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1. 发明申请

US20030039609A1 Zeolite formed product, zeolite laminate intermediate, zeolite laminate composite and method for their preparation 审中-公开
标题翻译：沸石成型产品，沸石层压板中间体，沸石层压复合材料及其制备方法
公开(公告)号：US20030039609A1
公开(公告)日：2003-02-27
申请号：US09980260
申请日：2001-11-01
发明人： Toshihiro Tomita , Shinji Nakamura
IPC分类号： C01F007/00 , C01B033/36 , C01B039/00
CPC分类号： C01B39/04 , B01D53/228 , B01D71/028 , B01D2323/12 , B01J29/035 , B01J29/06 , B01J35/065 , C01B37/02 , Y10S423/22
摘要： A porous zeolite shaped body of a zeolite is characterized in that the porous zeolite shaped body is made of a completely crystallized zeolite or a zeolite still under crystallization and composed of tetrapropylammonium ion (TPA) and silica sol in a mixing ratio (TPA/SiO2) of 0.015 to 0.08 by mole: a zeolite shaped body has an average particle diameter of 1.0 nullm or larger, a bending strength of 1.5 MPa or higher, and a difference in pressure between a feed side and a permeation side of 1.0 atmospheric pressure or lower at 10 ml/cm2.min of helium gas permeation flux when a thickness of the porous zeolite shaped body is adjusted to be 1.8 mm: and a zeolite shaped body has 70% or more of the area of the parts (the sound parts) where respective particles are clearly observed by grain boundary fracture among particles composing the shaped body in the entire area of the fractured surface in microstructure observation of the fractured surface of the shaped body itself.
摘要翻译：沸石的多孔沸石成形体的特征在于，多孔沸石成形体由混合比（TPA / SiO 2）的完全结晶的沸石或仍在结晶下的由四丙基铵离子（TPA）和二氧化硅溶胶构成的沸石构成，为0.015〜0.08摩尔：沸石成型体的平均粒径为1.0μm以上，弯曲强度为1.5MPa以上，进料侧和渗透侧的压力差为1.0大气压以下当多孔沸石成形体的厚度调节为1.8mm时，以10ml / cm2.min的氦气渗透通量测定，沸石成型体的面积（声部）的面积为70％以上，在成形体本身的断裂面的微观结构观察中，在构成成形体的整体区域的粒子之间，通过晶界断裂清楚地观察到各个粒子。

2. 发明申请

US20020192156A1 MTT zeolite comprising crystals and crystal aggregates with specific granulometries, and its use as a catalyst for isomerising straight chain paraffins 有权
标题翻译：包含晶体的MTT沸石和具有特定粒度的晶体聚集体，以及其作为直链烷烃异构化催化剂的用途
公开(公告)号：US20020192156A1
公开(公告)日：2002-12-19
申请号：US09788480
申请日：2001-02-21
发明人： Loic Rouleau , Frederic Kolenda , Eric Benazzi
IPC分类号： C01B039/00 , C01B033/36
CPC分类号： C10G45/64 , B01J20/18 , B01J29/70 , B01J29/74 , B01J35/023 , B01J2229/26 , B01J2229/42 , C01B39/48 , Y10S423/36
摘要： The invention concerns a zeolite with structure type MTT comprising MTT zeolite crystals with a size of less than 5 nullm, at least a portion of the MTT zeolite crystals being in the form of MTT zeolite crystal aggregates, said zeolite being characterized in that the granulometry of the aggregates is such that the dimension Dv,90 is in the range 40 nm to 100 nullm. The invention also concerns the preparation of the zeolite and the use of the zeolite as a catalyst in a process for converting hydrocarbon feeds, and in particular in a process for isomerising straight chain paraffins molecular sieve formed from an MFI, MEL or null type zeolite by means of the crystallisation temperature It should be noted that these prior art patent applications never mention the specific size of the zeolite crystals and aggregates in combination with particular catalytic properties.
摘要翻译：本发明涉及结构类型为MTT的沸石，其包含尺寸小于5um的MTT沸石晶体，至少一部分MTT沸石晶体为MTT沸石晶体聚集体形式，所述沸石的特征在于，粒度测定聚集体使得尺寸Dv，90在40nm至100μm的范围内。本发明还涉及沸石的制备以及沸石作为转化烃原料的方法中的催化剂的用途，特别是在由MFI，MEL或β型沸石形成的直链烷烃分子筛异构化的方法中，结晶温度的手段应当注意，这些现有技术的专利申请从未提及沸石晶体和聚集体的特定尺寸以及特定的催化性质。

3. 发明申请

US20020192155A1 Macrostructures of porous inorganic material and process for their preparation 失效
标题翻译：多孔无机材料的宏观结构及其制备方法
公开(公告)号：US20020192155A1
公开(公告)日：2002-12-19
申请号：US10117517
申请日：2002-04-05
发明人： Per Johan Sterte , Lubomira Borislavova Tosheva , Valentin Panov Valtchev , Svetlana Ivanova Mintova
IPC分类号： C01B033/36 , C01B033/26 , C01B039/00
CPC分类号： B01J20/28026 , B01J20/08 , B01J20/103 , B01J20/18 , B01J20/28004 , B01J20/28019 , B01J20/28057 , B01J20/2808 , B01J20/28083 , B01J20/28097 , B01J20/305 , B01J29/0308 , B01J29/041 , B01J29/40 , B01J37/0018 , B01J47/018 , B01J2229/60 , C01B33/124 , C01B33/26 , C01B37/02 , C01B39/04 , C01B39/145 , C01B39/40 , C01B39/48 , C04B38/0022 , C08K7/26 , Y10S423/22 , Y10S423/24 , Y10S423/27 , C04B35/03 , C04B38/0054 , C04B38/009 , C04B38/0615 , C04B38/0655 , C04B14/047 , C04B38/04
摘要： There is provided macrostructures of porous inorganic material which can have controlled size, shape, and/or porosity and a process for preparing the macrostructures. The macrostructures comprise a three-dimension network of particles of porous inorganic materials. The process for preparing the macrostructures involves forming an admixture containing a porous organic ion exchanger and a synthesis mixture capable of forming the porous inorganic material and then converting the synthesis mixture to the porous inorganic material. After formation of the composite material, the porous organic ion exchanger can be removed from the composite material to obtain the macrostructures.
摘要翻译：提供了可以具有受控尺寸，形状和/或孔隙率的多孔无机材料的宏观结构以及用于制备宏观结构的方法。宏观结构包括多孔无机材料颗粒的三维网络。制备宏观结构的方法包括形成含有多孔有机离子交换剂和能够形成多孔无机材料的合成混合物的混合物，然后将合成混合物转化为多孔无机材料。在形成复合材料之后，可以从复合材料中除去多孔有机离子交换剂以获得宏观结构。

4. 发明申请

US20020000537A1 Humidity adsorbent agent and humidity adsorbent element using thereof 审中-公开
标题翻译：湿度吸附剂和使用它的湿度吸附剂元素
公开(公告)号：US20020000537A1
公开(公告)日：2002-01-03
申请号：US09863671
申请日：2001-05-23
发明人： Hiroki Daikaku , Takeya Kobayashi , Teruji Yamazaki
IPC分类号： C09K003/00 , C01B033/36 , C01F007/00
CPC分类号： B01J20/186 , B01D53/28 , F24F2203/1036
摘要： To provide a humidity adsorbent agent having duplicating advantages of hydrophilic zeolite and silica gel, and a humidity adsorbent element using thereof, a humidity adsorbent agent is used an alumino-silicate which is replaced a part of sodium to Lanthanide in a hydrophilic zeolite. A humidity adsorbent element is constituted that is supported the agent on a carrier comprised of inorganic fiber paper.
摘要翻译：为了提供具有亲水性沸石和硅胶的重复优点的湿度吸附剂和使用其的湿度吸附剂元件，使用湿式吸附剂，其中将一部分钠替代为亲水性沸石中的镧系元素的铝硅酸盐。构成在由无机纤维纸构成的载体上负载该试剂的湿度吸附剂元件。

5. 发明申请

US20010055562A1 Process for preparing crystalline microporous and mesoporous metal silicates, products obtainable by said process and their use 有权
标题翻译：制备结晶微孔和介孔金属硅酸盐的方法，可通过所述方法获得的产物及其用途
公开(公告)号：US20010055562A1
公开(公告)日：2001-12-27
申请号：US09931025
申请日：2001-08-17
发明人： Steffen Hasenzahl , Helmut Mangold , Eckehart Roland , Mario Scholz , Georg Thiele
IPC分类号： C01F007/00 , C01B033/36 , C01B039/00 , C01B039/04
CPC分类号： B01J29/86 , B01J29/04 , B01J29/89 , C01B37/00 , C01B37/005 , C01B39/065 , C01B39/12 , C07D301/12 , Y10S423/22 , Y10S423/27 , Y10S423/29
摘要： Microporous and mesoporous metal silicates are prepared by the hydrothermal reaction of a silicon and metal source in the presence of a template. The choice of raw materials influences the purity and hence the catalytic activity of the products. A pyrogenic mixed oxide is used as the silicon and metal source. Prepared products have the composition (SiO2)1-x(AmOn)x, where A is Ti, Al, B, V or Zr and x is 0.005 to 0.1. Shaped objects of the microporous and mesoporous metal silicates are obtained directly by using a shaped object of the pyrogenic mixed oxide. The products obtained are used as oxidation catalysts.
摘要翻译：微孔和介孔金属硅酸盐通过硅和金属源的水热反应在模板存在下制备。原料的选择会影响产品的纯度和催化活性。使用热解混合氧化物作为硅和金属源。制备的产品具有组成（SiO 2）1-x（AmOn）x，其中A是Ti，Al，B，V或Zr，x是0.005至0.1。通过使用热解混合氧化物的成形物体直接获得微孔和介孔金属硅酸盐的成形物体。所得产物用作氧化催化剂。

6. 发明申请

US20010041162A1 Process for the manufacture of a crystalline solid 失效
标题翻译：制造结晶固体的方法
公开(公告)号：US20010041162A1
公开(公告)日：2001-11-15
申请号：US09785286
申请日：2001-02-20
申请人： SOLVAY (Societe Anonyme)
发明人： Jean-Paul Schoebrechts
IPC分类号： C01B033/36 , C01B039/00
CPC分类号： C01B37/00 , B01J29/89 , C01B37/005 , C07D301/12
摘要： Process for the manufacture of crystalline solids comprising at least one element chosen from Groups IIIa, IVa and Va and at least one transition metal, according to which at least one source of oxide of the element from Groups IIIa, IVa and Va and at least one transition metal oxide source, which was dissolved beforehand in an alcohol having a pKa below that of water, are hydrolysed in an aqueous medium comprising a mineralizing agent and the gel thus obtained is crystallized in the presence of a structuring agent.
摘要翻译：制备包含至少一种选自IIIa，IVa和Va族的元素的结晶固体的方法和至少一种过渡金属，根据该方法，来自IIIa，IVa和Va族元素的至少一种氧化物源和至少一种将其预先溶解在pKa低于水的醇中的过渡金属氧化物源在包含矿化剂的水性介质中水解，所得凝胶在结构剂存在下结晶。

7. 发明申请

US20010031241A1 Microporous and mesoporous silicoaluminate solid, process for preparation, use as a catalyst and for hydrocarbon conversion 有权
标题翻译：微孔和介孔硅铝酸盐固体，制备方法，用作催化剂和烃转化
公开(公告)号：US20010031241A1
公开(公告)日：2001-10-18
申请号：US09736048
申请日：2000-12-14
发明人： Sylvie Lacombe , David Marseault , Philippe Caullet , Henri Kessler , Eric Benazzi , Alexandre Jouve
IPC分类号： B01J029/06 , B01J021/00 , B01J029/00 , C10G047/00 , C01B033/26 , C01F007/00 , C01B033/36 , C01B039/00
CPC分类号： B01J29/005 , B01J29/0308 , B01J29/041 , B01J29/7007 , B01J29/7415 , B01J2229/42 , C01B39/023 , C10G47/20 , Y10S423/27
摘要： The invention relates to an acidic silicoaluminate solid that has a microporous zeolitic phase that is characterized by at least one infrared band between 400-1600 cm-1, an organized mesoporosity that is characterized by the presence of at least one X-diffraction line between 20-100 null, a silica/alumina molar ratio of between 5-250 and an acidity that is measured by infrared analysis via an area of the band at about 1545 cm-1 at least equal to 50 g of dry solid. The invention also relates to a process for the preparation of the solid, a substrate that consists of solid and at least one matrix, and a catalyst that comprises said solid. The catalyst can be used for the conversion of hydrocarbons and in particular hydrocracking.
摘要翻译：本发明涉及一种酸性硅铝酸盐固体，其具有微孔沸石相，其特征在于至少一个在400-1600cm -1之间的红外波段，有组织的介孔密度，其特征在于存在至少一个X射线在20 -100埃，二氧化硅/氧化铝摩尔比在5-250之间，并且通过红外分析通过在约1545cm -1至少等于50g干固体的带的面积测量的酸度。本发明还涉及制备固体的方法，由固体和至少一种基质组成的底物和包含所述固体的催化剂。催化剂可用于转化烃，特别是加氢裂化。

8. 发明申请

US20040186337A1 Crystalline aluminosilicate zeolitic composition: UZM-15 失效
标题翻译：结晶硅铝酸盐沸石组合物：UZM-15
公开(公告)号：US20040186337A1
公开(公告)日：2004-09-23
申请号：US10395399
申请日：2003-03-21
发明人： Lisa M. Rohde , Gregory J. Lewis , Stephen T. Wilson , Deng-Yang Jan , R. Lyle Patton , Susan C. Koster , Jaime G. Moscoso , Mark A. Miller , Michael G. Gatter
IPC分类号： C07C005/22 , B01J029/04 , B01J029/87 , C01F007/00 , C01B033/36 , C01B039/00 , C07C002/12
CPC分类号： B01J29/87 , B01J29/70 , B01J2229/16 , B01J2229/32 , B01J2229/36 , B01J2229/37 , C01B39/026 , C01B39/082 , C01B39/48 , C01P2002/72 , C07C7/13
摘要： An aluminosilicate zeolite and substituted versions designated UZM-15 have been synthesized. These zeolites are prepared using an organo-ammonium cation as a template in which at least one organic group has at least 2 carbon atoms. An example of such a cation is diethyldimethyl-ammonium cation. The template can optionally comprise other organoammonium cations, alkali metals and alkaline earth metals. These UZM-15 materials can be dealuminated by various processes to provide UZM-15HS compositions. Both the UZM-15 and UZM-15HS compositions are useful as catalysts or catalyst supports in various process such as the conversion of cyclic hydrocarbons to non-cyclic hydrocarbons and olefin oligomerization.
摘要翻译：已经合成了一种硅铝酸盐沸石，并且被认为是UZM-15的取代物。使用有机铵阳离子作为模板制备这些沸石，其中至少一个有机基团具有至少2个碳原子。这种阳离子的实例是二乙基二甲基铵阳离子。模板可任选地包含其它有机铵阳离子，碱金属和碱土金属。这些UZM-15材料可以通过各种工艺脱铝以提供UZM-15HS组合物。 UZM-15和UZM-15HS组合物可用作各种方法中的催化剂或催化剂载体，例如将环烃转化为非环烃和烯烃低聚。

9. 发明申请

US20040105814A1 Process for the preparation of nanocrystalline zeolite beta 失效
公开(公告)号：US20040105814A1
公开(公告)日：2004-06-03
申请号：US10306744
申请日：2002-11-29
发明人： Kottapalli Koteswara Rao , Bhavnari Puma Chandra Rao , Boyapati Manoranjan Choudary , Lakshmi Kantam Mannepalli , Vijaya Raghavan Kondapuram
IPC分类号： C01F007/00 , C01B033/36 , C01B039/00
CPC分类号： C01B39/48 , B01J29/7007 , Y10S423/27
摘要： The present invention relates to the preparation of nanocrystalline zeolite beta by a modified aerogel protocol comprising four steps, namely, hydrolysis, nucleation, crystallization and supercritcal drying.

10. 发明申请

US20040091419A1 Zeolite sol and method for preparing the same, composition for forming porous film, porous film and method for forming the same, interlevel insulator film, and semiconductor device 失效
标题翻译：沸石溶胶及其制备方法，用于形成多孔膜的组合物，多孔膜及其形成方法，层间绝缘膜和半导体器件
公开(公告)号：US20040091419A1
公开(公告)日：2004-05-13
申请号：US10703854
申请日：2003-11-07
发明人： Tsutomu Ogihara , Fujio Yagihashi , Hideo Nakagawa , Masaru Sasago
IPC分类号： C01B039/04 , C01B033/36 , C01F007/00 , C01B039/00
CPC分类号： H01L21/02126 , C01B39/04 , H01L21/02203 , H01L21/02216 , H01L21/02282 , H01L21/31695
摘要： The present invention provides a zeolite sol which can be formed into a porous film that can be thinned to an intended thickness by a method used in the ordinary semiconductor process, that excels in dielectric properties, adhesion, film consistency and mechanical strength, and that can be easily thinned; a composition for film formation; a porous film and a method for forming the same; and a high-performing and highly reliable semiconductor device which contains this porous film inside. More specifically, the zeolite sol is prepared by hydrolyzing and decomposing a silane compound expressed by a general formula: Si(OR1)4 (wherein R1 represents a straight-chain or branched alkyl group having 1 to 4 carbons, and when there is more than one R1, the R1s can be independent and the same as or different from each other) in a conventional coating solution for forming a porous film in the presence of a structure-directing agent and a basic catalyst; and then by heating the silane compound at a temperature of 75null C. or lower. A composition for forming a porous film which contains this zeolite sol is used.
摘要翻译：本发明提供一种沸石溶胶，其可以通过通常的半导体工艺中使用的方法来形成多孔膜，该多孔膜可以被薄化到预期的厚度，其具有优异的介电性能，粘附性，膜稠度和机械强度，并且可以容易变薄; 用于成膜的组合物; 多孔膜及其形成方法; 以及内部含有该多孔膜的高性能，高可靠性的半导体装置。更具体地说，通过水解和分解由以下通式表示的硅烷化合物制备沸石溶胶：Si（OR 1）4（其中R 1表示具有1至4个碳的直链或支链烷基，并且当有多于一个R 1时，R 1可以彼此独立地相同或相同）在常规的在结构导向剂存在下形成多孔膜的涂布溶液和碱性催化剂; 然后在75℃以下的温度下加热硅烷化合物。使用含有该沸石溶胶的多孔膜形成用组合物。

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