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51. 发明申请

US20040009385A1 Composite membrane 有权
标题翻译：复合膜
公开(公告)号：US20040009385A1
公开(公告)日：2004-01-15
申请号：US10429142
申请日：2003-05-02
发明人： David Edward Barnwell , Silvain Buche , Lorenz Gubler , Thomas Robertson Ralph
IPC分类号： H01M008/10 , B05D005/12 , C08J005/22
CPC分类号： C08J5/2206 , B01D69/12 , B01D69/141 , B01J35/065 , C08J2383/02 , H01B1/122 , H01M8/1007 , H01M8/1023 , H01M8/1039 , H01M8/1051 , H01M8/1053 , H01M8/1081 , H01M8/1083 , H01M2300/0082 , H01M2300/0094 , Y02P70/56
摘要： The present invention relates to a composite membrane comprising at least one ion-conducting polymer and a network of randomly orientated individual fibres, wherein there is a continuous region of the membrane at one or both of the membrane faces wherein the density of fibres is lower than the density of fibres in the membrane as a whole. The invention further relates to processes for manufacturing membranes according to the invention, and membrane electrode assemblies comprising membranes according to the invention.
摘要翻译：本发明涉及一种复合膜，其包含至少一种离子导电聚合物和随机取向的单独纤维网络，其中在一个或两个膜面上存在膜的连续区域，其中纤维的密度低于整个膜中纤维的密度。本发明还涉及根据本发明的制造膜的方法和包括根据本发明的膜的膜电极组件。

52. 发明申请

US20030068260A1 Integrated flameless distributed combustion/membrane steam reforming reactor and zero emissions hybrid power system 审中-公开
标题翻译：集成无焰分布式燃烧/膜蒸汽重整反应堆和零排放混合动力系统
公开(公告)号：US20030068260A1
公开(公告)日：2003-04-10
申请号：US10091108
申请日：2002-03-05
发明人： Scott Lee Wellington , Andreas Nikolaos Matzakos , Thomas Mikus , John Michael Ward
IPC分类号： B01J008/02 , B01J008/04
CPC分类号： B01D53/22 , B01D63/06 , B01D2313/38 , B01D2313/42 , B01J8/009 , B01J8/0214 , B01J8/0257 , B01J8/0278 , B01J8/0285 , B01J19/2475 , B01J23/755 , B01J35/065 , B01J2208/00309 , B01J2208/00495 , B01J2208/0053 , B01J2219/00006 , C01B3/323 , C01B3/384 , C01B3/501 , C01B32/50 , C01B2203/0227 , C01B2203/0233 , C01B2203/041 , C01B2203/047 , C01B2203/0475 , C01B2203/048 , C01B2203/06 , C01B2203/065 , C01B2203/066 , C01B2203/068 , C01B2203/0811 , C01B2203/1047 , C01B2203/1052 , C01B2203/1082 , C01B2203/1205 , C01B2203/84 , C01B2203/86 , H01M8/0612 , H01M8/0631 , H01M8/0662 , Y02P20/126 , Y02P20/129 , Y02P20/152 , Y02P20/52 , Y02P30/30
摘要： Disclosed is a new integrated flameless distributed combustion-membrane steam reforming (FDC-MSR) reactor apparatus for steam reforming of any vaporizable hydrocarbon to produce H2 and CO2, with minimal CO, and virtually no CO in the H2 stream. The flameless distributed combustion drives the steam reforming reaction which provides great improvements in heat exchange efficiency and load following capabilities. A further embodiment of the invention involves a zero emission hybrid power system wherein the produced hydrogen is used to power a high-pressure internally manifolded molten carbonate fuel cell. In addition, the design of the FDC-SMR powered fuel cell makes it possible to capture good concentrations of CO2 for sequestration or use in other processes.
摘要翻译：公开了一种用于任何可汽化烃的蒸汽重整以产生H 2和CO 2的最小的CO，并且在H 2流中实际上没有CO的新型无火焰分布式燃烧膜蒸汽重整（FDC-MSR）反应器装置。无焰分布式燃烧驱动蒸汽重整反应，其提供热交换效率和负载跟随能力的极大改进。本发明的另一实施例涉及一种零排放混合动力系统，其中所产生的氢气用于为高压内部歧管的熔融碳酸盐燃料电池供电。此外，FDC-SMR动力燃料电池的设计可以捕获良好的二氧化碳浓度以进行封存或用于其他工艺。

53. 发明申请

US20030039609A1 Zeolite formed product, zeolite laminate intermediate, zeolite laminate composite and method for their preparation 审中-公开
标题翻译：沸石成型产品，沸石层压板中间体，沸石层压复合材料及其制备方法
公开(公告)号：US20030039609A1
公开(公告)日：2003-02-27
申请号：US09980260
申请日：2001-11-01
发明人： Toshihiro Tomita , Shinji Nakamura
IPC分类号： C01F007/00 , C01B033/36 , C01B039/00
CPC分类号： C01B39/04 , B01D53/228 , B01D71/028 , B01D2323/12 , B01J29/035 , B01J29/06 , B01J35/065 , C01B37/02 , Y10S423/22
摘要： A porous zeolite shaped body of a zeolite is characterized in that the porous zeolite shaped body is made of a completely crystallized zeolite or a zeolite still under crystallization and composed of tetrapropylammonium ion (TPA) and silica sol in a mixing ratio (TPA/SiO2) of 0.015 to 0.08 by mole: a zeolite shaped body has an average particle diameter of 1.0 nullm or larger, a bending strength of 1.5 MPa or higher, and a difference in pressure between a feed side and a permeation side of 1.0 atmospheric pressure or lower at 10 ml/cm2.min of helium gas permeation flux when a thickness of the porous zeolite shaped body is adjusted to be 1.8 mm: and a zeolite shaped body has 70% or more of the area of the parts (the sound parts) where respective particles are clearly observed by grain boundary fracture among particles composing the shaped body in the entire area of the fractured surface in microstructure observation of the fractured surface of the shaped body itself.
摘要翻译：沸石的多孔沸石成形体的特征在于，多孔沸石成形体由混合比（TPA / SiO 2）的完全结晶的沸石或仍在结晶下的由四丙基铵离子（TPA）和二氧化硅溶胶构成的沸石构成，为0.015〜0.08摩尔：沸石成型体的平均粒径为1.0μm以上，弯曲强度为1.5MPa以上，进料侧和渗透侧的压力差为1.0大气压以下当多孔沸石成形体的厚度调节为1.8mm时，以10ml / cm2.min的氦气渗透通量测定，沸石成型体的面积（声部）的面积为70％以上，在成形体本身的断裂面的微观结构观察中，在构成成形体的整体区域的粒子之间，通过晶界断裂清楚地观察到各个粒子。

54. 发明申请

US20030000890A1 Tubular membrane and method of making 审中-公开
标题翻译：管状膜及其制造方法
公开(公告)号：US20030000890A1
公开(公告)日：2003-01-02
申请号：US10158392
申请日：2002-05-28
发明人： Nathaniel R. Quick , Michael C. Murray , Matthew R. June , Thomas Peloquin JR.
IPC分类号： B01D039/20
CPC分类号： B01D69/141 , B01D39/2044 , B01D67/0041 , B01D69/04 , B01D69/10 , B01D71/022 , B01D2325/10 , B01J35/065 , B22F3/002 , B22F3/1103 , B22F2999/00 , B22F3/22 , B22F3/10
摘要： An improved tubular membrane and process of making is disclosed comprising the deposition of fine metallic fibers onto a substrate. The deposited fine metallic fibers are heated to form a flexible membrane. Catalytically active particles can be dispersed with the fine metallic fibers. The flexible membrane is wound to form a membrane winding. The membrane winding is sintered for forming a substantially rigid tubular membrane.
摘要翻译：公开了改进的管状膜和制造方法，其包括将细金属纤维沉积到基底上。将沉积的细金属纤维加热以形成柔性膜。催化活性颗粒可以用细金属纤维分散。缠绕柔性膜以形成膜缠绕。膜绕组被烧结以形成基本上刚性的管状膜。

55. 发明申请

US20020141920A1 Metal gas separation membrane module design 失效
标题翻译：金属气体分离膜组件设计
公开(公告)号：US20020141920A1
公开(公告)日：2002-10-03
申请号：US09952186
申请日：2001-09-13
发明人： Mary Anne Alvin , Gerald J. Bruck
IPC分类号： B01J032/00 , B01J008/02
CPC分类号： B01D53/22 , B01D53/228 , B01D67/0069 , B01D67/0072 , B01D69/02 , B01D71/02 , B01D71/022 , B01D71/024 , B01D2325/02 , B01D2325/10 , B01J23/40 , B01J35/065 , C01B3/047 , C01B3/16 , C01B3/503 , C01B3/505 , C01B2203/0283 , Y02E60/364 , Y02P20/52
摘要： An improved metal gas separation membrane for separating hydrogen from a gas steam includes a quantity of metal particles that are bonded together to form a porous body. The porous body may have a porosity that increases from a first surface to an opposite second surface and may additionally include a coating of ceramic particles on the first surface. The metal gas separation membrane may include a coating of a dense precious metal applied thereto that is permeable by hydrogen via chemisorption-dissociation-diffusion. The porous body may include a catalytic enhancement. Also disclosed are three gas separation modules that employ the metal gas separation membrane disposed within a core of the gas separation module for separating hydrogen from a gas stream. The gas separation membranes are each supported on a first mounting member and a second mounting member. The gas separation modules may also include a catalytic enhancement.
摘要翻译：用于从气体蒸汽分离氢的改进的金属气体分离膜包括一定数量的结合在一起以形成多孔体的金属颗粒。多孔体可以具有从第一表面增加到相对的第二表面的孔隙率，并且还可以在第一表面上包括陶瓷颗粒的涂层。金属气体分离膜可以包括施加到其上的致密贵金属的涂层，其通过化学吸附解离扩散由氢可渗透。多孔体可以包括催化增强。还公开了三个气体分离模块，其使用设置在气体分离模块的核心内的金属气体分离膜，用于从气流中分离氢气。气体分离膜各自支撑在第一安装构件和第二安装构件上。气体分离模块还可以包括催化增强。

56. 发明授权

US06448199B1 Hydrophobic composite Pd-membrane catalyst useful for non-hazardous direct oxidation of hydrogen by oxygen to hydrogen peroxide and method of its preparation 失效
标题翻译：疏水复合Pd膜催化剂用于氧气对氧气的非危险的直接氧化过氧化氢及其制备方法
公开(公告)号：US06448199B1
公开(公告)日：2002-09-10
申请号：US09655978
申请日：2000-09-05
申请人： Vasant Ramchandra Choudhary , Subhash Dwarkanath Sansare , Abaji Govind Gaikwad
发明人： Vasant Ramchandra Choudhary , Subhash Dwarkanath Sansare , Abaji Govind Gaikwad
IPC分类号： B01J2342
CPC分类号： B01J23/38 , B01J23/44 , B01J35/065
摘要： A hydrophobic composite Pd-membrane catalyst, useful for the non-hazardous direct oxidation of hydrogen by oxygen to hydrogen peroxide, without a gas phase mixing of hydrogen and oxygen or air, having the general formula: HPM (c)/SOMF (b)/MxPd1−x (a)/IPM wherein, IPM is an inorganic porous membrane, MxPd1−x is a metal alloy, permeable only to hydrogen gas, Pd is a palladium metal; M is a metal other than palladium, or a mixture of two or more thereof; x is a mole fraction of the metal M in the metal alloy (MxPd1−x), a, in the round bracket, is a weight of the metal alloy per unit area of IPM; SOMF is a surface oxidized thin metal film comprising palladium b, in the round bracket, is a thickness of SOMF; HPM is a hydrophobic polymer membrane and c, in the round bracket , is a weight of the HPM per unit area of SOMF and a process for producing the said catalyst.
摘要翻译：具有以下通式的HPM（c）/ SOMF（b））的疏水性复合Pd膜催化剂，其用于将氢气氧化成过氧化氢而无气态混合氢气和空气的非危险性直接氧化， / MxPd1-x（a）/ IPM其中，IPM是无机多孔膜，MxPd1-x是仅对氢气可渗透的金属合金，Pd是钯金属; M是除钯以外的金属，或其两种以上的混合物; x是金属合金（MxPd1-x）中的金属M的摩尔分数，圆形支架中的a是每单位面积IPM的金属合金的重量; SOMF是包含钯b的表面氧化薄金属膜，在圆形支架中是SOMF的厚度; HPM是疏水性聚合物膜，c在圆形支架中，是单位面积的SOMF的HPM的重量和用于生产所述催化剂的方法。

57. 发明申请

US20020094466A1 Composites and composite membranes 有权
标题翻译：复合材料和复合膜
公开(公告)号：US20020094466A1
公开(公告)日：2002-07-18
申请号：US09984564
申请日：2001-10-30
发明人： Jochen Kerres , Thomas Haring , Rima Haring
IPC分类号： H01M008/10 , H01M010/40 , C25B013/00 , C25C007/04 , B01D061/42 , B01D061/44 , B01D069/00 , B01D071/00
CPC分类号： B01D67/0041 , B01D69/141 , B01D71/00 , B01D71/024 , B01D71/62 , B01D71/68 , B01D2325/18 , B01D2325/26 , B01J21/16 , B01J31/10 , B01J31/1633 , B01J35/065 , C08J5/2275 , C08J2383/02 , H01M8/0289 , H01M8/1023 , H01M8/103 , H01M8/1032 , H01M8/1051 , H01M8/1081 , Y02E60/523 , Y02P70/56 , Y10T428/249953 , Y10T428/249969
摘要： The invention relates to a composite or a composite membrane consisting of an ionomer and of an inorganic optionally functionalized phyllosilicate. The isomer can be: (a) a cation exchange polymer; (b) an anion exchange polymer; (c) a polymer containing both anion exchanger groupings as well as cation exchanger groupings on the polymer chain; or (d) a blend consisting of (a) and (b), whereby the mixture ratio can range from 100% (a) to 100% (b). The blend can be ionically and even covalently cross-linked. The inorganic constituents can be selected from the group consisting of phyllosilicates or tectosilicates.
摘要翻译：本发明涉及由离聚物和无机任选官能化的页硅酸盐组成的复合膜或复合膜。异构体可以是：（a）阳离子交换聚合物; （b）阴离子交换聚合物; （c）聚合物链上含有阴离子交换剂组和聚合物链上的阳离子交换剂组的聚合物; 或（d）由（a）和（b）组成的共混物，其混合比可以在100％（a）至100％（b）的范围内。共混物可以是离子的，甚至共价交联的。无机成分可以选自页硅酸盐或三硅酸盐。

58. 发明申请

US20020093008A1 Proton-conducting ceramic/polymer composite membrane for the temperature range up to 300nullC 审中-公开
标题翻译：质子导电陶瓷/聚合物复合膜，温度范围高达300°C
公开(公告)号：US20020093008A1
公开(公告)日：2002-07-18
申请号：US09984531
申请日：2001-10-30
发明人： Jochen Kerres , Norbert Nicoloso , Gunther Schafer
IPC分类号： H01B001/00 , H01C001/00
CPC分类号： B82Y30/00 , B01D69/141 , B01J31/0244 , B01J31/06 , B01J31/08 , B01J35/065 , C08J5/2275 , C08J2371/12 , C08K9/02 , C08K2201/011 , H01M2/166 , H01M8/04197 , H01M8/1011 , H01M8/1025 , H01M8/1027 , H01M8/1032 , H01M8/1048 , H01M8/1067 , H01M8/1081 , H01M2300/0068 , H01M2300/0082 , H01M2300/0091 , Y02E60/523 , Y02P70/56
摘要： A composite membrane comprising organic functional polymers and ceramic nanoparticles (1-100 nm), with the exception of sheet silicates and three-dimensional silicates, with intercalated water and/or a high surface concentration of acidic/basic groups (e.g. hydroxyl) and water. The use of such particles makes possible not only a satisfactorily high mechanical stability of the composite material but also stabilization of the proton concentration necessary for the conductivity in the membrane up to operating temperatures of 300null C. Important factors are the interfaces between polymer and ceramic powder which are formed in the microheterogeneous mixture and allow, if they are present in sufficient number (high proportion of the phase made up of nanosize particles), proton transport at low pressure and temperatures above 100null C. Modification of the polymer/ceramic particle boundary layer by means of different polar boundary groups, preferably on the polymer skeleton, influences the local equilibrium and thus the binding strength of the protic charge carriers. This makes it possible, for example in the case of alcohol/water mixtures as fuel, to reduce the passage of MeOH (where Me is CH3, C2H5, C3H7,) through the membrane, which is of particular importance for the development of efficient direct methanol fuel cells. Apart from fuel cells, other possible applications are the areas in energy and process technology where steam as well as electric power is produced or required or where (electro) chemically catalyzed reactions are carried out at elevated temperatures at from atmospheric pressure to superatmospheric pressures and/or under an atmosphere of water vapor. The invention further relates to a process for producing and processing such a composite membrane.
摘要翻译：包含有机官能聚合物和陶瓷纳米颗粒（1-100nm）的复合膜，除了硅酸盐和三维硅酸盐之外，具有插层的水和/或高表面浓度的酸性/碱性基团（例如羟基）和水。使用这种颗粒不仅使复合材料具有令人满意的高机械稳定性，而且使得膜的导电性所需的质子浓度稳定至300℃的工作温度。重要的因素是聚合物和陶瓷之间的界面在微不均匀混合物中形成的粉末，如果它们以足够数量（由纳米尺寸颗粒组成的相的高比例）存在，则在低压和高于100℃的温度下质子传输。聚合物/陶瓷颗粒的改性边界层通过不同的极性边界基团，优选在聚合物骨架上，影响局部平衡，从而影响质子电荷载体的结合强度。这使得例如在醇/水混合物作为燃料的情况下可以通过膜减少MeOH（其中Me是CH 3，C 2 H 5，C 3 H 7）的通过，这对于开发有效的直接特别重要甲醇燃料电池。除了燃料电池之外，其他可能的应用是能量和工艺技术领域，其中产生或需要蒸汽和电力，或其中（电）化学催化反应在大气压至高于大气压的高温下进行和/ 或在水蒸汽气氛下。本发明还涉及一种生产和加工这种复合膜的方法。

59. 发明申请

US20020022568A1 Ceramic membranes for use in catalytic membrane reactors with high ionic conductivities and improved mechanical properties 审中-公开
标题翻译：陶瓷膜用于具有高离子电导率和改进的机械性能的催化膜反应器
公开(公告)号：US20020022568A1
公开(公告)日：2002-02-21
申请号：US09905651
申请日：2001-07-13
发明人： Richard Mackay , Anthony F. Sammells
IPC分类号： B01J023/10 , C01B003/26 , C04B035/50
CPC分类号： B01D53/228 , B01D53/326 , B01D67/0041 , B01D67/0083 , B01D69/141 , B01D71/02 , B01D71/022 , B01D71/024 , B01D2323/08 , B01D2323/12 , B01J4/04 , B01J12/007 , B01J19/2475 , B01J23/002 , B01J23/83 , B01J35/0033 , B01J35/065 , B01J2219/00051 , B01J2219/00063 , B01J2219/0018 , B01J2219/00189 , B01J2523/00 , C01B3/36 , C01B3/386 , C01B13/0255 , C01B17/0465 , C01B2203/0261 , C01B2203/1035 , C01B2203/1041 , C01B2203/1052 , C01B2203/1082 , C01B2203/1241 , C01B2203/1258 , C01B2210/0046 , C01B2210/0051 , C01B2210/0062 , C01B2210/0071 , C01B2210/0075 , C01C3/0216 , H01M4/9033 , H01M4/9066 , H01M8/1231 , H01M8/1246 , Y02E60/525 , Y02P20/52 , Y02P70/56 , B01J2523/24 , B01J2523/3706 , B01J2523/842 , B01J2523/23 , B01J2523/31 , B01J2523/845 , B01J2523/22 , B01J2523/32
摘要： Ceramics of the composition:Ln1-xSryCax-yMO3-nullwhere Ln is an element selected from the f block lanthanides and yttrium or mixtures thereof; M is an element selected from the d block transition metals or mixtures thereof; 0.1nullxnull0.4; 0.01nullynull0.25 and null is a number that varies to maintain charge neutrality are provided along with methods of their use. These ceramics are useful in making and using gas-impermeable ceramic membranes that exhibit high electronic and ionic conductivity, low coefficients of expansion and high chemical and thermal stability under catalytic membrane reactor conditions. The ceramics provided are particularly useful for promotion of oxidation-reduction reactions and for separating molecular oxygen from oxygen containing gases.
摘要翻译：陶瓷的组成：<段落lvl =“0”> Ln1-xSryCax-yMO3-delta 其中Ln是从f块中选择的元素镧系元素和钇或混合物的; M是选自d嵌段过渡金属或其混合物的元素; 0.1 <= x <= 0.4; 0.01 <= y <= 0.25，并且delta是维持电荷中性而变化的数字及其使用方法。这些陶瓷可用于制造和使用气体不可渗透的陶瓷膜，其在催化膜反应器条件下表现出高电子和离子电导率，低膨胀系数和高的化学和热稳定性。提供的陶瓷对于促进氧化还原反应和从含氧气体中分离分子氧是特别有用的。

60. 发明授权

US06281403B1 Solid state proton and electron mediating membrane and use in catalytic membrane reactors 失效
标题翻译：固态质子和电子介导膜，用于催化膜反应器
公开(公告)号：US06281403B1
公开(公告)日：2001-08-28
申请号：US09457884
申请日：1999-12-10
申请人： James H. White , Michael Schwartz , Anthony F. Sammells
发明人： James H. White , Michael Schwartz , Anthony F. Sammells
IPC分类号： C07C5333
CPC分类号： C07C2/84 , B01J23/002 , B01J35/065 , B01J2523/00 , C07C2527/047 , B01J2523/24 , B01J2523/3712 , B01J2523/842
摘要： Mixed electron- and proton-conducting metal oxide materials are provided. These materials are useful in fabrication of membranes for use in catalytic membrane reactions, particularly for promoting dehydrogenation of hydrocarbons, oligomerization of hydrocarbons and for the decomposition of hydrogen-containing gases. Membrane materials are perovskite compounds of the formula: AB1−xB′xO3−y where A=Ca, Sr, or Ba; B=Ce, Tb, Pr or Th; B′=Ti, V, Cr, Mn, Fe, Co, Ni or Cu; 0.2≦x≦0.5, and y is a number sufficient to neutralize the charge in the mixed metal oxide material.
摘要翻译：提供了混合的电子和质子传导金属氧化物材料。这些材料可用于制造用于催化膜反应的膜，特别是用于促进烃的脱氢，烃的低聚和含氢气体的分解。膜材料是下式的钙钛矿化合物：其中A = Ca，Sr或Ba; B = Ce，Tb，Pr或Th; B'= Ti，V，Cr，Mn，Fe，Co，Ni或Cu; 0.2 <= x <= 0.5，y是足以中和混合金属氧化物材料中的电荷的数。

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