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    • 65. 发明申请
    • METHOD FOR PRODUCING FLUOROALKYL ALCOHOL
    • 生产氟代醇的方法
    • US20100168480A1
    • 2010-07-01
    • US12451659
    • 2008-05-23
    • Akinari SugiyamaAtsushi SuzukiMasahiro Tomita
    • Akinari SugiyamaAtsushi SuzukiMasahiro Tomita
    • C07C31/34
    • C07C29/00C07C31/38
    • The present invention provides a method for producing a fluoroalkyl alcohol represented by general formula (6) wherein Rf1 and Rf2 are the same or different, each represents a CF3(CF2)n group (wherein n is an integer of 0 to 10) or a CH3(CH2)m group (wherein m is an integer of 0 to 10), and at least one of Rf1 and Rf2 represents a CF3(CF2)n group, the method comprising: decarboxylating a compound represented by general formula (1) wherein Rf1 and Rf2 are the same as above; and R1 represents an optionally substituted alkyl group, an optionally substituted aryl group, an optionally substituted aralkyl group, an alkali metal, or M1/2 (wherein M represents an alkaline earth metal), in the presence of at least one member selected from the group consisting of pyridines, amines, quaternary ammonium salts, and quaternary phosphonium salts.According to the present invention, fluoroalkyl alcohol such as hexafluoroisopropyl alcohol can be easily produced with high selectivity, using an inexpensive starting material.
    • 本发明提供一种通式(6)表示的氟烷基醇的制造方法,其中Rf1和Rf2相同或不同,分别表示CF3(CF2)n基(其中n为0〜10的整数)或 CH 3(CH 2)m基团(其中m为0〜10的整数),Rf 1和Rf 2中的至少一个为CF 3(CF 2)n基团,该方法包括:将通式(1)表示的化合物脱羧, Rf1和Rf2与上述相同; 并且R 1表示任选取代的烷基,任选取代的芳基,任选取代的芳烷基,碱金属或M 1/2(其中M表示碱土金属),在选自 由吡啶,胺,季铵盐和季鏻盐组成的组。 根据本发明,使用廉价的原料,可以以高选择性容易地制备氟代烷基醇如六氟异丙醇。
    • 68. 发明授权
    • Apparatus for inserting insulation sheets into slots of a stator core
    • 用于将绝缘片插入定子芯的槽中的装置
    • US5553372A
    • 1996-09-10
    • US317571
    • 1994-10-04
    • Takayuki TsugawaMasahiro Tomita
    • Takayuki TsugawaMasahiro Tomita
    • H02K3/34H02K15/10
    • H02K15/105Y10T29/49009Y10T29/53152
    • A method of inserting a pair of connecting portions of an insulation sheet into the slots in a stator core is disclosed. The insulation sheet includes a pair of body portions interconnected at their opposite ends by the connecting portions. The top sheet in a stack of insulation sheets is picked up and manipulated to be disposed in a vertical position. The vertically disposed insulation sheet is then gripped at positions slightly spaced inwardly from the opposite end areas of each body portion. After being gripped, the sheet is moved to a position above the stator core. At the position above the core, the intermediate area of each body portion is bowed to assume a "U" shape whereas the opposite end areas of each body portion are disposed in registry with predetermined slots of the stator core, respectively. Then, the bowed insulation sheet is moved in a direction parallel to the axis of the stator core into the center of the core, and thereby the connecting portions of the sheet are inserted into the appropriate slots.
    • 公开了一种将绝缘片的一对连接部分插入定子芯中的槽中的方法。 绝缘片包括在其相对端部处由连接部互连的一对主体部。 拾取和操作堆叠的绝缘片中的顶片以垂直位置布置。 然后垂直设置的绝缘片被夹持在与每个主体部分的相对端部区域向内略微间隔开的位置处。 夹紧后,片材移动到定子铁芯上方的位置。 在芯部上方的位置,每个主体部分的中间区域被弯曲为呈“U”形,而每个主体部分的相对的端部区域分别设置成与定子芯的预定槽对准。 然后,将弓形绝缘片沿着与定子芯的轴线平行的方向移动到芯的中心,从而将片的连接部插入适当的槽中。