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51. 发明授权

US09249075B2 Process for producing porous or finely divided solid inorganic materials 有权
标题翻译：生产多孔或细分固体无机材料的方法
公开(公告)号：US09249075B2
公开(公告)日：2016-02-02
申请号：US14172122
申请日：2014-02-04
申请人： BASF SE
发明人： Johann Martin Szeifert , Michael Kutschera
IPC分类号： C07C29/32 , C01B33/154 , C01B33/155 , C01B33/158
CPC分类号： C07C29/32 , C01B33/154 , C01B33/155 , C01B33/158 , Y02P20/544
摘要： The present invention relates to a process for producing porous or finely divided solid inorganic materials, the surface of which has been modified with at least one organic substance, under supercritical conditions, wherein the supercritical conditions are lowered by addition of an inert organic substance.
摘要翻译：本发明涉及在超临界条件下，其表面已用至少一种有机物质改性的多孔或微细固体无机材料的制备方法，其中通过加入惰性有机物质来降低超临界条件。

52. 发明授权

US09155298B2 Loaded gel particles for anti-fouling compositions 有权
标题翻译：用于防污组合物的装载凝胶颗粒
公开(公告)号：US09155298B2
公开(公告)日：2015-10-13
申请号：US13582045
申请日：2011-03-02
申请人： Henrik Tofte Jespersen
发明人： Henrik Tofte Jespersen
IPC分类号： A61K9/14 , A01N25/10 , B01J13/00 , C01B33/158 , C09D5/16 , C09D7/12 , A61K9/16 , C08K3/08
CPC分类号： A01N25/10 , A61K9/1694 , B01J13/0069 , C01B33/1585 , C08K3/08 , C09D5/165 , C09D5/1687 , C09D7/62 , C09D7/70
摘要： The present invention provides polishing control components for anti-fouling paints for vessels which comprise rosin or other water-degradable polymers entrapped in gel particles, such as aerogel or aeromosil particles.
摘要翻译：本发明提供了用于容器的防污涂料的抛光控制组分，其包含包埋在诸如气凝胶或气体颗粒之类的凝胶颗粒中的松香或其它水可降解聚合物。

53. 发明申请

US20150141532A1 Solvent-Substitution Solvent Used in Aerogel Production, and Hydrophobised Aerogel Production Method Using Same 审中-公开
标题翻译：用于气凝胶生产中的溶剂替代溶剂和使用其的疏水性气凝胶生产方法
公开(公告)号：US20150141532A1
公开(公告)日：2015-05-21
申请号：US14398843
申请日：2013-05-09
申请人： REMTECH CO., LTD.
发明人： Byoung-Hoon Kim , Jeong-Kun Yoo , Jung-Ho Han , Roshan Wagle
IPC分类号： C01B33/155 , C01B33/158
CPC分类号： C01B33/155 , C01B33/14 , C01B33/152 , C01B33/1585
摘要： Provided are a solvent-substitution solvent for producing a hydrophobized aerogel and a method for producing a hydrophobized aerogel. The solvent-substitution solvent includes pentanol in an amount of 41 wt % to 100 wt % and n-butanol in an amount of 0 wt % to 59 wt %. The method includes performing a solvent substitution process using the solvent-substitution solvent. If the solvent-substitution solvent is used for solvent substitution and/or hydrophobization in an aerogel production process, water (moisture) contained in a wet gel may be effectively substituted with the solvent-substitution solvent, and the solvent-substitution solvent may easily be collected at a high degree of purity and may be reused if necessary. Therefore, the rate of solvent loss may be minimized. In addition, if the solvent-substitution solvent is used for solvent substitution, a hydrophobized aerogel may be obtained without having to perform a hydrophobizing process using an additional hydrophobizing agent such as a silylating agent.
摘要翻译：提供用于制备疏水化气凝胶的溶剂置换溶剂和制备疏水化气凝胶的方法。溶剂置换溶剂包括41重量％至100重量％的戊醇和0重量％至59重量％的正丁醇。该方法包括使用溶剂置换溶剂进行溶剂置换过程。如果在气凝胶制造方法中使用溶剂置换溶剂进行溶剂置换和/或疏水化，则可以用溶剂置换溶剂有效地取代湿凝胶中所含的水分（水分），溶剂置换溶剂容易以高纯度收集，如果需要可以重复使用。因此，可以使溶剂损失的速度最小化。此外，如果使用溶剂置换溶剂进行溶剂置换，则可以不使用另外的疏水化剂如甲硅烷基化剂进行疏水化处理来获得疏水化气凝胶。

54. 发明申请

US20120225003A1 METHOD OF PREPARING SILICA AEROGEL POWDER 有权
标题翻译：制备二氧化硅气泡粉的方法
公开(公告)号：US20120225003A1
公开(公告)日：2012-09-06
申请号：US13099936
申请日：2011-05-03
申请人： Young Chul JOUNG , Myung Je Roe , Young Jong Yoo , Jong Chul Park , Hee Jung Choi , Min Woo Kim
发明人： Young Chul JOUNG , Myung Je Roe , Young Jong Yoo , Jong Chul Park , Hee Jung Choi , Min Woo Kim
IPC分类号： C01B33/158
CPC分类号： C01B33/158 , C01B33/166
摘要： A method of preparing silica aero-gel powders having a short preparation time and stable preparation processes. In the method, the silica aerogel powders are generated by using a water glass solution, an inorganic acid, an organosilane compound and an organic solvent. The method includes dispersion-solution generating, gelating and solvent exchanging and drying. In the dispersion-solution generating, a dispersion solution is generated by dispersing the water glass solution and the organosilane compound in the organic solvent. In the gelating and solvent exchanging, silica hydrogel is generated by adding the inorganic acid to the dispersion solution and simultaneously performing gelating and solvent-exchanging. In the drying, the silica aerogel powders are generated by drying the silica hydro-gel.
摘要翻译：一种制备具有较短制备时间和稳定制备方法的二氧化硅气凝胶粉末的方法。在该方法中，通过使用水玻璃溶液，无机酸，有机硅烷化合物和有机溶剂来生成二氧化硅气凝胶粉末。该方法包括分散溶液产生，凝胶化和溶剂交换和干燥。在分散液生成中，通过将水玻璃溶液和有机硅烷化合物分散在有机溶剂中而产生分散液。在凝胶化和溶剂交换中，通过向分散液中加入无机酸，同时进行凝胶化和溶剂交换，生成二氧化硅水凝胶。在干燥过程中，通过干燥二氧化硅水凝胶来生成二氧化硅气凝胶粉末。

55. 发明授权

US08114371B2 Process for production of precipitated silica from olivine 有权
标题翻译：从橄榄石生产沉淀二氧化硅的方法
公开(公告)号：US08114371B2
公开(公告)日：2012-02-14
申请号：US10585475
申请日：2005-01-13
申请人： Gudmundur Gunnarsson , Oddmund Wallevik , Lars Øyvind Ekornrød , Birger Langseth , Per Bjøm Engseth
发明人： Gudmundur Gunnarsson , Oddmund Wallevik , Lars Øyvind Ekornrød , Birger Langseth , Per Bjøm Engseth
IPC分类号： C01B33/12 , C01B33/148 , C01B33/158
CPC分类号： C09C1/3018 , C01B33/187 , C01P2004/61 , C01P2006/12 , C01P2006/19 , C09C1/30 , C09C1/3009 , C09C1/3045 , Y10T428/2982
摘要： Process for the production of precipitated silica from olivine including the following steps: providing olivine particles with a particle size preferably below 1 mm in diameter, preferably mixing olivine and water to form an olivine/water slurry, mixing the olivine/water slurry with hydrochloric acid (HCl), preferably at a Concentration at 18 wt % or above, and at a temperature preferably between 50 -130° C., and reacting for a period of time, preferably between 20-360 minutes, removal of coarse mineral impurities (sand product), separation of precipitated silica from mother solution, mechanical treatment of the separated precipitated silica and optionally some water to obtain a slurry, preparation of a low viscosity slurry by adding sodium aluminate or another suitable aluminate, preferably to 100-6000 p.p.m., and adjusting the pH, preferably to values between 4-9 ageing at a temperature between 50-150° C. according to product requirements dispersion of silica slurry removal of fine mineral impurities (sand product) drying of the silica.
摘要翻译：用于从橄榄石生产沉淀二氧化硅的方法，包括以下步骤：提供直径优选小于1mm的粒度的橄榄石颗粒，优选混合橄榄石和水以形成橄榄石/水浆料，将橄榄石/水浆料与盐酸混合（HCl），优选浓度为18重量％或更高，温度优选为50-130℃，并反应一段时间，优选20-360分钟，除去粗的矿物杂质（砂产物），将沉淀二氧化硅与母溶液分离，对分离的沉淀二氧化硅和任选的一些水进行机械处理以获得浆料，通过加入铝酸钠或另一种合适的铝酸盐制备低粘度浆料，优选为100-6000ppm，以及根据产品要求调节pH，优选在4-9之间的温度在50-150℃之间的老化值。二氧化硅浆液的分散除去细矿物杂质（砂制品）干燥二氧化硅。

56. 发明授权

US07452518B2 Process for treating synthetic silica powder and synthetic silica powder treated thereof 有权
标题翻译：处理合成二氧化硅粉末和合成二氧化硅粉末的方法
公开(公告)号：US07452518B2
公开(公告)日：2008-11-18
申请号：US11266575
申请日：2005-11-02
申请人： Richard L. Hansen , Theodore P. Kircher , Douglas M. Korwin
发明人： Richard L. Hansen , Theodore P. Kircher , Douglas M. Korwin
IPC分类号： C01B33/158
CPC分类号： C01B33/18 , C03C1/022
摘要： A process for producing a synthetic quartz glass powder which is substantially free of carbon contaminant, for reduced bubble density and improved stability of articles made from the synthetic quartz glass during fusion molding by maintaining the synthetic silica powder in an oxidizing environment, e.g., an atmosphere comprising at least 3 vol. % ozone at a temperature of less than 1400° C., causing carbon containing compounds to be reduced to less than 10 ppm.
摘要翻译：一种制造基本上不含碳污染物的合成石英玻璃粉末的方法，用于通过将合成二氧化硅粉末保持在氧化环境例如大气中，在熔融成型期间通过合成石英玻璃制造的制品的气泡密度降低和稳定性提高包括至少3体积％在低于1400℃的温度下的臭氧％，使含碳化合物减少到小于10ppm。

57. 发明申请

US20050244323A1 Method for the preparation of aerogels 失效
标题翻译：气凝胶的制备方法
公开(公告)号：US20050244323A1
公开(公告)日：2005-11-03
申请号：US10519986
申请日：2003-06-24
申请人： Lorenzo Costa , Fulvio Costa
发明人： Lorenzo Costa , Fulvio Costa
IPC分类号： B01D11/00 , B01J13/00 , C01B33/158 , C01B33/12
CPC分类号： B01J13/0091 , C01B33/1585
摘要： A method for the preparation of aerogels that involves the exchange of the liquid present in the aquagel with xenon and the subsequent extraction thereof.
摘要翻译：一种用于制备气凝胶的方法，其涉及将鳗鱼中存在的液体与氙气交换并随后进行萃取。

58. 发明申请

US20050176864A1 Silicon composition 有权
标题翻译：硅组成
公开(公告)号：US20050176864A1
公开(公告)日：2005-08-11
申请号：US10515785
申请日：2003-05-27
申请人： Hagen Demes , Helmut Fackler
发明人： Hagen Demes , Helmut Fackler
IPC分类号： C04B38/00 , C01B33/155 , C01B33/158 , C04B35/00 , C04B35/16 , C04B35/18 , C04B35/63 , C04B35/66 , C08G77/48 , C08K3/00 , C22B1/244 , C08K3/10 , C08K3/34
CPC分类号： C04B35/6303 , C04B35/18 , C04B35/63 , C04B35/632 , C04B35/634 , C04B35/66 , C04B2235/3208 , C04B2235/3217 , C04B2235/3409 , C04B2235/3418 , C04B2235/349 , C04B2235/449 , C04B2235/483 , C04B2235/5463 , C04B2235/77 , C04B2235/9607 , C04B2235/9692 , C08G77/48 , C08K3/013 , C22B1/244
摘要： This invention provides a silicon composition comprising at least 15 wt % of hydrolysed silicon compounds and at least 3 wt % of a binder material. The silicon composition is used in the manufacture of ceramics. The hydrolysed silicon compounds can for example be the gel produced by hydrolysing higher boiling point organohalosilanes produced in the manufacture of organohalosilanes or halosilanes by the direct process.
摘要翻译：本发明提供一种硅组合物，其包含至少15重量％的水解硅化合物和至少3重量％的粘合剂材料。硅组合物用于制造陶瓷。水解的硅化合物可以是例如通过直接方法水解在制备有机卤代硅烷或卤代硅烷中产生的高沸点有机卤代硅烷产生的凝胶。

59. 发明授权

US6106802A Stable synthetic material and method for preparing same 失效
标题翻译：稳定的合成材料及其制备方法
公开(公告)号：US6106802A
公开(公告)日：2000-08-22
申请号：US24069
申请日：1998-02-17
申请人： Juan Lujano , Jose Carrazza , Norma Valencia de Zapata
发明人： Juan Lujano , Jose Carrazza , Norma Valencia de Zapata
IPC分类号： B01J23/44 , B01J20/02 , B01J20/28 , B01J23/46 , B01J35/10 , C01B33/158 , C01B33/46 , C01B37/00 , C01B37/02 , C01B39/00 , B01J21/06
CPC分类号： C01B37/02 , B01J20/02 , B01J20/06 , B01J20/103 , B01J20/3204 , B01J20/3236 , B01J29/0308 , B01J29/0325 , B01J29/041 , B01J35/002 , B01J35/10 , B01J35/1061 , B01J29/0316 , B01J29/0341
摘要： A composition of matter is provided including an inorganic porous material having wall portions defining mesopore-sized channels having a mean diameter of between about 15 .ANG. and about 100 .ANG. and a narrow diameter distribution of less than or equal to about 30 .ANG., the material having a void volume from the mesopore-sized channels of at least about 0.1 cc/g and a surface area of at least about 500 m.sup.2 /g and having a number of hydroxyl groups of at least about 1.5 mmol of hydroxyl groups per gram of material, and exhibiting thermal and hydrothermal stability at temperatures up to about 500.degree. C. Catalytic materials incorporating aluminum and other active metals, as well as a process for preparing the composition, are also disclosed.
摘要翻译：提供了一种物质组合物，其包括无机多孔材料，所述无机多孔材料具有限定中孔尺寸的通道的壁部分，其平均直径为约15至约100，窄直径分布小于或等于约30，所述材料具有来自中孔尺寸的通道的空隙体积为至少约0.1cc / g，表面积为至少约500m 2 / g，并且每克材料具有至少约1.5mmol羟基数量的羟基，并且在高达约500℃的温度下表现出热和水热稳定性。还公开了掺入铝和其它活性金属的催化材料以及制备该组合物的方法。

60. 发明授权

US5811031A Method for the subcritical drying of aerogels 失效
标题翻译：气凝胶亚临界干燥方法
公开(公告)号：US5811031A
公开(公告)日：1998-09-22
申请号：US888774
申请日：1997-07-07
申请人： Rolf-Michael Jansen , Birgit Kessler , Johann Wonner , Andreas Zimmermann
发明人： Rolf-Michael Jansen , Birgit Kessler , Johann Wonner , Andreas Zimmermann
IPC分类号： C08J9/28 , B01J13/00 , B01J21/08 , B01J32/00 , B01J37/03 , B01J37/34 , C01B33/158 , C01B33/16 , B32B7/02 , C01B33/12
CPC分类号： B01J21/08 , B01J13/0091 , B01J37/036 , B01J37/346 , C01B33/1585 , C01B33/16 , Y10S521/915
摘要： Process for the preparation of aerogels by subcritical drying of inorganic and organic hydrogels and lyogels to give aerogels, dielectric drying methods being used.
摘要翻译：通过亚临界干燥无机和有机水凝胶和溶胶凝胶制备气凝胶以制备气凝胶的方法，使用介电干燥方法。

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