至少两种组分的复合结构中的结合剂，其中所述化学多功能纳米材料具有不同于所述第一官能团的第一官能团和至少第二官能团功能组。还提出了用于生产所述化学多功能纳米材料的两种替代方法。此外，提出了包含所述化学多功能纳米材料的复合结构。

69. 发明申请

US20150364265A1 METHOD FOR PREPARING FLUORINE/NITROGEN CO-DOPED GRAPHITIZED CARBON MICROSPHERES WITH HIGH VOLUMETRIC SPECIFIC CAPACITANCE 有权
标题翻译：用于制备具有高体积电容器的氟/氮共沉淀碳纳米微球的方法
公开(公告)号：US20150364265A1
公开(公告)日：2015-12-17
申请号：US14672454
申请日：2015-03-30
申请人： Yanshan University
发明人： FAMING GAO , Junshuang ZHOU , Junchuan ZHANG , Zhichao LI , Li HOU
IPC分类号： H01G11/34 , H01G11/38 , H01G11/44
CPC分类号： H01G11/34 , C01B31/04 , C01B32/20 , C01P2004/32 , C01P2004/61 , H01G11/42 , H01G11/44 , Y02E60/13
摘要： A method for preparing fluorine/nitrogen co-doped graphitized carbon microspheres with high volumetric specific capacitance, mainly comprises: successively adding a carbon source, a nitrogen source, a fluorine source and a surfactant to a reactor under a nitrogen atmosphere, and stirring for 10-30 minutes before sealing the reactor; placing the reactor into a crucible furnace, heating at 300-600° C., for 6-48 hours, followed by naturally codling the reactor to room temperature and removing the reaction mixture therefrom; successively washing the resulted reaction mixture with absolute ethanol, 0.1 M-5 M diluted hydrochloride acid and distilled water for 3-6 times, filtering, and placing powder thus obtained in a vacuum oven and drying in vacuum at 60-100° C. for 6-12 hours. The present invention provides a simple process with moderate reaction conditions, high reproducibility, and low costs. The fluorine/nitrogen co-doped graphitized carbon microspheres prepared according to the present invention have a very high density, exhibit good electrochemical properties in an alkaline environment, as well as very high volumetric specific capacitance and good cyclic stability, and is of great importance in improving the properties of the electrode material for a capacitor.
摘要翻译：制备具有高体积比电容的氟/氮共掺杂石墨化碳微球的方法主要包括：在氮气氛下向反应器中连续加入碳源，氮源，氟源和表面活性剂，并搅拌10 -30分钟前密封反应堆; 将反应器放入坩埚炉中，在300-600℃下加热6-48小时，然后将反应器自然地加热至室温并从其中除去反应混合物; 依次用无水乙醇，0.1M-5M稀盐酸和蒸馏水将所得反应混合物洗涤3-6次，过滤并将如此获得的粉末置于真空烘箱中并在60-100℃真空干燥，得 6-12小时。本发明提供了具有中等反应条件，高重现性和低成本的简单方法。根据本发明制备的氟/氮共掺杂石墨化碳微球具有非常高的密度，在碱性环境中表现出良好的电化学性质，以及非常高的体积比电容和良好的循环稳定性，并且在改善用于电容器的电极材料的性质。

70. 发明申请

US20150360954A1 SEGMENTED GRAPHENE GROWTH ON SURFACES OF A PATTERNED SUBSTRATE LAYER AND DEVICES THEREOF 有权
标题翻译：图案基底层表面上分离的石墨生长及其装置
公开(公告)号：US20150360954A1
公开(公告)日：2015-12-17
申请号：US14761290
申请日：2014-01-15
申请人： Mark Alan DAVIS , SOLAN, LLC
发明人： Mark Alan DAVIS
IPC分类号： C01B31/04
CPC分类号： C01B32/182 , C01B32/00 , C01B32/152 , C01B32/16 , C01B32/18 , C01B32/184 , C01B32/186 , C01B32/188 , C01B32/20 , C01B2204/04 , C23C14/0605 , C23C14/34 , C23C16/04 , C23C16/26 , H01L21/02 , H01L21/02104 , H01L21/02115 , H01L21/02225 , H01L21/0226 , H01L21/02263 , H01L21/02266 , H01L21/02271 , H01L21/02296 , H01L21/02318 , H01L21/0237 , H01L21/02527 , H01L21/02587 , H01L21/0262 , H01L21/02628 , H01L21/02631 , H01L21/02636 , H01L21/02645 , H01L21/2855 , H01L21/28556 , H01L21/28562 , H01L29/1606 , H01L29/413 , H01L29/66015
摘要： A method of forming a graphite-based structure on a substrate comprises patterning the substrate thereby forming a plurality of elements on the substrate. Each respective element in the plurality of elements is separated from an adjacent element on the substrate by a corresponding trench in a plurality of trenches on the substrate and each respective element in the plurality of elements has a corresponding top surface. The method further comprises segmentedly depositing a graphene initiating layer onto the top surface of each respective element in the plurality of elements; and generating graphene using the graphene initiating layer thereby forming the graphite-based structure.
摘要翻译：在基板上形成石墨基结构的方法包括使基板形成图案，从而在基板上形成多个元件。多个元件中的每个元件通过衬底上的多个沟槽中的对应沟槽与衬底上的相邻元件分离，并且多个元件中的每个相应元件具有对应的顶表面。该方法还包括在多个元件中的每个相应元件的顶表面上分段沉积石墨烯起始层; 并使用石墨烯起始层产生石墨烯，从而形成基于石墨的结构。

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